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Reaction conditions are studied, and the result shows that it is better to adopt mercuric oxide or mercuric fluoride as fluorination catalyst with reaction temperature -20~-10℃.

结果表明,采用氧化汞或氟化汞作氟化催化剂、氟化氢作溶剂较好,适宜的反应温度为-20~-10℃,较长的反应时间(48 h)和增加氟化氢和催化剂的量有利于氟化。2-氯-5-三氯甲基吡啶的转化率和选择率均可达到97%以上。

METHODS: With formamide as dispersing agent, agarose was sulfated with the method of chlorosulfonic acid-pyridine.

以琼脂糖为原料,甲酰胺为分散剂,通过氯磺酸吡啶法制备了硫酸酯化琼脂糖。

Structure unit 2 was conveniently synthesized from 3-cyanopyridine by methylation, rearrangement reaction, and reduction of formyl.

以价廉易得的3-氰基吡啶为原料,通过甲基化、重排、还原三步反应合成了结构单元2。

A method for determining trace Cu is described based on the catalytic effect of trace copper on the decolorizing oxidation reaction of acid fuchsin by potassium periodate in the presence of a,a'-dipyridyl.

本文研究了在α,α′-联吡啶存在下,铜离子催化高碘酸钾氧化酸性品红褪色的新指示反应及动力学条件,建立了催化光度法测定痕量铜的方法。

96H LC 0,96 h LC 50 ,and 96 h LC 100 of twelve chemicals of phenol ,alkyl benzene and nitrobenzene,and three water samples to sword fish(\%Xiphophorus helleri)\% and rare minnow(\%Gobiocypris rarus\%) were tested.3. The phenol ic waste water was purified through the absorption of polyvingl pyridine.

介绍了含酚废水与聚乙烯基吡啶类树脂接触,酚类会吸附在树脂上,使废水得到净化,然后将吸附了酚类的树脂加热处理回收酚,与此同时,对树脂也进行了再生处理,再生后的树脂可循环使

Monocholesterylsuccinate is synthesized using cholesterol and succinic anhydride as raw materials in heptane and trace pyridine as catalyst.

以正庚烷为溶剂、吡啶为催化剂,采用丁二酸酐和胆固醇以均相法合成了丁二酸单胆固醇酯。

The fluorescence properties and photolysis behavior of this CdS were studied in heptane and pyridine.

用反胶束法合成了用表面活性剂分子磺基琥珀酸双-2-乙基己酯钠盐进行表面修饰的CdS纳米粒子(记为CdS/AOT-SO-3),研究了这种纳米粒子在正庚烷和吡啶溶剂中的荧光及光解行为。

Then the PMAA molecules were modified on the array membranes, molecular transport under different pH value was investigated by fluorescence measurements using tris(22-bipyridyl) dichlororuthenium hexahydrate and quantum dots as probes.

接着将PMAA分子修饰到氨基化金纳米通道阵列膜上,以联钌吡啶和水溶性量子点为探针考察了不同pH值下膜的渗透性。

And then the title compound was synthesized through reacting of 5-fluorouracil with hexyl isocyanate in the presence of 4-(N,N-diethylamino)pyridine as catalyst.

以正庚酸、氯化亚砜和叠氮化钠为原料,通过酰化、库尔提斯重排反应制备异氰酸己酯,然后在4吡啶催化下与5氟尿嘧啶缩合得到抗癌药物卡莫氟,总收率75.4%。

Take CdS for account, hexagonal spherical CdS with average particle size of 50nm was formed in pyridine, cubic rod-like in 1,6 hexyl diamine, mixtures of cubic and hexagonal spherical particles in biethylamine .

以CdS为例,在吡啶中形成六方相球形CdS纳米晶,平均粒径约为50nm;在1-6已二胺中得到的是棒状立方纤锌矿的CdS;在二乙胺中,得到的是立方和六方的混合相,产物形貌为球形粒子。

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