含氮的

Starting from 3-benzoyl-5-formyl-indolizine, 3-benzoyl-5-(2'2'-diacetylethenyl)-indolizines and analogs were obtained by the 〓mediated aldol condensation or Wittig reaction. These compounds,promoted by low-valent titanium, gave highly functionlizedcycl[3,2,2]azine derivatives. The coupling reaction proceeded betweenthe carbonyl group and the carbon-carbon double bond, a rare example inMcMurry reaction.

我们以3-苯甲酰基-5-甲酰基中氮茚为原料，通过三碘化钐促进的aldol反应和Wittig反应制备了3-羰基-5-羰基乙烯基中氮茚，随后经低价钛还原偶联，没有生成正常的分子内羰基-羰基偶联产物，而是得到反常的羰基与α，β-不饱羰基的双键偶联产物，较高收率地得到了含多官能团的CycI[3，2，2]azine衍生物。

The synthesis methods of energetic salts and energetic ionic liquids(cations including triazole, tetrazole, bridged azole, hexamethyenetetrammonia, etc;and anions including nitrate, perchlorate, azide, tetranitratealuminate, polycyan anion, N,N'-dinitrourea, etc.) are reviewed, and the effects of cations, anions and their substitution groups on melting point, enthalpy of formation, density of the materials are summarized.

本文综述了多种含能盐和含能离子液体（阳离子包括三唑、四唑、双环唑、六次甲基四胺等；阴离子包括硝酸根、高氯酸根、硝基唑、叠氮根、四硝基铝、多腈基化合物、二硝基尿素等）的合成；结合其表征结果分析了阳离子上的取代基以及阴阳离子对它们的性能如熔点、生成焓、密度等的影响。

A series of novel dendrons with 1,3,5-triazine structure were synthesized by convergent strategy using cyanuric chloride, p-hydroxyazobenzene,β-naphthol, 1-hydroxyanthraquinone, 3,5-dihydroxybenzyl. They were the first generation p-phenyl-azo-phenyloxy-terminated dendron G1.0, the first generation naphthyloxy-terminated dendron G1.0, the first generation naphthyloxy-terminated and 1-anthraquinonoxy-cored dendron G, and the second generation naphthyloxy-terminated dendron G2.0.

以对羟基偶氮苯、β-萘酚为端基，三聚氯氰、3，5-二羟基苄醇为支化单体，1-羟基蒽醌为核心，用收敛法合成了一系列新型结构的含均三嗪环的树枝块：第一代端基为偶氮苯的树枝块G1.0、端基为萘氧基的树枝块G1.0、端基为萘氧基、中心为蒽醌的树枝块G、第二代端基为萘氧基的树枝块G2.0。

2 New carbonyl functionalized imide derivatives of maleimide were synthesized by the direct reaction of amino acids with maleic anhydride.

用氨基酸与苹果酸酐直接反应，合成了两个含羧基官能团的苹果酰亚胺，为氨基酸氮端的保护以及含羧基官能团的酰亚胺类化合物的合成提供了一种直接、简便的新方法。

The novel complex (1) in which both benzylic nitrogens and heteroaromatic ones to the same metal ion with the rigid ligand imposed by the large heteroaromatic moiety first time was synthesized; a 2: 1 (ligand: metal ions) type complex which has steric resistance and strong thermochemical driving force was obtained. The crystal structures of characteristic ligand (LA4) and complexes (4, 7, 10), in which one cell includes two moieties: there exist minute difference in coordinated bonds and angles despite the same metal ions with the same ligand, were obtained. It shows that several stable conformation in one complex cell.

首次合成了含邻菲罗啉的具有较大刚性的四氮配体中四个氮原子全部与同一金属离子配位的配合物的晶体结构；得到了一个在空间上存在位阻作用的配体与金属离子2：1结构的晶体；解析了具有特色的一个配体（LA4）和三个配合物（4、7和10）的晶体结构，其中的配体与金属离子的配位作用显示出细微的差异，表明在同一金属配合物的晶胞中，可以同时存在着多个稳定的构象。

Relevant works of other groups worldwide are introduced, espically as the synthesis, performance and application investigation of tetrazine, tetrazole and furazan based HiNC.

本文综述了新型高氮化合物及其含能材料的研究进展，介绍了国内外近十年来众多研究小组的相关工作，重点阐述了四嗪、四唑和呋咱3大类高氮含能化合物的合成、性能及应用研究进展。

According to the microalloying and strengthening and toughening principles of steel,a theoretical calculation method and optimum alloying design to determine titanium content in carbonizing steel were proposed.

根据钢铁材料的微合金化原理和强韧化原理，对广泛使用的含钛渗碳钢的钛含量进行了理论计算分析和优化设计，结果表明，适当降低钛含量，不影响其在渗碳过程中阻止奥氏体晶粒长大的作用，但可有效地减少或消除含钛渗碳钢中的液析氮化钛，从而提高钢材的力学性能。

In this paper boron-doped diamond single crystals was synthesized at high pressure and high temperature with iron-based catalyst doped with B4C, h-BN and Na2B4O7. The effects of multiple boron sources on diamond were studied according to the characterization of structure and properties of the boron-doped diamond.

本文使用碳化硼、六方氮化硼和硼砂三种硼源材料复合添加的铁基触媒在高温高压下合成含硼金刚石，通过对金刚石结构与性能的表征，探讨多种硼源复合添加对含硼金刚石的影响。

Three series of disperse dyes based on heterocyclic diazo components have been designed. The structures of the synthesized compounds were identified by MS, IR and NMR.

本文设计并合成了三个系列的含杂环重氮组分的偶氮分散染料，通过质谱、红外光谱及核磁共振谱等测试手段验证了所合成的化合物的结构。

Lead as activator in the fluorescent powder (1 % lead by weight or less) of discharge lamps when used as sun tanning lamps containing phosphors such as BSP (BaSi2O5 b) as well as when used as speciality lamps for diazo-printing reprography, lithography, insect traps, photochemical and curing processes containing phosphors such as SMS (Sr,Ba2MgSi2O7 b.

放电灯中的萤光粉中作为触媒剂的铅含量在其重量的1%以下，当放电灯用作含磷仿日晒灯，比如含有BSP(BaSi2O5 b)，以及用于重氮复印、平版印虫器、光化学和食物加工过程的含磷特种灯时，比如SMS(Sr，Ba2MgSi2O7：Pb 。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。