和硫

Diallyl trisulfide was synthesized with a yield of 76.4% based on sodium thiosulfate, allyl bromide and sodium sulfide. And diallyl tetrasulfide was synthesized by the reaction of sulfur monochloride with ally1 mercaptan with a yield of 81.0%.

以硫代硫酸钠、烯丙基澳和硫化钠为原料，合成了二烯丙基三硫，产率为76.4%；以一氯化硫和烯丙硫醇为原料合成了二烯丙基四硫，产率为81.0%。

According to the compared analysis of prevention sulfur deposition during the production of high sour gas well, the key of prevent sulfur deposition and to control sulfur blocking is choose right element sulfur, carry out some research on the selection of sulfur solution, remix the triethylenetetramine, diethylenetriamine and monoethanolamine in different ratios, finally formed LJ-1 compounding which is best fit the production of north Sichuan province.

对比分析了多种硫沉积防治方法，防治的关键在于溶硫剂的合理选择，通过溶硫剂优选室内评价实验研究筛选出三乙烯四胺、二乙烯三胺和乙醇胺等三种单剂，按照不同的比例与现场使用的防冻剂乙二醇进行复配，最终形成了适合川东地区高含硫气井的溶硫剂LJ-1合理配方，性能评价实验表明溶硫剂LJ-1溶硫速率快、溶解度高、腐蚀小。

The pyrolysis characteristics and sulfur release characteristics during coal pyrolysis of three different coals, which include high volatile, were studied by TG-GC-MS(Thermal gravimetry-Gas Chromatography-Mass spectrum), tube furnace of pyrolysis reactor and intelligent fixup sulfur equipment.

本文应用热重—质谱—色谱联用系统、管式炉热解反应器和快速智能定硫仪，研究三种高挥发分煤种的热解特性和热解硫析出特性，对热解硫析出的两种主要产物(H_2S和COS)进行了监测分析，得到硫的赋存形态、粒径大小以及矿物质对各种形态含硫气体析出的影响规律。

According to the fluorescence measurement results from mixed solution, the association constant estimated for thioridazine hydrochloride-BSA binding and the number of the binding site with Scatchard analysis were 1.2×104 L/mol and 0.98, respectively.

将盐酸硫利达嗪与牛血清白蛋白以不同比例混合并在37 ℃下培养，以流动注射透析采样技术从混合液中分离出游离盐酸硫利达嗪，在线氧化为强荧光化合物后测定其浓度；应用Scrathard方程分析所测数据，求得盐酸硫利达嗪和牛血清白蛋白的结合常数为1.2×104 L/mol，结合位点数为0.98；根据热力学参数推断，盐酸硫利达嗪与牛血清白蛋白之间以疏水作用力为主；进一步基于荧光猝灭现象和Fster非辐射能量转移理论，得到盐酸硫利达嗪小分子与牛血清白蛋白之间的能量转移效率( E =0.497)和结合距离( r 0=3.27 nm)。

Results show that Calamagrostis angustfolia wetland is higher than cropland in content of total sulfur and available sulfur, which indicates cultivation depletes soil S, and soil total sulfur and available sulfur show a decreasing trend with each passing year.

结果表明，小叶章湿地土壤总硫和有效硫含量高于开垦后的农田土壤，开垦导致土壤硫含量下降，且随着耕种年限的增加，土壤总硫和有效硫含量呈逐年下降趋势。

Firstly, 3-ethylthiobutanal was prepared from crotonaldehyde reacting with ethanehiol in triethylamine with high yield. Secondly, methyl acetoacetate was converted to 6-ethylthiohept-3-en-2-one by three steps via hydrolysis, condensation with 3-ethyltio-butanal and dehydration, then 6-ethylthiohept-3-en-2-one was cycloco ndensed with dimethyl malonate by Michael addition and Claisen condensation, followed by saponification and decarboxylation to give the intermediate of 5-(2-ethylthiopropyl)-cyclohexane-1,3-dione.

首先，以巴豆醛与乙硫醇为原料，在三乙胺的催化作用下高收率制得3-乙硫基丁醛；然后从乙酰乙酸甲酯出发，通过碱水解、与3-乙硫基丁醛缩合、脱水三步反应合成6-乙硫基-3-烯-2-庚酮，接着6-乙硫基-3-烯-2-庚酮与丙二酸二甲酯通过Michael加成和Claisen缩合成环，再通过皂化和脱羧反应生成中间体5-[2-丙基]-1，3-环己二酮；再与丙酸酐反应丙酰化，最后与0-3-氯-2-丙烯基羟胺肟化，得到目标化合物烯草酮。

To research the desulfuration characteristics of calcium-based sulphur-fixing agent and decomposing-rate of desulphur object CaSO4 systemically under different conditions, and analyzed its desulfuration mechanism .

为了探求煤燃烧过程中传统钙基固硫剂固硫率低下的原因，本实验选用有代表性的含硫为2.92％的国家标准煤样，在不同条件下系统的研究了钙基固硫剂的固硫特性和固硫产物CaSO4的分解率；并分析了其固硫机理。

It depicts the species of microbesThibacillus ferrooxidans,SRB,filaceous sulfur bacteria,synthetic sulfur bacteria,colorless(sulfur bacteria and thiobacillus denitrificans,their metabolism pathway,treatment capability and key affecting factors of processes,and their disadvantages and advantages.

叙述了烟气吸收和吸收尾液的处理工艺所利用的脱硫微生物种类，并阐述了氧化亚铁硫杆菌、硫酸盐还原菌、丝状硫细菌、光合硫细菌、无色硫细菌和脱氮硫杆菌的代谢途径、作用效果和关键影响因素，并且指出其优缺点。

It depicts the species of desulfurizing microbes (Thibacillus ferrooxidans, SRB, filaceous sulfur bacteria, synthetic sulfur bacteria, colorless sulfur bacteria and thiobacillus denitrificans), their metabolism pathway, treatment capability and key affecting factors of different processes, and their disadvantages and advantages.

叙述了烟气吸收和吸收尾液的处理工艺所利用的脱硫微生物种类，并阐述了氧化亚铁硫杆菌、硫酸盐还原茵、丝状硫细菌、光合硫细菌、无色硫细菌和脱氮硫杆菌的代谢途径、作用效果和关键影响因素，并且指出其优缺点。

During temperature-programmed combustion, the evolution sequence of different sulfur forms is aliphatic sulfur, aromatic sulfur and pyritic sulfur, thiophenic sulfur and sulfatic sulfur.

2大同煤各形态硫燃烧逸出的基本顺序为：脂肪硫，芳香硫和黄铁矿硫，噻吩硫和硫酸盐硫。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。