吡唑啉

Several kinds of 4-aminopyrazolone derivatives were synthesized. The reactions between those derivatives and phenol under potassium ferricyanide were used to enrich and determine phenol by an on-line capillary tube coupled with flow injection system with our own design.

文章摘要：本文合成了几种4-氨基吡唑啉酮衍生物，比较了它们在铁氰化钾存在下与苯酚及其衍生物的反应，并利用这些反应生成的化合物于自行设计的流动注射分析系统，实现了总酚在线分离富集。

The quantitative determination method of potassium ferrocyanide in edible salt is described in the paper.

本方法采用蒸馏食用盐中亚铁氰化钾，吸收氰根，吡啶-吡唑啉酮显色定量测定。

The title compound C_(27)H_(23)FN_(4)O_(2)C_(2H_(5)OH was obtained by the reaction of 1-phenyl-3-methyl-5-pyrazolone with 2-fluorobenzaldehyde in ethanol in the presence of piperidine under microwave irradiation and recrystallization from ethanol.

标题化合物C27H23FN4O2(C2H5OH)是由2分子1-苯基-3-甲基-5-吡唑啉酮和1分子2-苯甲醛微波辐射4 m in，用乙醇重结晶得到。

Ethanol was substituted for N,N-dimethyl sulfoxide as solvent of colouring agent pyrazolone and better results were obtained.

改用无水乙醇代替N，N-二甲基甲酰胺作为显色剂吡唑啉酮的溶剂，效果更好。

After the diazotization ,2-aminophenol-4-(2-'carboxy)sulfanil phenylamine was coupled with acetoacetanilide,2-naphthol,1-phenyl-3-methyl-5-pyrazolone,1-naphthol-4-sulfonic acid,separately to get the different diazotized compounds,then complexed with potassium chromium sulfate or cobaltous chloride to obtain the yellow,orange,red,purple,blue and other colour dyestuffs.

2-氨基苯酚-4-(2'-羧基)磺酰苯胺重氮化，分别与乙酰乙酰苯胺、2—萘酚、1-苯基-3-甲基-5-吡唑啉酮、尼文酸、1-乙酰氨基-7-萘酚等偶合，得到不同的偶氮化合物，然后分别与硫酸铬或氯化钴进行络合反应，得到黄、橙、红、紫、蓝多种颜色染料，并进行了毛织品的染色实验。

The sodium salt condensed with phenyl hydrazine in the acid condition to prepare 1 phenyl 3 carbethoxy 5 pyrazolone.

用此盐与苯肼在酸性条件下进行加成缩合反应可制得 1 苯基 3 羧酸乙酯 5 吡唑啉酮。

Sodium diethyl oxalacetate ; \ Claisen condensation ; \ 1 phenyl 3 carbethoxy 5 pyrazolone

钠代草酰乙酸乙酯； Claisen酯缩合； 1苯基3羧酸乙酯5吡唑啉酮

Measurement of cyanide ; isonicotinic acid-pyrazolone colorimetric method ; experimental condition

氰化物测定；异烟酸—吡唑啉酮比色法；实验条件

The lower detection limit was 0.0006 mg/L Conclusion: Compared with the conventional isonicotinic acid 3-methy-1-pheny 1-5-pyrazolone spectrophotometry method, the advantages of the method are auto-sampling, rapid analysis speed and lower reagent consumption, etc.

与传统异烟酸－吡唑啉酮分光光度法相比，该方法具有自动进样、分析速率快、试剂耗量低等优点，可应用于大批量常规地表水分析。

A new photochromic organic compound of thiosemicarbazone, 4-( p -bromo-α-methylaminothiocarbonyl hydrazonobenzal)-2,5-dihydro-3-methyl-5-oxo-1-phenyl pyrazole, was synthesized and characterized by elemental analyses, IR, 1H NMR spectra, and X-ray single-crystal diffraction analysis.

文章合成了一个新的有机化合物1-苯基-3-甲基-4-对溴苯亚甲基-吡唑啉酮-5 缩甲基氨基硫脲(1)，并分别用元素分析、红外光谱、氢核磁共振及X-射线单晶衍射对化合物的结构进行了确证和表征。

By the time of its fall, most of the prisoners were writers who had written against the corruptions of the government.

到它被攻陷的时候，里面多数的犯人是写了反对政府贪污文章的作家。

The most obvious variation to ovum morphological character was that the color was changed from light green to sepiaceous in embryonic development, and all the ovums were almost hatched after 96h.

在胚胎发育过程中卵的形态特征最明显的变化是颜色从淡绿到深褐色，卵在发育96h后卵基本全部孵化。