吡啶

AIM: To establish a method to determine 2,6Dimethyl4(3nitropheny1)1,4 dihydropyridine3carboxylic acid dimethylester5carboxylic acid pentyl ester (MN9202) in biological medium by reversephase highperformance liquid chromatography.

目的：建立生物介质中1，4二氢2，6二甲基4(3硝基苯基)3，5吡啶二甲酸甲戊酯（MN9202）的高效液相色谱检测方法。

Mission:"equality and mutual benefit, reputation first, unity and cooperation and friendship between the long-term" supply products: ethylenediamine; diethylamide; triethylamine; Diethylenetriamine; three ethylene diamine; three ethylene amines 40; 40 Five ethylene amines; five ethylene amines 6; caprolactam; DMF; allyl amine; N, N dimethylaniline; propylamine; are butylamine; are TOA; 3 Poly Cyanamide; 1,2 c diamine; ethanolamine; diethanolamine, triethanolamine; potassium iodide, potassium hydroxide, potassium permanganate, toluene, xylene, toluene of chlorine ; Acetone, butanone; acetylacetone; ethyl acetate, butyl acetate; Y-butyrolactone; DMC; acetyl of methyl acetate; Sanfu acetyl acid; Sanfu acetyl B Ethyl; methanol, ethanol, isopropanol; propylene glycol; glycerol; propargyl alcohol; 1.3 propylene glycol; xylitol; acetic acid; have acid; mercaptoacetic acid; vary Bitterness; adipic acid; trifluoroacetic acid; oxalic acid, the amino acid; o-amygdalin acid; DL-Acid; anhydrous piperazine; six non-piperazine, furfural, castor oil, ethylene Aldehyde; glutaraldehyde, multi-POM; isopropyl ether; anisole; tetrahydropyrrole; pure pyridine; 1.2 dichloroethane; methylene chloride, chloroform, carbon tetrachloride; hydrazine hydrate; Nonylphenol;-m-cresol; Se phenol; phenol; the tert-butyl phenol; Titanium Dioxide; iron; full Tangfen; Bisphenol A; azo two different nitrile; sodium azide; sodium carbonate ; Sodium chloride; iron oxide; cuprous chloride; thionyl chloride; D4; sodium bicarbonate; ammonia, potassium chloride; anhydrous sodium sulphite; ammonium persulfate; glycol Dingmi; B Glycol ether; calcium chloride; cyclohexanone; cyclohexane, methyl tertiary butyl ether, potassium carbonate, ferric chloride, potassium nitrate; Linsuansanna; zinc oxide; sodium nitrite; antimony oxide; Tartrate; OP-10; TX-10; tablets base; AES; sodium benzoate, sodium citrate; partial sodium silicate, sodium perborate, a sodium carbonate, sodium benzene; Asia sodium chlorate; Wuluo Care products; urea; hydrochloric acid, sulfuric acid, lactic acid; amino acid, hydrogen peroxide, ammonium bicarbonate

公司宗旨："平等互利，信誉至上，团结合作，友谊长久"乙二胺；二乙胺；三乙胺；二乙烯三胺；三乙烯二胺；三乙烯四胺；四乙烯五胺；五乙烯六胺；己内酰胺；二甲基甲酰胺；烯丙基胺；N，N二甲基苯胺；正丙胺；正丁胺；正辛胺；三聚氰胺；1，2丙二胺；一乙醇胺；二乙醇胺；三乙醇胺；碘化钾；氢氧化钾；高锰酸钾；甲苯；二甲苯；对氯甲苯；丙酮；丁酮；乙酰丙酮；醋酸乙酯；醋酸丁酯；Y-丁内酯；碳酸二甲酯；乙酰乙酸甲酯；三伏乙酰乙酸；三伏乙酰乙酸乙酯；甲醇；无水乙醇；异丙醇；丙二醇；丙三醇；丙炔醇；1.3丙二醇；木糖醇；冰醋酸；己醛酸；巯基乙酸；异辛酸；己二酸；三氟乙酸；乙二酸；对氨基苯乙酸；邻氯苦杏仁酸；DL-扁桃酸；无水哌嗪；六无哌嗪；糠醛；蓖麻油；乙二醛；戊二醛；多聚甲醛；异丙醚；苯甲醚；四氢吡咯；纯吡啶；1.2二氯乙烷；二氯甲烷；三氯甲烷；四氯化碳；水合肼；壬基酚；纯间甲酚；硒酚；苯酚；对叔丁基苯酚；钛白粉；铁粉；全糖粉；双酚A；偶氮二异丁腈；叠氮化钠；碳酸钠；氯化钠；三氧化二铁；氯化亚铜；氯化亚砜；D4；碳酸氢钠；氨水；氯化钾；无水亚硫酸钠；过硫酸铵；乙二醇丁醚；乙二醇乙醚；氯化钙；环己酮；环己烷；甲基叔丁基醚；碳酸钾；三氯化铁；硝酸钾；磷酸三钠；氧化锌；亚硝酸钠；氧化锑；酒石酸；OP-10；TX-10；粒碱；AES；苯甲酸钠；柠檬酸钠；偏硅酸钠；过硼酸钠；过碳酸钠；苯磺酸钠；亚氯酸钠；乌洛托品；尿素；盐酸；硫酸；乳酸；氨基磺酸；双氧水；碳酸氢铵

RESULTS:LMWH 16000 and 8000 u.L-1 could significantly inhibit the constriction of the isolated ileum smooth muscle of ovalbumin-sensitized guinea pigs induced by OA in vitro (P0.01,P0.05 vs vehicle);LMWH 200,50 and 12.5 u.kg-1ip could markedly inhibit the degranulation of pericranium MC in rats (P0.01 vs vehicle),LMWH 60 and 30 u.kg-1 ip could sigificantly depress the licking response induced by 4-aminopyridine and the increasing of capillary permeabili ty induced by acetic acid in mice (P0.01,P0.05 vs vehicle).

结果：LMWH 16000 u.L-1(P0.01)和8000 u.L -1(P0.05)均能显著降低OA所致的致敏豚鼠离体回肠平滑肌收缩高度；LMWH 200，50和12.5 u.kg-1 (P0.01)均能明显抑制颅骨骨膜肥大细胞脱颗粒；LMWH 60 u.kg-1(P0.01)和30 u.kg-1(P0.05)均能显著减少4-氨基吡啶诱发的小鼠舔体反应次数，并能抑制冰醋酸所致的小鼠毛细血管通透性增加。

METHODS:Guinea-pigs were sensitized by ovalbumin and the effects of LMWH on the constriction of ileum smooth muscle induced by OA were observed in vitro;The effects of LMWH on the degranulation of pericranium mast cell induced by OA were observed throu gh the passive anaphylaxis ratmodel which was made by vaccinating antiserum at pericranium;Licking response was induced by 4-aminopyridine(4-AP) scat scruff in mice,then the effect of LMWH on licking response was studied the capillary p emeabilty increasing induced by glactal acetic acid and the effect of LMWH on ca pillary pemeability were studied.

用卵白蛋白(ovalbumin，OA)免疫豚鼠造成过敏模型，观察LMWH对OA所致的豚鼠离体回肠平滑肌收缩的影响；在大鼠颅骨骨膜接种抗血清使肥大细胞被动致敏，观察LMWH对OA引起肥大细胞脱颗粒的影响；以4-氨基吡啶诱发小鼠舔体反应，观察LMWH对舔体反应的影响；以冰醋酸使小鼠毛细血管通透性增加，观察LMWH对通透性的影响。

The method is based on the catalytic effect of trace activated manganese on the oxidation of brilliant green and 1-(2-pyridylazo)-2-naphthol by patassium periodate in Na2HPO4-KH2PO4 medium.

研究了在pH6.15的Na2HPO4-KH2PO4缓冲溶液介质中，氨三乙酸活化痕量锰催化高碘酸钾氧化灿烂绿和1-(2-吡啶偶氮)-2-萘酚褪色的指示反应。

Three new ternary copper complexes: 3.5H2O(1)、 2H2O (2) sand 1.5H2O(3)(phen=1, 10-phenanthroline, tatp=1, 4, 8, 9-tetranitrogen, dppz =dipyrido [3,2-a; 2,3-c]phenazine, Gly-L-Val=Gly-L-Valine), were synthesized characterized by elemental analysis, molar conductivity, IR and UV-Vis spectroscopes.

本文合成了3个新的三元铜配合物：3.5H2O(1)、2H2O(2)和1.5H2O(3)［Gly-L-Val=甘缬二肽，Phen=l，10-邻菲咯琳，TATP=l，4，8，9-四氮三联苯，DPPZ=二吡啶并［3，2-a；2，3-c］吩嗪］。通过元素分析、红外光谱、紫外－可见光谱以及摩尔电导率测定对这些配合物进行了表征。

The maximal absorption band could be assigned mainly to intra-ligand charge transfer transition character. It mostly originated from transitions starting from the phenoxide side containing chlorine to pyridyl side.

最大吸收主要来自配体内电荷转移跃迁，电荷从苯酚环和氯向含氮的吡啶环跃迁。

The results suggest that the electronic π-π* transitions in AlQ_3 are localized on the quinolate ligands; the transition from a phenoxide donor to a pyridyl acceptor includes C→C and O→N transferences. There hardly is any relation to the metal aluminum.

结果表明，电子从基态跃迁到低激发态时主要为π-π*跃迁；电荷从含氧的苯酚环转移至含氮的吡啶环上，包括两环之间 C→ C转移和 O→ N转移，与金属离子关系不大。

The 400nm femtosecond laser photoionization and dissociation of pyridine-(water 〓 cluster was studied.

在吡啶-水团簇的质谱中同样看到了在纳秒激光下看不到的非质子化产物〓。

The photosensitization effects of trisruthenium- on DNA caused by visible light has been studied by using of agarose electrophoresis.

采用琼脂糖凝胶电泳研究了以可见光引发的三联吡啶钌与DNA之间的光敏反应。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了