后中的

Accelerated solvent extraction and Soxhlet extraction were used to extract capparis spinosa seed oil with he-xane and ethyl ether.

采用加速溶剂萃取及索氏提取法，用正己烷和乙醚为提取剂从野西瓜种子中提取油脂，经浓H2SO4催化，甲醇甲酯化处理后，以气相色谱-质谱联用技术鉴定出野西瓜种子中的脂肪酸主要组成为：油酸、亚油酸、硬脂酸等，其中不饱和脂肪酸总量占91.4%，主要成分油酸占73.3%。

The main steps include as follows: CO2 is led into the mother liquor of sodium meta-aluminate to carry out carbon content decomposing; the primary separation between the aluminum and the gallium is realized by primary carbonatation to filter out sodium hydroxide; secondary carbonatation is carried out on the filtrate to obtain the deposit of the complex salt of gallium and aluminum; a sodium carbonate crystal is obtained after the filtered filtrate is condensed and vaporized; the deposit of the complex salt of gallium and aluminum is dissolved in the mother liquor of sodium meta-aluminate; the processes are repeated until the proportion of gallium and aluminum in the complex salt of gallium and aluminum is larger than 1/340; then the complex salt of gallium and aluminum is added into the NaOH liquor and electrolyzed, thus obtaining the metal gallium with a purity larger than 99.9 percent which reaches the level of 3; simultaneously, the byproducts of the aluminum hydroxide and the sodium carbonate during the process of carbonatation by steps are obtained.

主要步骤包括：向铝酸钠母液中通入CO 2 进行碳分分解，一次碳酸化实现铝镓的初次分离；过滤出氢氧化钠，滤液进行二次碳酸化获得镓铝复盐沉淀，过滤后滤液经浓缩蒸发获得碳酸钠晶体，铝镓复盐沉淀溶解在偏铝酸钠母液中，重复上述过程直至铝镓复盐中的镓铝比例大于1/340，将其加入到NaOH溶液中，电解可获得纯度＞99.9％的金属镓，达到3N级水平同时在分步碳酸化的过程中获得氢氧化铝和碳酸钠副产品。

The invention relates to a way to prepare nickel, manganum and cobalt hydroxide. The method includes making the mixed solution a coprecipitate with mixed solution B in base solution C. The mixed solution A contains nickel salt, manganese salt and cobalt salt, the mixed solution B is a strong base solution, the base solution C is aqueous ammonia solution. The solution A also contains ammonium salt while solution B also contains aqueous ammonia; besides, after being mixed, the molarity of ammonia in solution A and solution B is the same with that in solution C.

一种镍锰钴氢氧化物沉淀的制备方法，该方法包括将混合液A和混合液B在底液C中进行共沉淀反应，所述混合液A中含有镍盐、锰盐、钴盐，所述混合液B为强碱溶液，所述底液C为氨水溶液，其中，所述混合液A中还含有铵盐，混合液B中还含有氨水，并且参于等当量反应的混合液A中的铵盐与混合液B中的氨水在混合液A和混合液B混合后氨的摩尔浓度与底液C中氨的摩尔浓度相等。

The UV and IR spectroscopic studies of the monomer films showed that the photoreaction ratio of monomer (about 50%) was higher than the corresponding photosensitive polymer (about 10%, PVCi). The polarized IR spectra proved that obvious anisotropic absorption was displayed in the irradiated photosensitive film. With polarizing microscopy method, we found that these kinds of photoalignment films exhibited good alignment ability, and the stability of the photoalignment film could reach about 100℃. 2 A photosensitive self-assembled monolayer was fabricated that contained photo-cycloadditable groups, such as, coumarin and cinnamate. The reaction process were detected by contact angle method because the IR absorption of monolayer was very weak. The photosensitive self-assembled monolayer promote uniform alignment of nematic liquid crystals by LPUV, and it thermal stability could reach about 130℃. 3 A cationic bolaform amphiphiles was synthesized that had two photosensitive double bonds, and can be polymerized by ultraviolet. A layer-by-layer self-assembled deposition film was prepared in aqueous solution by using this material and poly (sodium 4-styrenesulfonate). The UV-Vis. spectra proved that the multilayers film was uniform and layer-by-layer. When LPUV irradiated the film, the photopolymerizable double bond underwent [2+2] cycloaddition, and the production of the reaction distributed along the polarized direction of incident LPUV. Polarized UV-Vis. spectra indicated that the irradiated self-assembled multiplayer film was anisotropic, and the dichromic ration is about 0.09, it is higher than the spin-coating method of photosensitive polymer or monomer. We used this anisotropic film as alignment layer of nematic liquid crystals, and obtained a uniform and stability alignment result, the static contrast ratio is about 100, which is very close to application of liquid crystal device. This thesis is an instance that the photochemical material was used in the physics region of liquid crystals, the route that was from photosensitive monomer, self-assembled monolayer film to self-assembled multiplayer film was undergone, by this logical research method photoailgnment of liquid crystal was extended and consummated.

围绕上述思路开展了如下工作：1合成了三种可进行光二聚反应的光敏小分子单体，LPUV 辐照制作了光控取向膜；用紫外-可见光谱法和红外光谱法分析了薄膜中的光化学反应，发现小分子的光反应程度可达到50%以上，至少比光敏高分子高出5倍；薄膜的偏振红外光谱证实，经过LPUV 辐照后薄膜出现了明显的各向异性；将小分子光控取向膜制成液晶器件，在偏光显微镜下观察看到均匀一致的液晶取向；并且热稳定性达到100℃左右，接近实用化要求。2制备了含肉桂酸、香豆素基团的自组装单层膜；采用接触角的方法监测自组装反应的动力学过程；紫外-可见光谱证实了自组装单层膜在石英基板表面形成；自组装单层膜经LPUV 辐照后能诱导液晶均匀取向，而且热稳定性可达130℃，热稳定性进一步提高。3合成了含有光敏双键的双季铵盐，在水溶液状态下将它和聚乙烯基苯磺酸钠沉积生成layer-by-layer 自组装多层膜，紫外-可见光谱证实这是一个逐层均匀的沉积；在LPUV 照射下，自组装膜中的光敏双键按照偏振方向发生[2+2]环加成反应，形成取向膜，用二向色性值评价的分子取向度高于高分子及小分子光控取向膜的水平；实验证明用自组装多层膜制成的液晶器件亮暗态均匀，静态对比度约为100，达到实用化器件的水平。

The critical cooling rates in undercooled austenite transformation process of T91 ferritic heat-resistant steel were studied by DIL805A/D high-resolution differential dilatometer. According to the dilatometric measurements, phase transformation kinetic information was obtained with the aid of the analysis of the lever rule from the recorded dilatometric curves.

利用DIL805A/D高精度差分膨胀仪，通过线膨胀行为测量与微观组织分析，获得T91铁素体耐热钢连续冷却转变过程中相关动力学信息，结合冷却后T9l钢组织特征，确定了T91钢过冷奥氏体转变过程中的临界冷却速度。

Results (1) Primary callus came into being 3 days after operation. Mesenchymal cells from peripheral tissues around the primary callus were differentiated into chondrocytes 1 week later. Endochondral ossification was going on then. Bridging callus was formed in the fracture sites 4 weeks after operation.

结果 (1)伤后3 d开始形成原始骨痂。1周时肉芽组织中的间质细胞开始分化为软骨细胞，软骨形成后再进行软骨内化骨。4周时形成连接骨折端的桥接骨痂。

Bone marrow transplantation + habu snake venom + GM-CSF group: recipients received GM-CSF intraperitoneal injection for seven days continuously after habu snake venom injection, and observed the green fluorescence in kidney on above-mentioned times.

骨髓移植+竹叶青蛇毒+GM-CSF组：骨髓移植后的受体鼠在竹叶青蛇毒注射后连续腹腔注射GM-CSF一周，在上述各时间点观察肾脏组织中的绿色荧光。

Bone marrow transplantation + habu snake venom + Ligustrazine + GM-CSF group: recipients received Ligustrazine and GM-CSF intraperitoneal injection for seven days continuously after habu snake venom injection, and observed the green fluorescence in kidney on above-mentioned times.

骨髓移植+竹叶青蛇毒+GM-CSF+川芎嗪组：骨髓移植后的受体鼠在竹叶青蛇毒注射后连续腹腔注射GM-CSF及川芎嗪一周，在上述各时间点观察肾脏组织中的绿色荧光。

B one marrow transplantation + habu snake venom + Ligustrazine group: recipients received Ligustrazine intraperitoneal injection for seven days continuously after habu snake venom injection, and observed the green fluorescence in kidney on above-mentioned times.

骨髓移植+竹叶青蛇毒+川芎嗪组：骨髓移植后的受体鼠在竹叶青蛇毒注射后连续腹腔注射川芎嗪一周，在上述各时间点观察肾脏组织中的绿色荧光。

Among patients with proximal junctional kyphosis, the magnitude of junctional kyphosis correlated directly with the degree of pelvic incidence.

在近侧交界处后凸的患者中，交界后凸的强度与骨盆倾角度数直接相关。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。