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Benzyloxy benzoyldimethylsulfoxide was prepared by the reaction of ethyl 4-benzyloxybenzoate and dimethyl sulfoxide in the presence of sodium hydride, followed by Pummerer reaction with concentrated hydrochloric acid to afford eo-hydroxy-co-thio-methyl-(4/-benzyloxy) acetophenone, which reacted with urea, thiosemicarbazide, semicarbazide hydrochloride and o-phenylenediamine to give imidazolidine-2,4-dione, l,2,4-triazine-3- one and quinoxaline derivatives, respectively.

本文用4-苄氧基苯甲酸乙酯和二甲亚砜为原料,在氢化钠存在下反应,合成了(4′-苄氧基)-苯甲酰基-二甲亚砜。研究了该亚砜在浓盐酸的存在下发生的Pummerer重排反应,用重排产物ω-羟基-ω-甲硫基-(4′-苄氧基)-苯乙酮分别与尿素、氨基脲、氨基硫脲和邻苯二胺反应合成了2,4-咪唑啉-二酮、1,2,4-三嗪-3-酮、喹喔啉等含氮杂环化合物。

For this,experimental study was made on a new process of potential-controlled preferential flotation in a sequency of copper,lead and zinc,which used LP-01 as collector for copper mineral,DDTC as collector for lead mineral,copper sulfate and butyl...

为此,以LP-01为铜矿物的捕收剂、乙硫氮为铅矿物的捕收剂、硫酸铜和丁黄药为锌矿物的活化剂和捕收剂、石灰为矿浆电位调整剂,并在选铜、铅时配合使用铅矿物的组合抑制剂ZnSO4+YN,对该多金属复杂硫化矿进行了电位调控铜、铅、锌依次优先浮选新工艺试验研究,获得了含铜21.74%、铜回收率62.31%的铜精矿,含铅61.23%、铅回收率55.07%的铅精矿和含锌56.43%、锌回收率90.02%的锌精矿。

In this paper, quantum chemistry methods were used to investigate themicrocosmic reaction mechanisms and dynamics of a series of activatenitrogen-, sulfur- and halogen-containing radicals and some smallmolecules in the gas phase theoretically, including isocyanic acid,isothiocyanic acid and ketenyl radical.

本研究论文是采用量子化学理论和计算方法,对异氰酸 HNCO、异硫氰酸 HNCS 及其自由基、乙烯酮自由基 HCCO 与若干气相含氮、硫、卤素的活性小分子自由基反应的微观反应动力学进行理论计算研究。

In this paper, quantum chemistry methods were used to investigate the microcosmic reaction mechanisms and dynamics of a series of activate nitrogen-, sulfur-and halogen-containing radicals and some small molecules in the gas phase theoretically, including isocyanic acid , isothiocyanic acid and ketenyl radical .

本研究论文是采用量子化学理论和计算方法,对异氰酸HNCO、异硫氰酸HNCS及其自由基、乙烯酮自由基HCCO与若干气相含氮、硫、卤素的活性小分子自由基反应的微观反应动力学进行理论计算研究。

Sulfur can promote the formation of chlorophyll; sulfur involved in the process of nitrogen fixation, to increase the utilization rate of fertilizer; in cruciferous rape, peanuts propylene mustard oil, Liliaceae onions and garlic contained in Suanyou fat, such as sulfur compounds in human nutrition and medicine There are special effects to enhance the quality of these crops.

硫能促进叶绿素的形成;硫参与固氮过程,提高肥料利用率;十字花科中油菜、花生的丙烯芥子油,百合科葱、蒜中所含的蒜油等硫脂化合物在人体营养和医药方面有特殊的功效,提高这类作物的品质。

As CAAX-mimetics, 1, 3-dihydro-5-phenyl-2-H-1, 4-benzodiazepin-2-one was modified by linking carboxyl groups with various carbon through N-1 and C-3, 3-(imidazol-4-yl) propion amido group with different substituents was connected at C-7; In the synthesis of bisubstrate analogues, thiocarbamido compounds was alkylated by alkyl iodide and then hydrolyzed to give alkylthiol benzoate compounds.

1,4-苯并二氮杂草-2-酮类化合物的合成过程中分别对其1、3、4和7位进行了基团变化,在1和3位连接不同长度含羧基或酯基的侧链,在7位连接不同取代的咪唑丙酰氨基。在苯甲酸硫醇酯化合物合成过程中,建立了一种硫原子连有不同长度碳链的苯甲酸硫醇酯的合成方法。

Sulfur ore concentrate to chromic, nickel, in zinc waste water treating processes, increment, agitation time factors and so on discussed the temperature through the experiment, has thrown galvanizes the heavy metal waste water to sulfur ore concentrate processing the influence, thus obtains the galvanization waste water processing being suitable experimental condition.

本课题采用的硫精矿是邯郸市插箭岭磷肥有限公司所提供,硫精矿对含铬、镍、锌废水的处理过程中,通过实验探讨了温度、投加量、搅拌时间等因素对硫精矿处理电镀重金属废水的影响,从而得到电镀废水处理的适宜的实验条件。

It must be grinded strictly before processing;(2) sulphide iron ore has high tin content, it is necessary to recover tin ore from this mineral.

选别时必须磨到一定的细度;(2)硫铁矿物含锡高,有必要在硫铁矿物中回收锡石。

Chlorine contents of the representative composition of MSW are quantitatively analyzed by using silver nitride volumetric analysis method, mercury thiocyanate spectrophotometer method and ion chromatography method etc, the results have been tabled and the determination methods are confirmed.

文章首先分析了入炉垃圾中PVC类的主要赋存形态,常见塑料的用途和种类,选用有代表性的垃圾组分采用离子色谱法、硝酸银容量法和硫氰酸汞分光光度法测定垃圾组分含氯量,得到了常见垃圾组分的含氯量数据,确定了不同垃圾组分的含氯测定方法。

Tourmaline rock s widely occur within the pyrite deposits of the Proterozoic rift in the eastern part of Liaoning province, particularly in the pyritized sequences of the Gaojiayu formation of the Liaohe group.

电气石岩在辽东元古宙裂谷内的硫铁矿床中广泛发育,辽河群高家峪含矿建造中,富电气石岩主要与硫铁矿体成矿关系密切。

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