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The reaction of polyfluoroalkyl iodides with 4-pentenoic acids initiated by sodium dithionite was realized to give polyfluoroalkyl substituted lactones.

我们研究了多氟烷基碘代烷与4-戊烯酸类化合物等在连二亚硫酸钠引发下的反应,得到了氟烷基取代的内酯化合物,我们将该反应称为氟烷基化内酯化反应;并建立了一个利用该反应合成含氟内酯的新方法,首次利用氟烷基化内酯化反应进行高立体选择性双环含氟内酯及手性含氟内酯等的合成,已合成含氟内酯新化合物50余种。

Results:Normal rats as the donator of serum, using methanolic extract of CWC, 10 times equivalent dose for adults every day, intragastric administration twice a day of 8-hour interval, keeping on 3 days, hemospasia after 2 hours of the last administration was the better preparative method of the serum containing drug.

建立CCl4诱导的原代培养大鼠肝细胞损伤模型,大鼠为含药血清供体,以含药血清对损伤肝细胞增殖及丙氨酸氨基转移酶泄漏的影响两个指标,结合含药血清中五味子乙素的含量测定,分别采用单因素考察、多因素的正交试验,优选含药血清的制备方法,并确定体系中血清添加量。

B ides the tellurides mentioned above that are common in gold deposits, Te isalso seen in such rare minerals as hessite, Au2Te and, a variety of unnamed telluritesand tellurates that may be subdivided into Au-bearing and Au free minerals.

除上述碲化物外,碲在本矿床形成罕见的碲银矿、Au2Te和种类繁多的未名碲化物、碲酸盐等含氧盐,含氧盐进一步可分为含 Au、不含Au,包括 AuT。。。

B ides the tellurides mentioned above that are common in gold deposits, Te isalso seen in such rare minerals as hessite, Au2Te and, a variety of unnamed telluritesand tellurates that may be subdivided into Au-bearing and Au free minerals. Theformer includes AtteO3, Au2TeO4, AuTeO4; and the latter schieffinilite, Zn2Te3O8,H2Pb2Fe4[TeO4]9.7-12H2O that were found by the author and are yet to be furtherstudied for acceptance by IMA-CNMMN as potential new minerals.

除上述碲化物外,碲在本矿床形成罕见的碲银矿、Au2Te和种类繁多的未名碲化物、碲酸盐等含氧盐,含氧盐进一步可分为含 Au、不含Au,包括 AuTeO3、Au2TeO4、AuTeO4 等以及水硫碲铅石、Zn2Te3O8、H2Pb2Fe4[TeO4]9.7-12H2O等,后二种为待申报的新矿物。

Analysis of the material change, garlic cells bioactive aliphatic thio cysteine sulfoxide and thiosulfate propenyl cysteine sulfoxide sulfur compounds in garlic, such as the role of enzymes, the generation of thiobarbituric acid sub - ester, propylene-based thiosulfinates, allyl thiosulfinates as garlic pigment precursor substances, and further changes occurred in the green garlic.

从物质变化分析,大蒜细胞中的生物活性物质硫代脂肪族半胱氨酸亚砜和硫代丙烯基半胱氨酸亚砜等含硫化合物在蒜酶的作用下,生成硫代亚磺酸酯、丙烯基硫代亚磺酸酯、烯丙基硫代亚磺酸酯,作为大蒜色素物质的前体,进一步发生大蒜绿变。

The invention discloses a synthetic using method of smelting high-furnace dust, which comprises the following steps: grinding the high-furnace dust with 1.5-15% zinc; proceeding magnetic cobbing; reclassifying to obtain the refined ferric ore; disposing ore tail through waste acid of titanium dioxide with 15-30% sulphuric acid; transmitting the zinc oxide in the solution at zinc sulfate pattern; separating solid and liquid solution through lime; obtaining refined zinc ore through S2-, CO32-, HCO3- ion; floating the immersed slag through neutral oil.

一种炼铁高炉炉尘资源综合利用的方法,含锌1.5%~15%的高炉炉尘经磨矿、磁选、重选回收铁矿物获得铁精矿,选矿尾矿用含硫酸15%~30%的钛白废酸处理,使其中的氧化锌以硫酸锌的形式转入溶液中,固液分离得出的溶液用石灰中和除铁后,再用S2-、CO32-、HCO3-离子沉锌获得锌精矿,浸出渣用中性油浮选获得炭精矿。该方法将钛白废酸和高炉炉尘结合在一起,使之成为互为所需的原料和试剂,有效地将两种废弃物变成了有价资源,较好解决了环境污染问题,同时又能产生好的经济效益。

This article approaches the treatment of Cd-contained acid waste liquid from a precious metal plant of certain smelter and points out that distillation and electrolyze processes can be used in the recovery of Cdcontained acid waste liquid.

通过对某厂贵金属车间在生产过程中产生的含镉酸洗废液,进行治理试验研究,得出了通过蒸馏、电解的方法,可以实现含镉酸洗废液的回收利用,达到了闭路循环的目的。

The anodic behavior of electrolytic nickel anode in nickel sulfamate plating Solution was investigated,using anodic polarization curves,metallographic observation of cross-sections of nickel deposits,Hull Cell tests with solutions with and without Cl-,F-,bending tests with five solutions of different compositions,and sulfur content analysis in nickel deposit with mass spectrometry.

采用极化曲线、金相观察、赫尔槽电镀试验、弯曲试验和质谱分析方法,研究了氨基磺酸盐镀镍的阳极行为,证明了当在氨基磺酸盐镀液中使用电解镍阳极时,其活化峰值电流和镀液组成有很大的相关性,当镀液中不含F-和Cl-时其阳极活化峰值电流小,阳极处于极化状态,或相当大面积处于极化状态,使氨基磺酸根在极化的阳极表面氧化,从而使含硫化合物夹附于镀镍层,形成镀层内应力,并使镀层成为层状结构,并出现半光亮的外观。

Its structure was determined by a combination of MALDI-TOF MS ana lyses, N-terminal Edman degradation and amino acid analyses. Amino acid sequenc e of VAPP was: N-terminus VLSAADKSNVKAAWGKVGGNAPAFGAEALLRM.

结合激光解析电离飞行时间质谱,N-端Edman降解和氨基酸分析结果表明,该多肽是由32个氨基酸残基组成的直链多肽,分子量3 216 u,主要含缬氨酸、丙氨酸、赖氨酸和甘氨酸,无半胱氨酸,其一级结构氨基酸排列顺序为:N端-VLSAA DKSNVKAAWGKVGGNA PAFGAEALLRM,与已知蛋白序列同源性远小于50%。

This text through to various treatment include chromium, last cyanogens and alkali waste water craft comparison of the method sour, treatment craft of choosing economy to be effective separately; Adopt alkaline chlorine France punish, include cyanogens waste water, chemistry reduce, take place, deal with, include chromium waste water, in handle course among to waste water sour alkaline go on regulate, design one small-scale sewage treatment plant, demand to reach second in world and handle the standard.

本文通过对各种处理含铬、含氰及酸碱废水工艺方法的比较,分别选择经济有效的处理工艺;采用碱性氯化法处理含氰废水,化学还原发处理含铬废水,在处理过程中对废水的酸碱性进行调节,并设计一座小型的污水处理厂,要求达到国际二级处理标准。

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