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Has established the Avey rhzomorph through the field test remains the analysis method in the sea cabbage and the soil, and remained to it in the sea cabbage and the soil has carried on the determination, the sample with the methyl cyanide extraction, after extracting the revolving concentration nearly did, with the few methyl cyanides dissolves, passed through PRS the solid phase extract column to purify again, eluent air-dried after the nitrogen with the nitrogen methyl imidazole and the trifluoroacetic acid bitter wine grows, the derivative with the highly effective liquid chromatography analysis, used the external standard legal quantity.

通过田间试验建立了阿维菌素在甘蓝及土壤中的残留分析方法,并对其在甘蓝和土壤中的残留进行了测定,样品用乙腈提取,提取液旋转浓缩近干后用少量乙腈溶解,再经PRS固相萃取柱净化,洗脱液经氮气吹干后用氮甲基咪唑和三氟乙酸酐衍生,衍生物用高效液相色谱分析,采用外标法定量。

A self-drilling anchor (10) for use in a friable material (1) comprises a body (12) having an axis (13), a flanged rear end (14), a drilling front end (16) and a generally cylindrical portion (18) therebetween having an outer surface (20) with a thread (22) disposed thereon, wherein the body forks, beginning at a predetermined distance from the flanged rear end, into a first leg (24) and a second leg (26), the first leg extending forwardly into a drilling tip (28) and having a generally rearward facing shoulder (30) angled obtusely outwardly with respect to the axis, wherein the body (12) has an axial bore (32) for receiving an elongate fastener (2), the axial bore (32) extending substantially through the flanged end (14) and the generally cylindrical portion (18) and leading to the generally rearward facing shoulder (30), wherein the anchor (10) has a drilling mode wherein the second leg (26) nests behind the generally rearward facing shoulder (30) of the first leg (24), and an anchoring mode wherein the legs are pivoted apart from one another.

一种用于易碎材料(1)中的自攻螺钉(10),包括:主体(12),其具有中心轴(13)、带有凸缘的后端部(14)、用于钻孔的前端部(16)和位于所述后端部和前端部之间的通常为圆柱状的部分(18),所述圆柱状部分(18)的外表面(20)上布置有螺纹(22),其中主体从距离带有凸缘的后端部的预定的距离处开始分叉为第一腿(24)和第二腿(26),第一腿向前伸入钻孔尖端(28),并且具有相对于中心轴向外成钝角的通常面向后的肩部(30),主体(12)具有容纳细长状紧固件(2)的轴向孔(32),轴向孔(32)基本延伸穿过带有凸缘的端部(14)和通常为圆柱状的部分(18),并且通向通常面向后的肩部(30),螺钉(10)具有钻孔状态和固定状态,在钻孔状态,第二腿(26)套在第一腿(24)的通常面向后的肩部(30)之后,并且在固定状态,腿彼此转动分离。

The difference between the test groups and the control group was statistically significant. It could be deduced that all the insecticides tested in this experiment damaged the spiders′ intestinal mucosa, compromising its function as a barrier and letting large molecules such as FTIC-D more easily penetrate. Among the insecticides, pyrethrin and Bt preparation are bio-insecticides, and the FITC-D concentrations of the spiders exposed to these two bio-insecticides were more than those of the spiders exposed to the chemical insecticides imidacloprid and dipterex. The difference between the bio-insecticide groups and the imidacloprid group was significant, but there was no significant difference between the bio-insecticide groups and the dipterex group.

结果表明:4种杀虫剂处理后拟环纹豹蛛血液中的荧光素浓度远高于对照组,各个处理组拟环纹豹蛛血液样本中的荧光素浓度均与对照组存在极显著差异,可见4种杀虫剂均将对拟环纹豹蛛肠黏膜的屏障功能造成损伤,导致大分子物质易于通过;其中1.5%除虫菊素水乳剂三保奇花和Bt制剂强杀处理后拟环纹豹蛛中肠黏膜的通透性高于仿烟碱类化学杀虫剂吡虫啉处理组,差异达到显著水平,但与有机磷杀虫剂敌百虫处理组差异不显著。

The invention relates to a method for treating gaseous VOCs by a solid extraction-electro-catalytic oxidation method and a device thereof. The method has the steps that: firstly, an electromagnetic type air compressor is used for controlling the gas flowing velocity by a glass rotameter so as to ensure contaminations in the contamination solution in a gas washing bottle to be stripped into an electrochemical reactor; secondly, microporous aeration heads are distributed in the electrochemical reactor, after being stripped into the electrochemical reactor, the gas is distributed in the electrochemical reactor by the microporous aeration heads, takes parts in the electrochemical reaction and passes through the cathode of absorptive and conductive porous material and the anode of iron sheet in sequence; thirdly, the treated gas finally flows out from the top end of the electrochemical reactor and enters into the gas absorption solution.

本发明涉及一种固态萃取-电催化氧化法处理气态VOCs的方法及装置,方法步骤:第一步,电磁式空压机通过玻璃转子流量计控制气体流速,将气体洗瓶中的污染物溶液中的污染物吹脱进电化学反应器;第二步:电化学反应器中布有微孔曝气头,气体吹脱进入电化学反应器后,通过微孔曝气头分布于电化学反应器内,参加电化学反应,依次经过通过吸附性导电多孔材料阴极和Fe片阳极;第三步,经处理后的气体最后从电化学反应器顶端流出进入气体吸收溶液。

It is embodied concretely:(1) With the adoption of grouting bolts, the cranny in wall rocks can be blocked up, the air can be isolated, the wall rocks can be prevented to be weatherized and make water, the strength of wall rocks can also be avoided to be lowered;(2) The lax broken wall rocks are commentated to a whole by liquid after they were grouted and the rock"s strength is increased, so the wall rocks become a part of the support structure by using itself and become a whole with the original rock, and the roadway is made to keep stable but not easy to be broken;(3) The spray layer wall are filled with liquid after grouting, the stress is avoided to be concentrated because the load could be evenly acted on the spray layer and the support;(4) The pressure acted on the plank can be delivered to the two sidepieces and then to the bottom by reinforcing the sidepiece; At the same time, the concentration degree of loads acted on the motherboard can be weaken because of the enlargement of the combination arch"s thickness, as result, the rock"s stress is lowered and the heaving is alleviated;(5) The common bolt is made to be fixed the whole length after grouting, the layers are connected to a integral whole and bear the weight of loads, so the support structure"s unity is increased.

具体体现在:(1)采用注浆锚杆注浆,可以利用浆液封堵围岩裂隙,隔绝空气,防止围岩风化,且能防止淋水和渗水,避免围岩被水浸湿而降低围岩的本身强度及造成的巷道变形。(2)注浆后浆液将松散破碎的围岩胶结成整体,提高了岩体强度,实现利用围岩本身作为支护结构的一部分,且与原岩形成一个整体,使巷道保持稳定而不易产生破坏;(3)注浆后使得喷层壁后充填密实,保证荷载能均匀地作用在喷层和支护上,避免出现应力集中点而首先破坏;(4)注浆后使作用在顶板上的压力能有效地传递到两帮,通过对帮的加固,又能把荷载传递到底板;同时由于组合拱厚度的加大,这样又能减小作用在底板上的荷载集中度,从而减小底板岩石中的应力,减轻底臌;(5)注浆加固后能使普通端锚锚杆实现全长锚固,它们共同将多层组合拱连成一体,共同承载,提高了支护结构的整体性。

Calcium carbonate and soluble glass and so on were confected as alkaline antifouling agent. The Infrared Spectrometry results showed that 2275-2250 cm~(-1) diagnostic absorb wave crest in part A and 3390-3200 cm~(-1) in part B and 1730 cm~(-1) in coating film strongly proved polymers reacted just as the reacting mechanism, that means polysiloxane which offer low-surface-energy property linked Polyurethane system by —OH groups reacting with —NCO groups. Relative molar mass of part A and part B was determined by Gel Permeation Chromatography and the results were appropriate. Surface-energy was determined and results were between 33.6-47.17 mN/m and it increased when alkaline antifouling agent was put into the coating. Alkaline antifouling agent was releasing steadily when the coating film was dipped in seawater. As time gone, the pH value of seawater was increasing. Solubility parameter and results showed that there was no corrasive phenomenon between the polyethylene strand and the coating.

红外光谱分析结果表明,出现在A组分中的2275~2250cm~(-1)处的异氰酸酯特征吸收峰、B组分中的3390~3200cm~(-1)处硅羟基的特征吸收峰及出现在固化后涂膜中的1730cm~(-1)处氨基甲酸酯基团的特征吸收峰证明了涂料成膜物质交联固化符合本文的设计要求,即赋予涂膜低表面能特性的有机硅组分通过—OH基团与—NCO基团的反应已经链接到聚氨酯体系中;凝胶渗透色谱结果表明,成膜物质的A、B组分均为低分子量,符合预聚物的要求;涂膜表面能的测算结果表明,涂膜的表面能在33.6~47.17mN/m之间;加入碱式防污剂后涂膜的表面能略有升高;碱式防污剂的释放平稳,随着涂膜在海水中浸泡时间的增长,pH值有增加的趋势;用溶解度参数原则来评价涂料与网绳的涂装,结果表明,本试验研制的防污涂料对聚乙烯网绳无溶蚀作用。

This paper introduced the application of the coal resource filler after crushing and surface treatment in rubber,which included high sulfur coal,coal gangue stone,fly ash and coal cinder and so on,and the research progress about carbon and silica which were produced by the coal resource wastes.

介绍了高硫煤、煤矸石、粉煤灰和石煤渣等煤炭资源类填充剂经粉碎、表面改性后在橡胶中的应用,以及制备炭黑、白炭黑后应用于橡胶中的进展。

With X-ray diffraction and TEM analysis,it is proved that the microstructures of both undeformed and deformed matrixes are austenite and carbide with some striation structure in the matrixes,the amount of stripes in the deformed matrix is obviously more than that in the undeformed matrix.

通过X衍射和电子显微分析证明,变形前和变形后的基体组织都是奥氏体基体加上碳化物,变形前后的基体中均存在条纹状组织,且变形后基体中的条纹数量明显高于变形前基体中的条纹数量。

The density of AR of HFSC is consistent with the capability of differentiation of those cells. 3. Cells induced in vitro expressed EMA and Lipid droplets were observed by rathonum red staining, while those as control didn't, which confirmed that androgen can facilitate the differentiation of vibrissa follicle stem cells into sebocytes.

用免疫细胞化学检测到EMA在诱导后的细胞中的表达呈阳性,而在未经诱导处理的细胞中的表达呈阴性;用油红O染色检测到诱导后的细胞中有脂滴的形成,而在未经诱导的细胞中没有脂滴的形成;表明雄激素对毛囊干细胞向皮脂腺细胞定向分化具有促进作用。

The results showed that the TiN andN films are polycrystalline phase. The properties and structure of TiN films are mainly determined by the N2 mass flow rate, and as the N2 mass flow rate increases, the structure of the TiN films transforms to f.c.c. type leading to better the properties of films. The presence of negative bias voltage can optimize the grain of TiN films, lower the defect proportion and denser the films, which improves the hardness of films. The TiN films conform to the free carrier absorption mechanism and there are many of free electrons with lower N content in TiN films. With the increase of N content, the quantity of free electrons and reflectivity of films decrease, and the plasma frequence shifts to the lower energy, which leads to the regular change of colors of films from silver, yellowy, golden to yellow-red, meanwhile the lightness of films decreases. The goldenN film consists of TiN and ZrN phase, but belongs to a sigle f.c.c. structure with (111) preferred orientation. The Zr-doping dosen't change the position of the valance band, conduction band and forbidden band ofN film, but leads to the presence of new energy levels, which is the reason thatN film remains golden. The transparent hard films with good corrosion resistance and high hardness have been prepared and the further reseachs showed that the grain size of those films is by far smaller than the wave length and the width of forbidden band of those films is very broad, is the reasons that those films are transparent.

研究表明:氮化钛和N 薄膜为多晶态,氮流量决定了氮化钛薄膜的结构和性能,增加氮流量能使氮化钛薄膜的结构向面心立方结构转变,从而得到性能良好的氮化钛薄膜;施加负偏压能优化氮化钛晶粒和减少薄膜中的缺陷,使膜层变得更致密,从而提高薄膜硬度;氮化钛主要遵循自由载流子光吸收,氮含量较少时薄膜中的自由电子数目较多,随着氮含量的增加,薄膜中的自由电子数目不断减少,反射率逐渐降低,等离子体频率向低能端移动,从而使薄膜颜色出现规律变化,由金属色银白色到淡黄、金黄再到红黄,并且薄膜亮度呈下降趋势;金黄色的N 薄膜中存在TiN 和ZrN 的分离相,但其为单一的面心立方结构并具有(111)面择优取向;相对于TiN 薄膜,Zr 掺杂后,并没有使薄膜的导带、价带和禁带发生变化,只是在TiN 禁带内增加了新能级,这也正是掺杂Zr 后,薄膜仍

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On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.

另一方面,更重要的是由于城市住房是一种异质性产品。

Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.

气候直方图是将所收集的降水量测定值,分为几个相等的区间作为横轴,并将各区间内所测定值依所出现的次数累积而成的面积,用柱子排起来的图形,也叫做柱状图。

You rap, you know we are not so good at rapping, huh?

你唱吧,你也知道我们并不那么擅长说唱,对吧?