含钛的

When the molar fraction of SnO2 is 83%, the main component of the coating isO2 solid solution with rutile structure. When the molar fraction of SnO2 is 44%, the main components of coating are theO2 solid solution with rutile structure andO2 solid solution with fluorite structure. When the molar fraction of SnO2 is 17%, the main component of the coating isO2 solid solution with fluorite structure. Annealed at higher temperature than 450 ℃, CeO2 is found in the coating containing 83%Sn, and there is not SnO2 in the coating containing 83%Ce, which suggests that fluoriteO2 has higher thermal stability than rutileO2. When the molar fraction of SnO2 increases, the dispensability of the coatings is improved greatly.

结果表明：通过控制制备条件可获得具有纳米结构的钛阳极涂层；当Sn的摩尔分数为83%时，涂层主要为金红石相的O2固溶体；当Sn的摩尔分数为44%时，涂层中金红石相O2固溶体和萤石结构的O2固溶体共存；当Sn的摩尔分数为17%时，涂层由萤石结构的O2固溶体组成；高于450 ℃退火时，含83%Sn的涂层中出现CeO2相，而在含83%Ce的涂层中没有出现SnO2相，表明在相同的溶质浓度下，萤石结构的O2固溶体比锡基金红石相O2固溶体具有更好的热稳定性；而涂层中的SnO2具有明显改善涂层分散性的作用。

Produce the BF gas mud 100, OOOt every year. The raw mineral of puddling is the magnetite containing vanadium and titanium. The grade of iron is only 53%. The grade of sinter mineral is only 47-48%. So the percentage composition of iron is relatively low, only 29.70%. The grade of zinc is relatively high, reach 9.92%. And the percentage composition of carbon is relatively high, reach 16. 80%. In the next place, the BF gas mud is the production through sinter in high temperature.

攀钢炼铁的原矿物为钒钛磁铁矿，铁品位仅为53％，烧结矿品位为47％～48％，所以攀钢高炉瓦斯泥的铁品位也相对较低，仅为29.70％，并且含锌量高，达到了9.92％，含碳则高达16.80％；其次高炉瓦斯泥是高炉冶炼过程中的产物，SiO_2、Al_2O_3和铁部分熔融在一起，选矿难度增加。

Three kinds of CpTiCl had been synthesized when was catechol , 2, 2′-biphenol , or 2, 2′-binaphthol , respectively. In the case of CpTiCl〓, was 8-hydroxylquinoline , 2-methyl-8-hydroxyl-quinoline , and 8hydroxyl-5-nitro-quinoline , respectively.

研究表明，这三类半茂钛配合物在助催化剂MAO作用下，于30℃、0.1MPa乙烯压力下均可催化乙烯聚合，并显示较高的活性，远高于未引入非茂配体的CpTiCl〓及不含茂环的相应非茂配合物的活性，这说明同时含一个茂配体和一个非茂配体的半茂配合物是烯烃聚合的优良催化剂。

Four half-sandwich complexes (01-04) with pendant furyl group were successfully synthesized.

合成了四个侧链含呋喃基的半夹心茂钛络合物。

The influence of Zr/Ti on the mechanical and electrical properties ,phase composition,lattice constant of lead niobium stibium zirconate titanatePb(Nb1/2Sb1/2TiO3-PbTiO3-PbZrO3 (Nb1/2Sb1/2=0.02mol piezoelectric ceramics ,in which there are tetragonal and rhombohedral phases coexistent (morphotropic phase boundary,MPB),was studied by conventional containing lead piezoelectric ceramic processing and X-ray diffraction.

借助X-射线衍射仪，采用传统含铅压电陶瓷制备工艺研究了Zr/Ti对准同型相界附近铌锑锆钛酸铅（Pb(Nb1/2Sb1/2)TiO3-PbTiO3-PbZrO3）(Nb1/2Sb1/2=0.02mol压电陶瓷机电性能、相组成和晶格常数的影响。

I. oxid granite tile , include magnetic iron ore, red iron ore, brown iron ore, etc.

一、氧化铁：含铁氧化物的矿物有磁铁矿、赤铁矿、褐铁矿、钛铁矿等。

Two series of polyurethane acrylate grafted acrylic resins (Acr-g-TPU-PETA and Acr-gPPU-PETA) self-emulsifying systems are obtained by grafting -NCO group modified polyurethane acrylates with acrylic copolymer prepared from n-butyl acrylate, styrene,βhydroxyethyl methacrylate and acrylic acid The self-emulsifying systems showed Newtonian fluidity with viscosity closed to that of water, the solid contents were around 30% The T〓 of 15～4℃ for dried film before photocuring favored film formation at room temperature DSC and DMA results showed that PU-PETA is compatible with acrylic resin in the grafted resin The TG and dTG curves for Acr-g-PU-PETA samples were substantially different from the corresponding blends, and the brodened dTG peaks for photocured grafted resin suggest that there might be multiple interactions among chain segments The photocued film of the grafted resins self-emulsifying system exhibited good overall properties with polyurethane acrylate grafts ranging from 30% to 50%, and Acr-g-TPU-PETA series showed better properties than Acr-gPPU-PETA series The adhesion of the photocured film was 1～2 grade, impact strength was 50kg-cm and flexibility was 1mm The Shore hardness and the adhesion of the film decreased markedly if PETA was replaced by HEMA as photoactive group due to the lower C=C double bond content in the grafted resin The polyhydroxy amine-linked thioxanthones photoinitiators can be evenly dispersed in self-emulsifying system without color spot appearing in the dried film The films photocured with IV〓～IV〓 generally exhibited higher Shore hardness, gloss and solventresistance than that cured with Irgacure 2959 and did not induce the rusting of the iron substrate Pigmenting with titanium oxide had no effect on the photocuring The polyhydroxy amine-linked thioxanthone IV〓 and IV〓 can be new candidates for the formulation of titanium oxide pigmented photocurable water-borne coatings for their pale-yellow appearance and slight interference with the color of the coatings WB 4759 with high water-solubility coalesced and separated from the dried resin film, and even induced the rusting of iron substrate.

以丙烯酸丁酯，甲基丙烯酸-β-羟乙酯，丙烯酸及苯乙烯合成厂丙烯酸共聚树脂，并与含-NCO端基的聚氨酯丙烯酸酯接枝反应，经水性化后，得到两个系列（Acr-g-TPU-PETA和Acr-g-PPU-PETA）各5个不同配比的丙烯酸树脂接枝聚氨酯丙烯酸酯自乳化体系，粘度与水相近，为牛顿流体，固含量30％左右。光固化前干燥涂膜的玻璃化转变温度在-15℃～4℃之间，有利于室温下成膜。DSC及DMA谱表明两种树脂基本相容。Acr-g-PU-PETA的热失重行为明显不同于共混材料，接枝样dTG峰明显宽化，表明接枝样中链段之间的相互作刚有多重性，丙烯酸树脂与聚氨酯之间有一定的相容性。接枝树脂自乳化体系光固化涂层的综合性能以聚氨酯丙烯酸酯成分为50％～30％者相对较好，且以Acr-g-TPU-PETA系列更理想。光固化膜的附着力为1～2级，冲击强度为50kg·cm，柔软性多为1mm。以HEMA代替PETA作为接枝树脂的活性基团，碳—碳双键密度太低，光固化膜交联点太少，硬度和附着力均较差。多羟基胺连硫杂蒽酮光引发剂能均匀分散于树脂自乳化体系和接枝树脂干膜中，不出现色斑，光固化膜肖氏硬度一般高于以Irgacure 2959为光引发剂的光固化膜，光泽度及耐丁酮溶剂性能均有所提高，不会诱导铁基生锈，钛白着色对光固化结果几乎没有影响。本论文所合成的多羟基胺连硫杂蒽酮光引发剂IV〓与IV〓为浅黄色，对光固化涂层的颜色干扰较小，为配制钛白着色光固化水性涂料提供了新的光引发剂。水溶性太强的WB 4759在干膜中易聚结析出，且对所附着的铁基有诱导锈蚀作用。

The development of spiral alga beer, compounding SOD beer and Birch Liquid beer could not only make full use of biological resources and modern beer brewing techniques but also enrich beer variety.

螺旋藻所含的维生素及矿物质微量元素不仅种类齐全，而且含量较高；复方SOD除含有SOD外，还含有猴菇多糖，多种必需氨基酸，维生素，及锌、硒、铁、钙等10多种微量元素；桦树液中富含生物活性物质，含有多种碳水化合物、20多种氨基酸和微量元素硅、铁、锶、钛、钡、铜等。

Transition metal borides and inorganic boron-containing compounds, such as TiB〓, BN, B〓C and BP, are one of the most important groups for application in high-temperature performance, electronics and catalysts. Traditionally, they were prepared by high-temperature reactions; however, the products were beyond nanometer scale.

中文题名溶剂热合成硼化物及非金属含硼化合物纳米材料副题名外文题名论文作者谷云乐导师钱逸泰学科专业无机化学研究领域\研究方向学位级别博士学位授予单位中国科学技术大学学位授予日期2003 论文页码总数70页关键词纳米材料硼化物溶剂热合成馆藏号BSLW /2003 /O613 /6 硼化物、非金属含硼化合物功能材料（如硼化钛、氮化硼、碳化硼和磷化硼等）通常具有高硬度、高熔点、机械强度大、高温化学稳定性好等一系列优良性能，有些还具有奇异的光、电、磁、热学性能和催化活性，是一类最富潜力的非氧化物高温结构材料、电子材料和催化材料。

Aiming at solving the problem in the electrochemical oxidation of ammonia wastewater,the tin and antimony electrodes based on titanium were manufactured,the effect of different manufacturing condition to the impact of electrochemical oxidating ammonia wastewater was researched. After researching the influential factor and optimizing the manufacturing condition,the appearance analysis and the electrochemical analysis was hold on, the electroactivated character of the electrodes was studied to provide warrant to its application in the ammonia wastewater.

本论文从电化学氧化法处理含氨氮废水的问题出发，对钛基锡锑电极材料进行研制，考察了不同的制备条件对含氨氮废水的电化学氧化去除的影响，研究了各影响因素并优化了制备条件，并对其进行了表面形貌分析、电化学分析的研究，微观地研究了电极的电催化性能，为其应用于实际氨氮废水处理中提供了依据。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。