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The aliquot was determined and confirmed by gas chromatography-negative chemical ionization mass spectrometry using external standard method.

样品中三唑醇残留物由正己烷饱和的乙腈(含1%冰醋酸)提取,加入无水硫酸镁与无水醋酸钠振荡促使提取液分层后进行固相分散萃取净化,用气相色谱-负化学离子源质谱法进行测定与确证,外标法定量。

Results INS SOL (5 U·kg -1 ) containing eucalyptol, sodium caprate, sodium deoxycholate and menthol significantly decreased the blood glucose level ( P 05), and eucalyptol appeared to be more effective 38 8%,...

结果 含桉油醇、癸酸钠、脱氧胆酸钠和薄荷醇的INS SOL(5U·kg-1)均可降低血糖(P 0 5 ),而桉油醇的作用最明显,最大降糖百分数为 38 8%(P 0 1)。

A total of one hundred fifty three healthy male and female adults were entered into a six month,doubleblind clinical study designed to evaluate the effect of a dentifrice containing 0.3% triclosan and 2.0% PVM/MA copolymer in a 0.243% sodium fluoride/silica base, relative to a 0.243% sodium fluoride silica base control dentifrice on supragingival plaque accumulation and gingivitis.

本研究的目的是证实含0.3%三氯羟苯醚,2.0%PVM/MA及0.243%氟化钠以二氧化硅磨料牙膏在减少菌斑积聚和牙龈炎形成方面对中国成年人群的效果。153名健康男女分为实验组及对照组,用双盲法评价6月后临床效果。采用纳入和排除的评价标准后进行了基线检查,实验对象每日使用分配的牙膏和软毛牙刷早晚刷牙一次,3个月和6个月再次检查。检查结果表明,使用含有三氯羟苯醚-共聚体牙膏组与使用不含该成分的对照组相比,实验对象的牙菌斑、牙龈炎指数分别减少16.1%及24.3%,均有统计学显著性意义(P<0.001)。

The optimum process conditions of treating chromium-contained wastewater with low concentration and the optimum reflux rate of settled bottom stream of flocculate are obtained.

以长沙铬盐厂的含铬废水为试验水样,研究了用七水硫酸铁、亚硫酸氢钠、铁屑 3种还原剂达标处理较低浓度含铬废水的适宜工艺条件和悬浮液絮凝体沉降底流的最佳回流率。

METHODS: Heparin with an aldehyde group as reducing end was prepared by nitrous acid degradation method.

将肝素钠用亚硝酸降解法降解,得到还原末端为醛基的肝素,分别溶解于二甲亚砜、含0.05 mL,0.5 mL冰醋酸的二甲亚砜溶液,再与对巯基苯胺发生还原胺化反应,用氰基硼氢化钠作还原剂,得到带巯基的肝素衍生物。

The influenced of sodium hexame taphospha on the dispersion of nano-ZnO in glaze,and its effects on chinaware products were investigated,in which sedimentation test,granularity analysis,rheology of glaze,reflet of chinaware and sintering temperature were used to characterize the aqueous and glaze systems with nano-ZnO and chinaware products.

研究了六偏磷酸钠对纳米ZnO在水中和陶瓷釉料中的分散性以及纳米ZnO对陶瓷成品性能的影响。采用沉降实验、粒度分析、釉料流变性、陶瓷成品光泽度、烧成温度测试手段,对含纳米ZnO的水溶液、釉料和陶瓷成品进行表征。结果表明,在实验条件下,纳米ZnO在水中最佳分散条件为:0.5%六偏磷酸钠,3.0%纳米ZnO,pH为9。

Results The reaction was not turbidness which was between modified reagent containing potassium hydroxide 143 mmol/L, tartrate kaliumna natrium 56.7 mmol/L and blood serum containing triglyceride 5.6 mmol/L,glucose polymer 60 g/L and need not sample blank.

结果含氢氧化钾 143mmol/L、酒石酸钾钠 56.7mmol/L的改良试剂与含 TG 5.6mmol/L、葡聚糖60g/L的血清反应均不显混浊,可不设标本空白。

To the collophanite of certain region, Liaoning Province, the content of P_2O_5 was 19.50% and MgO was 6.87%. Using MG as collector to reversely float dolomite, its concentrate can be upgraded to 24.68%(P_2O_5), and the P_2O_5 grade of concentrate of sodium oleate as collector was only 21%. Simultaneity, the recovery of P_2O_5 of concentrate was 83.20%; the tailing contained P_2O_5 only 10%, it obviously declined compareing with sodium oleate.

对于辽宁某地胶磷矿(原矿含P_2O_5 19.50%,MgO 6.87%),使用MG药剂及单一反浮选工艺,可获得P_2O_5品位24.68%的精矿,较传统的油酸钠提高约3个品位,磷回收率83.20%,而尾矿P_2O_5品位仅为10%左右,比油酸钠等的尾矿P_2O_5有明显下降。

First take the administration team group first forIM model making by given ranitidine 0.06g and the 5%hyperhaline typical finemixtured powder with the 50ug/ml MNNG, 0.1%ammonia water,2g sodiumsalicylate added into 100ml 30%alcoholic solution for intragastric administration 6weeks and the nomal control group by given the ordinary feeds and commonwater;After 9 weeks administration,the model groups rats was put to death for modelmaking detection.

从实验第一天起正常对照组给予普通饲料和正常饮水;模型组大鼠则食用含0.06雷尼替丁和5%的高盐的标准粉末状混合饲料,给予含有浓度为50μg/ml的甲基硝基亚硝基胍溶液每日自由饮用,MNNG溶液装入涂有黑漆的避光饮水瓶内,每24 h更换1次药液,每周饮5天,周2和周5则给予浓度0.1%的氨水饮用;同时将2g水杨酸钠放入100ml 30%的酒精溶液中,配置成2%的水杨酸钠和30%的酒精的混合溶液,从第4周起每天早上9点灌胃。

The weight loss rate in 600 ℃ sodium containing 30 μg/g oxygen is about 1×10~(-4) mm·a~(-1) and 2×10~(-4 mm·a~(-1), respectively for the rotary swaging tungsten and polishing tungsten.

在600℃、含30μg/g氧的金属钠中,旋锻钨和抛光钨的失重速率分别为1×10-4mm·a-1和2×10-4mm·a-1,两种钨与钠均有良好的相容性。

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