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In order to solve the problems of aging of dope and Weather fastness energy balance,we have researched and developed the impregnant dope of tetracopoly merization,which constitute mainly.

引言含氟聚合物的碳氟键离解能比碳氢键离解要大得多,而碳氟键的键长又比碳氢键短,所以氟树脂有良好的机械性能、优异的耐化学品性、优良的热稳定性、耐侯性以及高度不粘性和低的磨擦系数。

The structure and morphology of CNTs which have been purified and not yet, were characterized by TEM, SEM, XRD, Raman, TG-DTA, BET, IR. The results indicated that when the stokehole reaction temperature was 1170℃,the decompose temperature of Ferrocene was 150℃,he volatilize temperature of Benzene was 50 ℃, hydric flow rate was 270ml/min, the concentration of thiophene was l% and the reaction time was 20 minutes, the CNTs with single-walled and multi-walled were prepared.

结果表明:炉膛反应温度1170℃、二茂铁的分解温度150℃、苯的挥发温度50℃、氢气的流量270ml/min、噻吩体积分数1.00/100ml苯、反应时间20min时,可以得到碳纳米管,既有单壁管又有多壁管,单壁管的内径分布在0.88~1.15nm之间,多壁管的直径分布在40~120nm之间;纯化后的碳纳米管比表面积增加,管壁光滑,而且产生了大量的含氧官能团,有利于在水溶液中的分散。

The structure and morphology of CNTs which have been purified and not yet, were characterized by TEM, SEM, XRD, Raman, TG-DTA, BET, IR. The results indicated that when the stokehole reaction temperature was 1170℃,the decompose temperature of Ferrocene was 150℃,he volatilize temperature of Benzene was 50 ℃, hydric flow rate was 270ml/min, the concentration of thiophene was 1% and the reaction time was 20 minutes, the CNTs with single-walled and multi-walled were prepared. The diameters of the single-walled CNTs are in the range of 0.08~1.15nm, and that of the multi-walled CNTs are in the range of 40~120nm.

结果表明:炉膛反应温度1170℃、二茂铁的分解温度150℃、苯的挥发温度50℃、氢气的流量270ml/min、吩体积分数1.00/100ml苯、反应时间20min时,可以得到碳纳米管,既有单壁管又有多壁管,单壁管的内径分布在0.881.15nm之间,多壁管的直径分布在40120nm之间;纯化后的碳纳米管比表面积增加,管壁光滑,而且产生了大量的含氧官能团,有利于在水溶液中的分散。

The characteristics of the AP include (1) in addition to the formation of hydrogel in aqueous alkaline or polar organic solution, AP can form carbonaceous hydrogel in neutral and acidic aqueous solutions, which extents the application of carbonaceous sol-gel;(2) AP contains a large amount of nitric groups which decomposes quickly by thermal initiation, releasing a large amount of gases and heat, indicating explosive properties of the AP;(3) metal salt-containing AP is also explosible by thermal initiation, and the metal in AP promotes the explosion.

以沥青为碳源,用氧化法制备水性沥青过程中,浓硫酸和浓硝酸的比例、用量、氧化温度及氧化时间对水性沥青的收率皆有影响。经过氧化后,沥青上含有许多含氧官能团,导致水性沥青溶于水。含氧官能团越多,水性沥青越易溶于水。调节制备条件,可使水性沥青不仅可以在碱性水溶液中形成凝胶,而且可以在中性和酸性水溶液中形成溶胶、凝胶,从而拓宽了炭基溶胶—凝胶法制备炭基纳米材料的应用范围。

In this paper, the carbon nanotubes made by CVD were purified by acid solution. Results indicate that the ports of CNTs were oxidated and opened up, the surface of CNTs bring a lot of oxygenous functions, which was useful for dispersion of CNTs in the water solutions.

采用液相氧化法对CVD法制备的碳纳米管进行了提纯,结果表明,经过提纯后碳管的端口被打开且表面产生了大量的含氧官能团,使其在水溶液中的分散性得到了改善。

Oxygen plays critical roles in lubrication mechanism. Oxygen affects the lubrication mechanism of additives all along, whether in sulfurized vegetable oil fatty acids containing active element or not in hydroxy vegetable oil fatty acids with pure carbon, hydrogen and oxygen not containing active element.

氧元素在润滑机理中有着关键作用,无论在含活性元素的硫化植物油脂肪酸,还是在不含活性元素的纯碳、氢和氧的羟基植物油脂肪酸中,氧元素始终影响着添加剂的润滑性。

The distillated condensate of furnace gas showed that NH3 cleaning efficiency will reach to 98% and the recovery rate of CO2 reach to 30% while adoptingMl asabsorber, CO2 in tail gas recovered for carbonation-soda ash production, then ammonia and CO2 are recovered; the condensation of ammonia in waste water is lower than 0.5tt, CO2 is below 0.03tt, so it can be used directly as soft water, then it has decreased the total quantity of various water containing ammonia in soda ash making system and improved environment.

蒸馏炉气冷凝液表明,以M I作为吸收剂,NH_3的净氨率达到98%,CO_2回收率达到30%,尾气中的CO_2再用于碳化制碱,氨和二氧化碳得到回收利用;废淡液中氨的浓度低于0.5tt,CO_2低于0.03tt,可直接作为软水使用,降低了含氨杂水的总量,使纯碱系统不再多余含氨杂水,改善了环境。

In this paper boron-doped diamond single crystals was synthesized at high pressure and high temperature with iron-based catalyst doped with B4C, h-BN and Na2B4O7. The effects of multiple boron sources on diamond were studied according to the characterization of structure and properties of the boron-doped diamond.

本文使用碳化硼、六方氮化硼和硼砂三种硼源材料复合添加的铁基触媒在高温高压下合成含硼金刚石,通过对金刚石结构与性能的表征,探讨多种硼源复合添加对含硼金刚石的影响。

Methods Cells were maintained in DMEM medium with 10% fetal bovine serum. Five days before the beginning of experiments, the cells were seeded in phenol red-free DMEM medium containing 5% charcoal dextran-treated FBS. The cells were harvested, and seeded in 6-well culture plates or in 75ml flacks. After NP, BisA and DBP treatments for 72h, the cells were harvested, and mRNA and protein expression of PCNA, bcl-2 and bax were detected by reverse transcription-polymerase chain reaction and immunohistochemistry, respectively.

方法]T47D细胞在含10%胎牛血清的DMEM培养液中进行常规传代培养,实验前将细胞转移至无酚红DMEM(含5%活性碳葡聚糖苷处理过的FBS)中继续培养5d,收集细胞,PBS洗涤后接种於内置盖玻片的6孔板或75ml培养瓶中,用32×10^(-7)mol/L NP、32×10^(-7)mol/L BisA及32×10^(-6)mol/L DBP对细胞分别处理72h,用半定量RT-PCR技术观察这3种化合物对核增殖抗原PCNA、bcl-2及bax mRNA表达的影响,并用免疫组化方法对结果进行验证。

Lignocellulose is the most abundant biomass in the world, its two major components, cellulose and hemicellulose, are composed of hexoses and pentoses, therefore, lignocellulosic biomass can be a very good feedstock for producing bioethanol and biohydrogen by some microorganisms via fermentation.

木质纤维素是地球上量最丰富的生质物,其所含的纤维素和半纤维素由六碳醣和五碳醣组成,因此若能将木质纤维素分解醣化,它正是用微生物以发酵的方式生产乙醇或氢气的最佳原物料。

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