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The Diels-Alder cycloadditions of [60] fullerene for preparation of optical limitingmaterials are discussed in chapter 3 and 6. Soluble cycloaddition derivatives of 〓aresynthesized by the reaction of 〓 with indene,1,1'-biindene andcyclopentadiene derivatives.〓Particular, the Diels-Alder cycloaddition of 〓 with1,1'-biindene under controlled conditions affords the stable monoadduct 〓〓of novel structure, which was confirmed by HPLC, FTIR, FD-MS,〓NMR,〓 NMR, HMQC and HMBC spectra, Its two bridgehead cage carbons resonate at70.91ppm, The 〓 NMR spectra showed 38 lines consistent with the 〓 symmetryassociated with [6,6] addition. The 〓 shows similar optical limitingproperties to that of 〓 in toluene for 8ns laser at wave length 532nm. Moreover, thehigh solubility of this adduct in polar solvents such as THF, acetone enables itsincorporation into sol-gel glass matrix. The thin films prepared via the sol-gel methodshow improved OL behaviour compared to those of 〓. The langmuir-Blodgett filmformation and uv-visible absorption of 〓 are also investigated. LBmonolayer of this compound is prepared on the air-water interface at 〓 mol/l. In chapter 4, three water-soluble derivatives of [60] fullerene: fullerol(1), theaddition product (2)of fullerol (1)with polyvinylpyrrolidone and fumaric acidderivative of 〓(3) are synthesized and characterized.

通过Diels-Alder环加成反应,用茚〓和1,1'-联茚〓及取代茂合成了一系列可溶性的〓环加成衍生物,发现可控制反应条件,使1,1'-联茚与〓反应,并高产率地得到具有新颖结构的单加成物,用HPLC、FTIR、FD-MS 及〓、HMQC、HMBC等多种波谱技术对其结构进行表征,测得它的两个〓杂化的桥头碳的化学位移为〓ppm,证明生成的衍生物为6∶6闭式环加成,〓NMR谱中共给出38个信号,表明〓联茚衍生物分子具有〓对称性;在波长532nm,脉冲宽度8ns的激光下,〓联茚衍生物的甲苯溶液的光限幅性能与〓的甲苯溶液相近,由于〓联茚单加成衍生物熱稳定性好,在四氢呋喃,丙酮等极性溶剂中溶解性好,能分别均匀地掺入溶胶-凝胶中,已发现它的溶胶(so1)光限幅性能优于纯〓的光限幅性能;使用Langmuir-Blodgett技术将〓联茚衍生物在空气和水的界面进行了LB单层膜和多层膜实验以及UV-Vis吸收谱研究,通过等温压缩曲线测试,证明浓度为〓〓时,〓联茚衍生物能够形成单层膜。

By synthetically analysizing the physical and chemical properties of all components and particle size, the content of F2641 in the JOB-iC is determined by gravimetric analysis after F2641 is seperated from HMX,TATB and PNP through ? alkali reflux. Determination conditions is set as follows the sample is boilingly refluxed for six hour in a constant temperature bath after adding lOOm! 8.0 ?? 0.1% NaOH. The solvent DMF saturated by TATB is used for extracting HMX,F21 and PNP from the sample and TATB is seperated by crucible filter G4. The mass precent of TATB is determined by extraction fractionation. The mass percent of PNP is measured by multiwavlength linear regression ultraviolet spectrophotometry. The testing conditions are set as follows:multiwavlength constitution: X=267nxn, 275nm, 283nm, 29mm, 299nm,the application scope of the Lambert-Beer law: the concentration of PNP is O.005?0.O25mgIml, the concentration of HMX is 0.060.3Omg/ml,absorption coefficents of PNP and HMX are solved by the slope of linear regression curve of absorbency- concentration of standard solution of PNP and HMIX for measuring wavelengthes,on the basis of the Lanibert-Beer law and absorbancy additivity principle, the slope of linear regression curve of A/E(1) and E1 of PNP and HMX solution is regarded as the concentration of PNP in the solution.

根据传爆药中各组分的物理、化学性质及主体炸药的粒度大小,进行综合分析,确定了采用碱回流重量法测定JOB-1C 中F_(2641)的含量,测定条件:加入100ml浓度为8.0±0.1%的氢氧化钠,在恒温水浴中煮沸回流6h;采用溶剂萃取法测定JOB-1C中TATB的含量,选择TATB饱和的二甲基甲酰胺为萃取溶剂,用G4坩埚式过虑器进行萃取分离;采用多波长线性回归紫外分光光度法测定JOB-1C中PNP的含量,通过实验确定了多波长组合:λ=267nm,275nm,283nm,291nm,299nm;朗波—比耳定律的适用范围为PNP浓度:0.005~0.025mg/ml,HMX浓度:0.06~0.30mg/ml;在测定波长下,对PNP、HMX标准溶液的吸光度—浓度进行线性回归,由回归曲线的斜率得出PNP、HMX的吸收系数;根据朗波—比耳定律和吸光度加和性原理,在测定波长下,对PNP、HMX 两组分混合溶液A_i/E_HMX(i与E_PNP(i/E_HMX(i进行线性回归,回归曲线的斜率即为混合溶液中PNP的浓度。

The works exhibited this time is the production under this thinking. I will not limit myself in such an abstract or traditional label. The direct or indirect calligraphy, Taiji, sculpture, poem and philosophy, aesthetic thoughts absorbed from paintings allow me to realize that the form of paintings is not just a key problem, no one shall find the freedom exit as when Duchamp's works were completely destroyed. And there is no one who is as frank and smart as Picasso to change the form game into the local snack. In some history phases, a kind of thinking ways and a kind of language styles may gain the upper hand. But comparing to stable accumulation of the history of culture and aesthetic, the pure quality of painting spirant will forever be an important premise of painting criticism.

这次展览的作品,便是这样的思考前提下的产物,我不会把自己定身在抽象或者传统这样的标签之下,我在绘画过程中所吸收的书法、太极、雕塑、诗歌和哲学、美学思想的直接和间接的营养,让我体会到,绘画作品的形式远不是一个最关键问题,没有人可以在杜桑完全彻底的破坏面前找到自由的出口,也没有人可以像毕加索那样把形式游戏变成地方小吃一般的率性和机灵,在某一个历史阶段,一种思想方式,一种语言风格或许会占上风,但相对于文化史、美学史坚实的积淀,绘画精神性的纯粹质量将永远是绘画批判的一个重要前提。

Part four, the author gives some advice of perfecting the system of Chinese Counterclaim, which is the important part in the paper .In this part, the author introduces the system of counterclaim in other countries and makes comparison with Chinese counterclaim. On the basis of comparison, the author concludes that we should absorb the advantages of the two law system and perfect Chinese counterclaim from four aspects. That is to say prefect the premise for accusation, divide the compellent counterclaim and discretionary counterclaim, the instance for counter-counterclaim, the trial of claim and counterclaim and so on.

在这一部分,在涉及到反诉的相关制度时,笔者首先对英美法系和大陆法系的有关规定做以简要介绍,然后再与我国的有关规定进行对比,从中寻找可以为我国可以借鉴、吸收的相关理论和制度,并进而提出对我国反诉制度进行完善的具体构想,笔者主张从完善反诉提起的条件,对反诉的种类进行强制性反诉和任意性反诉的区分、界定提起再反诉的具体情况、反诉的审理四个大的方面来进行重构,而对于反诉提起的条件又从实质条件、程序条件和法定条件三个方面进行了详细的论述。

With the analysis and discussion of their photoini- liability, it was indicated that their max are all around 330 nm, and all of them have excellent solubility in water and good photoinitiability. Furthermore, the three Photoinitiators with α-tert-amine are obviously superior to the one with just α-sec-amine. Among the four photoinitiators l-(4-aminophenyl)-2-diethylamino-l- propanone dihydrochloride is the best and it has excellent use value.

通过对它们的光引发性能测试和构效关系的分析探讨,表明四种光引发剂的最大吸收波长λ_(max均在330nm左右,具有优异的水溶性和良好的光引发性能,其中具有α-叔胺基团的三种光引发剂明显优于具有α-仲胺基团的光引发剂,尤其以1-(4-氨基苯基)-2-二乙胺基-1-丙酮盐酸盐的光引发性能最好,具有推广应用前景。

Schwing poppet valve hydraulic piston pump be used in many municipal and industrial projects world wide.Today,Schwing was recognized as technology leader of"Dewatered sludge Pumping System".Schwing pump can pumping the sludge even with 56%solid content,for other inorganic material even with 80%solid content.Schwing units have operated continuously for years with 99%availablity.For sludge storage,Available in circular or rectangular design,the sliding frame/push floor technologies provide low cost methods to store large volumes of material w你好le awaiting final disposal.Schwing sliding frame system in the bottom of the silo,disc harge the sludge with the screw into sludge truck or Schwing pump.The typical installation is silo with pump installed beside the dewatering mac你好ne.A Schwing silo can be integrated into the process stream to equalize surges in solids production and subsequently meter cake to final disposal.Large diameter storage silos are useful for truck loading,and finally,both sliding frame and push floor designs are effective as receiving stations used to accept sludge hauled in from other facilities.Ultimately,the storage volume of the silos and bunkers dictate the plant''s flexibility in disposing of the solids.

施维英的晋升阀液压柱塞泵广泛应用活着界规模内的城市管理工作以及工业污泥输送项目今日,施维英被公以为是世界规模内&脱水污泥泵送体系&的科学技术带领者施维英泵可以泵送固体含量达56%的活性有生命的物质脱水污泥,甚或者固体含量达80%的非有生命的物质其它稀浆与污泥施维英泵颠末多年不中断地事情,靠患上住性仍维持在99%施维英滑架体系位于料仓的底部,可以将污泥排入卡车或者施维英泵中用来暂存污泥以及装车的料仓较典型的应用是以及施维英污泥泵一路被安装在污泥脱水举措措施相近施维英料仓在污水措置惩罚厂的预设中首要负担3种脚色,料仓被集成处措置惩罚流程之中,均衡物料出进,并对终极排出的污泥计量料仓用于装车料仓的储存体积说了然污水措置惩罚厂措置惩罚污泥的规模料仓可以用来吸收暂存从其它污水厂送来的污泥,尔后送到后续污泥措置惩罚装备中滑架技能已在被证实是最具国际性最有用率的技能

For frequency information fluid identification technology:the basic theory of fluid identification based on frequency information has been introduced,for inner and external factor affecting frequency,some steps have been proposed to attain reserved amplitude and frequency analysis data with high resolution,high S/N ratio;through the comparison of time-frequency analysis method, the high accuracy time-frequency analysis method has been selected to extract time-frequency attributes;the analysis method flow of common single frequency fluid identification has been proposed,according to the data of full frequency band,several anomaly zone modes of common single frequency attribute have segregated; incorporating converted wave and compression wave,fluid identification method based on PS wave combined time-frequency analysis has been proposed;the AVO property of various fluid type in frequency domain has been studied;the generalized fourier analysis method,Proni absorption filter has been introduced,and researched for anti-noise and for the seismic processing interpretation flow.The above technology have been applied to fluid identification of organic reef in WBT area in the east of Sichuan and fluid identification of clastic rock in GUANGAN area in the middle of Sichuan,the results show that the above methods are effective.

基于频率信息的流体识别技术方面:介绍了利用频率信息流体识别的基本理论,针对影响频率的内、外在因素,提出一些针对措施,以获得高分辨率、高信噪比的保幅、保频分析数据;通过时频分析方法的比较,选取高精度的时频分析方法提取时频属性;提出共单频属性进行流体识别的分析方法流程,结合全频带数据,分出几种共单频属性异常带模式;联合转换波资料和纵波资料,提出基于纵横波联合时频分析进行流体识别方法;研究了频率域内不同流体类型AVO现象;引进一种广义傅立叶分析方法:Proni吸收滤波,研究其抗噪性以及进行地震处理解释的流程;将这些技术应用川东北五百梯区块进行生物礁储层流体的识别和川中广安陆相碎屑岩的流体识别,取得较好的效果。

Winter,because of cold and food resource was shortage,animal to get more nutrition material andenergy,to adopt the changes of environment condition,to prolong alimentary canal andincrease food in alimentary canal detention time,to be able to absorb the nutrition materialdigestion countermeasure in food fully.As availability and nutrition were rich such as insummer and fall,however,shortening the length of alimentary canal,make food inalimentary canal current velocity accelerate,since make animal absorb in the season withabundant food the more nutrition material energy that is plenty of with accumulation.9adopt relative fatness,body chemical composition,kidney fatty index and marrow fattyindex 4 kinds of population nutrition condition assessment technique appraise as squirrelnutrition condition of population.

冬季,由于寒冷和食物资源匮缺,动物为了获取更多的营养物质和能量,采用延长消化道、增加食物在消化道内滞留时间,从而能充分吸收食物中的营养物质的消化对策,来适应外境环境条件的变化;在食物可利用性大、食物中营养物质较丰富的季节,则缩短消化道长度,使食物在消化道内的流速加快,从使动物在食物充裕的季节能摄取更多的营养物质和积累大量的能量。9采用肥满度、身体组成成分分析、肾脂肪指数和骨髓脂肪指数四种种群营养状况评价方法对松鼠种群的营养状况进行了评价。

Ma Yuan admires the great artists of the pre-Renaissance very ,mucn,sucn as ,poteqilli,Angelica,and Masaqeu,etc,The art of these artists lied in the period between theMiddla Ages and the Renaissance,during which the divine spirit of the Middle Ages was finely inherited,and the spitrit and breath ofa neew age was gradually standing out.

在马元的《红衣系列》中,画家内在性在吸收了欧洲文艺复兴前期大师形式语言资源,同时也找到了它和自己的表达主题的整合方式,这主要体现于马元的造型语言要素中,有两种因素是需要特别指出的,这就是垂直线造型的强调运用和红色的强调运用。

The results show that the as-synthesized chalcone-containing copolymers are a kind of thermosensitive polymer with a lower critic solution temperature and the LCST of the copolymer decreases with the increase of the chalcone content in the copolymer. With the increase of the solvent polarity, both the maximum absorption wavelength and the fluorescence emitting wavelength of the chalcone-containing copolymers redshifts, and the intensity of fluorescence first increases, then decreases, which exhibits solvent polarity sensitive fluorescence properties.

结果表明,侧链查尔酮共聚物是一类具有低临界溶解温度的温敏性聚合物,其LCST温度随着共聚物中查尔酮含量的增加而降低;随着溶剂极性的增加,侧链查尔酮共聚物的紫外-可见最大吸收波长红移,其荧光发光波长红移并且发光强度先增强后降低,具有溶剂极性敏感的荧光特性;同时对比侧链查尔酮共聚物水溶液低温和高温下的荧光,发现低温下几乎无荧光,高温下其荧光得到明显增强,其荧光具有可逆的温度&开/关&特性。

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The basic concept of FOP can be summarized as to further optimize effective prescription according to the standard of curative effects and with the aid of modern science and technology and theories of traditional Chinese medicine.

其基本内涵可概括为:以确有疗效的中药复方为研究对象,以现代科学技术和传统中医药理论为技术支持,以该复方所治病证的药效响应为评价标准,以优化重组疗效更优的新复方为研究目的。

Ever since our world has been a world, native forests have been indiscriminately exploited by man.

自从我们的世界一直是世界原生森林被任意剥削人。

I don't… don't know. He's unconscious.

我不……我不知道他休克了。