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Sitafloxacin epimers were separated by capillary zone electrophoresis using γ-cyclodextrin and D-phenylalanine as chiral selector.

以γ-环糊精和D-苯丙氨酸为手性选择剂,采用毛细管区带电泳成功地分离了新型抗菌素西他沙星差向异构体。

A baseline separation of Sitafloxacin epimers was achieved with a background electrolyte of 10 mmol/L KH2PO4-K2HPO4 (pH 4.5), 10 mmol/L CuSO4, 20 mmol/L γ-CD and 10 mmol/L D-Phe. The linear range for Sitafloxacin was 32-400 mg/L (0.996). The relative standard deviations of migration time and peak area were less than 1.9% and 3.8% respectively.

实验结果表明,添加剂的种类和浓度是影响西他沙星手性分离的重要因素,只有当D-苯丙氨酸、铜离子和γ-环糊精同时存在并达到一定浓度时,西他沙星差向异构体在毛细管电泳中才具有良好的分离效果。

Human rights are abso- lute, unconditional and gratuitous. If they are ethicized, the human right relationship between an individual and the state will become the common relationship between an individual and others.

若把人权伦理化,则就把人权之个人或群体与国家或政治社会的关系转变为个人与别人的关系;同时由于伦理的利他性,伦理化的人权就不但不应向别人要求权利,倒是相反地把本应属于个人的权利让渡给别人。

Doubt not but that sin [ 285 ] Will reign among them, as of thee begot; And therefore was Law given them to evince Thir natural pravitie, by stirring up Sin against Law to fight; that when they see Law can discover sin, but not remove, [ 290 ] Save by those shadowie expiations weak, The bloud of Bulls and Goats, they may conclude Some bloud more precious must be paid for Man, Just for unjust, that in such righteousness To them by Faith imputed, they may finde [ 295 ] Justification towards God, and peace Of Conscience, which the Law by Ceremonies Cannot appease, nor Man the moral part Perform, and not performing cannot live.

因此把法律颁发给他们,用以显示他们本质的腐败堕落,鼓动罪恶向法律开战,以便使他们明白法能揭露罪恶而不能取消,虽有像征性的微薄祭物,公牛和山羊的血,也无法赎罪,必须用更贵重的血用公正来为不公正来为人类付出代价。就是说通过信仰归还他们正义,在神前有正确的认识和平安的良心;法律不能用仪式来抚慰良心,人也不能靠实行法律的道德部分而活,法律道德不能实行就不能活。

Metropolitan newspapers are thus turning into city newspapers, a blow to their future prospects, since virtually all the population growth in America is in the suburbs and exurbs.

于是都市报纸开始向城市性报纸转型,这对他们日后的发展是毁灭性的打击,因为事实上现在美国的人口增长都在市郊。

Metropolitan newspapers are thus turning into city newspapers, a blow to their future prospects, since virtually all the population growth in America is in the suburbs and exurbs.

于是全国性报纸开始向城市性报纸转型,这对他们日后的发展是毁灭性的打击,因为事实上现在美国的人口增长都在乡村或郊区。

Metropolitan newspapers are thus turning into city newspapers, a blow to their future prospects, since virtually all the population growth in America is in the suburbs and exurbs.

于是开始向城市性报纸转型,这对他们日后的发展是毁灭性的打击,因为事实上现在美国的人口增长都在

Switch can be adjusted back up hand-held point of view (maximum 80 degrees) and leg drop angle (100 degrees);◆ foot bed lowest point from the ground 130mm, the highest point of the bed from the ground 680mm; also elevated bed of different heights;◆ bed in back with plexiglass plate, the user can seat on the bed for X-ray;◆ aluminum fence, can also choose to use push-pull PP flip rail or fence;◆ lift back, the waist angle of tilt, to prevent the sliding body;◆ by about 2 degrees of seat angle;◆ foot can be bent 100 degrees and can easily get out of bed from the bed and sat up and on;◆ foot horizontal position may rise higher than the height of 120mm;◆ with quiet casters with brakes and can be locked and lifted;◆ durability, operational quality, improved operating performance moving bed;◆ equipped with ABS headboard can be instantly demolished;◆ electric device of high quality fully enclosed permanent magnet DC control system;◆ low noise, high safety, long life;◆ new materials with polyester fiber mattresses;◆ can also choose to use low-rebound double-foam mattress or mattress waterproof material;◆ has good air permeability and durability.

可用手持开关任意调节背部上升角度(最大80度)和腿部下降角度(最大100 度);◆脚部床面最低处离地面130mm,床面最高处离地面680mm;还可升高床面不同高度;◆床体背部采用有机玻璃板,使用者可以座在床上进行X光检查;◆采用铝合金护栏,还可选择采用PP翻动护栏或推拉式护栏;◆抬升背部时,腰部有一定角度的倾斜,为防止身体的滑动;◆采用了约2度的座角;◆足部可以100度弯曲,能够很方便从床上坐起和上下床;◆足部可上升高度比水平位置高120mm;◆采用静音带刹车的万向脚轮,并能进行锁定和解除;◆耐久性、操作性优良,提高了病床搬运的作业性能;◆配有ABS床头板可瞬间拆卸;◆电动装置采用优质永磁直流全封闭式控制系统;◆噪音低、安全性高、使用寿命长;◆配有聚脂纤维新材料床垫;◆还可选择采用低反弹的双层海绵床垫或防水材料床垫;◆具有良好的透气性和耐用性。

METHODS: We assessed the number of fibrocytes in bronchial biopsy specimens and peripheral blood from subjects with mild-to-severe refractory asthma versus healthy control subjects.

我们评估了轻-重度难治性哮喘患者气道活检标本和外周血中成纤维细胞的数量,同时通过体外实验,探讨了调控纤维细胞向气道平滑肌移行的可能机制。

Colorado, protested the crime bill by opening fire on the White House with

击性武器向白宫开火,以表示对打击犯罪法案的抗议。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

The new PS20 solar power tower collected sunlight through mirrors known as "heliostats" to produce steam that is converted into electricity by a turbine in Sanlucar la Mayor, Spain, Wednesday.

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