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To determine the product distribution of the reaction mixture, an aliquot will be analyzed by thin-layer chromatography.

为了确定反应混合物中产物的分布,可以对一吸量管的产物进行薄层层析分析。

To determine the product distribution of the reaction mixture, an aliquot will be

为了确定反应混合物中产物的分布,可以对一吸量管的产物进行薄层层析分

Preparation by electronic analytical balance is more accurate and intuitionistic than transferpettor or pipet, which can be further corrected and widely used.

电子分析天平配制比用移液器或吸量管直接配制更加精确直观,并且还可以进一步校正,值得推广。

Result] It could be concluded through analyzing the model that both the mass uncertainties of quinoline phosphomolybdate precipitates and tested samples were from the resolving power and precision of balance and its maximum tolerance in assay certificate; the uncertainty brought in by volumetric flask was from the permissible error of 250 ml volumetric flask, the operation of increasing the volume to scale of volumetric flask while diluting solution and the difference between experimental temperature and the temperature at the time when the volumetric flask was calibrated; the uncertainty brought in by pipette was from the permissible error of itself, the operation of increasing the volume to intake scale while taking solution and the difference between experimental temperature and the temperature at the time when the pipette was calibrated.

结果]磷钼酸喹啉沉淀和试样质量的不确定度均来自天平的分辨力、精确度、鉴定证书上天平的最大允差,容量瓶引入的不确定度来自250 ml容量瓶本身的允许误差、稀释溶液时将体积增加到容量瓶刻度的操作和试验温度与容量瓶校准时温度的差异,吸量管引入的不确定度来自于吸量管本身的允许误差、吸取溶液时将体积增加到吸取刻度时的操作和试验温度与吸量管校准时温度的差异。

About 0.2 mL of foam was transferred with a 2 mL glass pipet into the well of a glass microscope slide (Fisher, 76 × 26 mm2, 1.4-1.6 mm thick, the well is 18 mm in diameter and 0.5 mm deep).

大约0.2mL的泡沫用一根2mL的玻璃吸量管转移进显微镜玻璃载片的阱中(Fisher, 76 × 26 mm2, 1.4-1.6 mm 厚,阱的直径 18 mm,深 0.5 mm)。

A pipette used to measure very small volumes of liquids.

这位试验者将20毫升的酸液吸入吸量管中。

In this thesis, I summarize the theoretical calculation method, applied scope and notice of siphonic drainage system, and point out the advantage of siphonic drainage system compared with gravitation drainage system. In the archetype experiment study of siphonic drainage tube, I adopt different tube diameter and different structural height to survey the drainage volume and press in different place. I observe various kinds of flow state, and get chief factors which influence hydraulic peculiarity of system as the tube diameter or structural height, and find out the relevance of factor to flux. I apply CFD Fluent software and adopt standard k-ε model and RNG k-ε model, then use finite volume method and second-order upwind scheme to discrete numerical model, while coupling numeration of velocity field and press is based on SIMPLE. In the numerical simulation of curved part of tube, siphonic drainage tube experiment system and multi-outlet siphonic drainage system, I make research on internal velocity and press of system in different project condition by changing the tube diameter of curved part, negative press value in tube export and improving the quantity of water gutter. This thesis first adopts a method of combining archetype experiment and numerical simulation to study the siphonic drainage system, test and verify the validity of experiment and numerical simulation, and makefurther study on system, it solves the problems of limited testing conditions, and has a logical results, it can provide a valid method for optimizing and designing the drainage tube-net system. The conclusion have referring value for study and design of siphonic drainage system.

本文首先对虹吸式排水系统理论计算方法、适用范围以及注意事项做出总结,并分析了虹吸式排水系统的优势;再对虹吸式排水管道进行原型试验研究,采用不同管径不同立管高度,对系统流量、管道压强进行量测,观察了各种工况下的流态,对其水力特性进行研究分析,找出影响水力特性的落差、管径主要因素以及与排水量的关系;进一步应用计算流体力学Fluent软件,采用标准κ-ε模型与RNGκ-ε模型,计算过程应用有限体积法和二阶迎风格式对数值模型进行离散,速度和压力的耦合采用SIMPLE算法,分别对系统弯管段、虹吸排水管道试验系统、多斗虹吸式排水系统进行数值模拟分析,通过改变管段弯头处半径、管段出口负压值、增加雨水斗数对不同工况下系统内部的速度和压力进行研究;本文首次采用结合原型试验与数值模拟相结合的方法,对虹吸式屋面雨水排水系统进行研究,试验与模拟相互验证,并进行拓展,很好地解决了虹吸式屋面雨水排水系统由于试验条件限制问题,结果正确合理,为排水管网系统设计和优化研究提供了有效的方法,对工程设计有较好的参考价值。

The lunate thermosiphon elevation tube was increased from 1 to 3 in order to improve the elevation of the solution.

弦月形的热虹吸提升管由原来的1根增加到3根,增大了溶液提升量,降低了热源启动温度。

Two 0.5-ml volumes of an isobutanol internal standard (10 mg/ml water; pipette 12.4 ml of isobutanol and dilute to 1 liter with water) are pipetted into two different 2-dram (7.4-ml) shell vials, one market "known."

将两份0.5毫升的异丁醇内标物(浓度为10mg/ml水,其配制法为:用吸量管吸取12.4ml 异丁醇用水稀释至1L ),用吸量管分别吸入两个不同的2-打兰(7.4毫升)的壳型小瓶中,一个标为&已知&,另一个标为未

Two 0.5-ml volumes of an isobutanol internal standard (10 mg/ml water; pipette 12.4 ml of isobutanol and dilute to 1 liter with water) are pipetted into two different 2-dram (7.4-ml) shell vials, one market "known."and the other "unknown."

将两份0.5毫升的异丁醇内标物(浓度为10mg/ml水,其配制法为:用吸量管吸取12.4ml 异丁醇用水稀释至1L ),用吸量管分别吸入两个不同的2-打兰(7.4毫升)的壳型小瓶中,一个标为&已知&,另一个标为&未知&。

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