含酸的

Copper arsenite prepared from waste acid containing arsenic was applied in copper electrolyte purification.

利用含砷废酸制备亚砷酸铜，并将所得亚砷酸铜应用到铜电解液的净化。

To improve the cyano reactivity, cyano-terminated PPENs were prepared by the end-capping reaction of PPEN-OL with CBN; benzonitrile terminated polys were also prepared by the polycondensation of excess 4,4'-oxydianiline with 1,2-dihydro-2-(4-carboxyphenyl)-4-[4-(4-carboxyphenoxyl)phenyl]-phthalazinone, followed by end-capping with CBA. The polymers synthesized exhibited good solubility in NMP, DMAc and DMF, and were crosslinked to afford phenyl-s-triazine-containing polymers under the similar conditions.

为提高氰基活性，以对氯苯腈为原料，对PPEN-OL进行封端，设计合成了含氰端基的聚芳醚腈；以含二氮杂萘酮联苯结构二酸单体与4，4'-二氨基二苯醚为原料，经Yamazaki膦酰化缩聚，并用对氰基苯甲酸进行封端，合成了含氰端基的聚芳醚酰胺。

These humic small molecules are probably the humified products of various compounds in different humification procession. Their composition and amount will be different in different environment. This indicated the complex composition of the humic acid-like geomacromolecules and the various effect in the environment.

这些具有不同性质的腐殖酸小分子可能与腐殖酸形成过程中不同母质来源物质在不同阶段的腐殖化产物有关，并且不同环境中的腐殖酸分子由于其地质条件的差异，所含腐殖酸小分子的组成和数量都不会完全相同，表明腐殖酸类地质大分子物质结构组成的复杂性和在环境中影响的多样性。

On the other hand, 3(2)-fluoro-4-methoxyl methyl benzyl alcohol and 3(2)-fluoro-4-methyl benzyl alcohol are mixture and components of pyrethrum esters. Both of them have "mixture fluorine effect " and higher activity, lower drug resistance. As we know, the mixture benzyl alcohol containing fluorine is more easy to be synthesized than the single, so the cost of preparation is lower. We hope to apply it to molecule design of the new agriculture chemical. On the base of molecule design and structure-activity relationship research of pyrethric acid II and mixture of alcohol containing fluorine, we intend to get new pyrethrum ester that have higher activity and lower resistance.

另一方面，混合含氟对甲氧甲基苄醇和混合含氟对甲苄醇都是具有"混合氟效应"的高活性、低抗性的拟除虫菊酯醇组分，由于混合含氟醇的合成要比单一异构体的合成容易，成本较低，本文希望将其应用到新农药的分子设计中，用第二菊酸和一些含氟醇进行分子设计及进一步的构效关系的研究，筛选出一些高活性低抗性的拟除虫菊酯换代新品种。

Serum samples should be collected instead of plasma samples from anticoagulants heparin and trisodium citrate when copies of HBV DNA were detected. Plasma samples from anticoagulant dipotassium EDTA is also used with quantitative assays for HBV DNA.

实时荧光定量PCR技术检测乙型肝炎病毒DNA拷贝数，应避免使用含肝素钠和枸缘酸钠的血浆标本，使用不含抗凝剂或含EDTA-K2抗凝剂的无菌试管收集标本。

A novel drum organooxotin cluster hexameric phenyloxotin 3 indolpropylcarboxylate was synthesized by the reaction of Ph 3SnOH with 3 indolpropylcarboxylic acid in 1∶1 molar ratio.

利用Ph3SnOH和 3 吲哚丁酸以 1∶1摩尔比反应，合成了新型含羧酸配体的鼓形有机锡氧簇合物：六聚苯基锡氧 3 吲哚丁酸酯。

Amino-6-nitrobenzodifuroxan was prepared through a three-step reaction from starting material 3, 5-dinitrobenzoic acid:(1)3, 5-dinitroaniline (1) was synthesized from the reaction of DNBA and hydrazoic acid in inert solvent 1, 2-dichioroethane through Schmidt rearrangement with yield of 89.6%;(2) 1 was subjected to nitration to prepare pentanitroaniline (2) with yield of 51.1%;(3) The title compound was prepared from 2 and sodium azide in acetic acid through denitrogenation and then Schmidt rearrangement with yield of 86.8%, m.p.204℃～206℃.

以3，5-二硝基苯甲酸为原料经过3步反应合成了7-氨基6-硝基苯并二氧化吠咱：第1步反应，在二氯乙烷惰性溶剂中，DNBA与叠氮酸反应并发生Schmidt重排反应生成3，5-二硝基苯胺(1)，产率89.6%；第2步反应，1在含100%硫酸的硝硫混酸中硝化生成五硝基苯胺(2)，产率51.1%；第3步反应，2与叠氮酸反应，不经分离直接进行热解脱氮、Schmidt重排反应，得到目标化合物， m.p.204℃~ 206℃，产率86.8%。

The molecular designs and synthesis of triarylamine-based picolinic acid derivatives used as ancillary ligands, and their cyclometalated iridium complexes used as red-and green-emitters, as well as optoelectronics properites of these compounds were investigated in order to solve current problems of organic/polymeric electroluminescent materials and devices.

本论文针对目前有机/聚合物电致磷光材料和器件存在的问题，开展了新型三芳胺吡啶羧酸类辅助配体及其红光和绿光环金属铱配合物电致磷光材料的分子设计、合成和光电性能研究，主要包括：(1)设计、合成了三种新型的三芳胺吡啶羧酸类双齿阴离子型辅助配体；(2)以三芳胺吡啶羧酸衍生物作为双齿阴离子型辅助配体，合成得到了两个系列的红光和绿光环金属铱配合物；(3)研究了三芳胺吡啶羧酸类辅助配体分子结构对环金属配合物的紫外吸收和光致发光性能的影响；(4)以环金属配合物为客体，聚芴和恶二唑衍生物为主体，制作了聚合物电磷光器件，研究了含三芳胺吡啶羧酸类辅助配体、环金属配合物客体材料和聚合物主体材料等分子结构对电致发光性能的影响。

Groups were feeded with routine dietary(Zn37.15mg/kgDM),among which,group A was used to as the control group andB,C,D groups were added 120mg/kg,240mg/kg,360mg/kg Zn-Met in routine dietary. Pretesting date was 10 days.

各组奶牛均饲喂含锌量37.15mg／kg的基础日粮，其中，A组=基础日粮；B组=基础日粮+120mg／kg蛋氨酸锌；C组=基础日粮+240mg／kg蛋氨酸锌；D组=基础日粮+360mg／kg蛋氨酸锌，预试期为10天。

Treatments contained skim milk and 50 g fat from high–oleic acid safflower and canola oils (monounsaturated fatty acid; MUFA), MUFA + 3.5 g α-linolenic acid (ALA; MUFA + ALA) from high-ALA canola oil, or MUFA + 4.0 g both eicosapentaenoic acid and docosahexaenoic acid (DHA; MUFA + EPA/DHA) from sardine oil.

处理因素为：脱脂奶及50g脂肪（来源于含高油酸的草红花和芸苔油）（单不饱和脂肪酸，MUFA组）， MUFA＋3.5g γ－亚麻酸（来源于高γ－亚麻酸含量的芸苔油），MUFA＋4.0g二十碳五烯酸和二十二碳六烯酸（MUFA+EPA/DHA组）。

For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降，而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

弗四23 而在你们心思的灵里得以更新