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The optimal carrier gas velocity of prepared SE-30 series capillary chromatographic columns was studied and used to separate isomeric compounds. The efficiency of SE-30 capillary chromatographic columns has been studied with different diameters, film thicknesses and oven temperatures, using n-do-decane, phenol, aminobenzene, and butyl acetate as test samples.

研究自制的SE-30系列毛细管气相色谱柱的载气最佳线速度,并应用于同分异构体的色谱分离分别用十二烷、苯酚、苯胺、醋酸丁酯作试祥在不同载气线速条件下对不同口径、不同膜厚、不同柱温的SE-30毛细管色谱柱的柱效进行考察,并在最佳线速度条件下分离异戊醇、硝基氯苯、硝基甲苯及二乙苯同分异构体体系。

High speed countercurrent chromatography was successfully used for the separation and preparation of isomeric compounds .

应用高速逆流色谱法对同分异构体的分离纯化进行研究。

Isopentanol, nitrochlorobenzene, nitrotoluene and diethylbenzene were well separated in the range of optimal carrier gas velocity of 13~17cm/s.

SE-30系列毛细管色谱柱的最佳载气线这范因为13~17cm/s,且在最佳线速度下很好地分离了异戊醇、硝基氯苯、硝基甲苯及二乙苯同分异构体体系。

This paper introduces tests of constituents and isomeric compound contents of PXE、PEPE and M/DBT produced by several chemical plant by way of gas chromatography and gas chromatography-mass spectrograph combination , and also gibes some comments on present status and quality control of the insulation oil.

本文介绍了采用气相色谱分析及气质联用分析方法对各厂家生产的PXE、PEPE、M/DBT的组份及其同分异构体的含量进行测定的情况,对绝缘油品质的现状及质量的控制提出了一些见解。关键词:绝缘油;气相色谱;组分分析;同分异构体

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