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To improve the cyano reactivity, cyano-terminated PPENs were prepared by the end-capping reaction of PPEN-OL with CBN; benzonitrile terminated polys were also prepared by the polycondensation of excess 4,4'-oxydianiline with 1,2-dihydro-2-(4-carboxyphenyl)-4-[4-(4-carboxyphenoxyl)phenyl]-phthalazinone, followed by end-capping with CBA. The polymers synthesized exhibited good solubility in NMP, DMAc and DMF, and were crosslinked to afford phenyl-s-triazine-containing polymers under the similar conditions.

为提高氰基活性,以对氯苯腈为原料,对PPEN-OL进行封端,设计合成了含氰端基的聚芳醚腈;以含二氮杂萘酮联苯结构二酸单体与4,4'-二氨基二苯醚为原料,经Yamazaki膦酰化缩聚,并用对氰基苯甲酸进行封端,合成了含氰端基的聚芳醚酰胺。

To promote development of low alloy steel bearing vanadium and mitrogen,the process,conditions and products of preparing nitrided ferrovanadium and vanadium nitride are introduced on the basis of main documents.

为推动含钒氮低合金钢的发展,在查阅主要文献的基础上,重点介绍了氮化钒铁及氮化钒制备的工艺方法、条件及产品情况。

The results of tests for production of 400?MPa-grade vanadium bearing concrete steel(Ⅲ-grade 20?MnSiV concrete steel)using VN alloying and ferrovanadium alloying were introduced.

介绍了攀钢采用氮化钒合金化与钒铁合金化生产 40 0MPa级含钒钢筋(2 0MnSiVⅢ级钢筋)的对比试验结果,研究了钒、氮微合金化对钢筋的性能和组织的影响,探讨了氮化钒的强化机理,比较了使用两种合金的生产成本。

OBJECTIVE To determine the relative and absolute molecular weight of working reference substance of Grifolafrondosa beta-Glucan and compare the two analysis methods.

目的测定灰树花倍他葡聚糖工作对照品的相对及绝对分子质量,并对两种分析方法进行比较。方法色谱柱为TSK-G4000PW,流动相为0.7%硫酸钠(含0.02%叠氮化钠)或0.2%叠氮化钠溶液,流速为0.5 mL.min-1,柱温为35℃,高效凝胶渗透色谱法用示差折光检测器,高效凝胶渗透色谱和激光光散射联用法用DNDC仪和激光光散射仪联用。

NH3-N is convered in to nitrogen under the condition of anoxic, which is termed as nitrification.

生物脱氮是指利用微生物将含氮化合物中的氮转化为氮气,它分为硝化和反硝化两个过程。

The use of benzazepin-N-acetic acid derivatives which contain an oxo group in the a position to the nitrogen atom and are substituted in the 3 position by a 1--cyclopentyl-carbonyl-amino radical, and of their salts and biolabile esters, for the prophylaxis and/or treatment of heart damage caused by cardiotoxic doses of medicaments or chemicals, in larger mammals and in particular humans.

本发明涉及苯并氮杂∴-N-乙酸衍生物及其盐和生物不稳定的酯的应用,其中苯并氮杂∴-N-乙酸衍生物在氮原子的α位置含有氧代基,且在3-位置上被1--环戊基-羰基-氨基残基取代,用于预防和/或治疗大的哺乳动物和特别是人体的心脏损伤,其中心脏损伤是由心脏中毒剂量的药物或化学品引起的。

Good thermal stability and self-extinguishing behavior was observed with the cured polybenzoxazine resins. Second, furan-containing benzoxazine monomers, P-FBz, BPA-FBz, and 4FP-FBz were prepared using furfurylamine as a raw material. Formation of furfurylamine Mannich bridge networks in the polymerizations of P-FBz and BPA-FBz increased the cross-linking densities and thermal stability of the resulting polybenzoxazines. P-FBz and BPA-FBz- based polymers also exhibited high glass transition temperatures above 300℃, high char yields, and low flammability with a limited oxygen index value of 31. The dielectric (Dk3.21–3.39) and mechanical properties (high storage modulus of 3.0–3.9 GPa and low coefficient of thermal expansion of 37.7– 45.4 ppm) of the P-FBz and BPA-FBz-based polymers were superior or comparable to other polybenzoxazines. 4FP-FBz used for polybenzo- xazine modification by means of formation of benzoxazine hybridation with P-FBz.

第二部份以2-呋喃甲胺为起始物,制备了P-FBz、4FP-FBz与BPA-FBz 三个含呋喃官能基之氧代氮代苯并环己烷的单体;BPA-FBz与P-FBz於开环聚合中形成之Mannich bridge网状结构有效地提升聚氧代氮代苯并环己烷聚合物之交联密度与热安定性;Poly与Poly具有大於300℃之玻璃转移温度、高的焦炭生成率与具有31之极限氧指数(Limited oxygen index, LOI)的难燃性特质,Poly与Poly之介电常数(Dk=3.21~3.39)与机械性质[3.0~3.9 GPa的储存模数与37.7~45.4ppm之低热膨胀系数( Low coefficient of thermal expansion, Low CTE)]均较其他聚氧代氮代苯并环己烷为优;4FP-FBz具有低之介电常数(Dk=2.7),以其作为降低介电常数之反应型改质剂,与P-FBz混成,证实可有效地降低Poly的介电常数。

Amino-6-nitrobenzodifuroxan was prepared through a three-step reaction from starting material 3, 5-dinitrobenzoic acid:(1)3, 5-dinitroaniline (1) was synthesized from the reaction of DNBA and hydrazoic acid in inert solvent 1, 2-dichioroethane through Schmidt rearrangement with yield of 89.6%;(2) 1 was subjected to nitration to prepare pentanitroaniline (2) with yield of 51.1%;(3) The title compound was prepared from 2 and sodium azide in acetic acid through denitrogenation and then Schmidt rearrangement with yield of 86.8%, m.p.204℃~206℃.

以3,5-二硝基苯甲酸为原料经过3步反应合成了7-氨基6-硝基苯并二氧化吠咱:第1步反应,在二氯乙烷惰性溶剂中,DNBA与叠氮酸反应并发生Schmidt重排反应生成3,5-二硝基苯胺(1),产率89.6%;第2步反应,1在含100%硫酸的硝硫混酸中硝化生成五硝基苯胺(2),产率51.1%;第3步反应,2与叠氮酸反应,不经分离直接进行热解脱氮、Schmidt重排反应,得到目标化合物, m.p.204℃~ 206℃,产率86.8%。

To improve the nonlinear optical property and stability of azo-dye chromophore, the nonlinear optical polyimide attached with azo chromophore side-chain is synthesized by diazo coupling reaction of 4-nitrohenzediazonium tetrafloroborate.

为了提高材料的非线性光学性能和偶氮染料发色团的稳定性能,通过对-稍基苯基重氮氟硼酸盐的重氮偶合反应,合成了侧链含偶氮非线性光学活性基团的聚酰亚胺材料,幷用红外光谱对其进行了结构表徵。

There was an obvious effect of different N, P and K application rates on N, P, K concentration of stem, leaf, rhizome and total ginger plant in each growth period, the uptake and accumulation of nutrient and distribution increased greatly. Ginger in the treatments of moderate fertilizer application rate of N450, P120 and K450 had a higher N, P and K concentration, which resulted in the increase amount of nutrient uptake and accumulation.

施用不同数量的氮磷钾对各生育期生姜茎、叶、姜各部位及全株N、P、K含量和养分吸收积累量、养分分配有明显影响,中等施肥量的N450、P120和K450处理在整个生育期含N、含P和含K量均较高,养分吸收量和积累量显著增多。

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书,王祥生,李德昌。安徽省首次发现嗜群血蜱。

Chapter Three: Type classification of DE structure in Sino-Tibetan languages.

第三章汉藏语&的&字结构的类型划分。