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XRD shows: when the value of x is between 0.1 and 0.3, the alloying thin film remains the structure of hexagonal wurtzite and the angle of (002) diffraction peak becomes bigger as the value of X increases; The photoluminescence spectra at room temperature shows that the PL spectra of the alloying thin film is composed of the stronger UV emission band and weaker visible band, and UV emission peak will have the blue shift with the content of Mg increasing and the visible emission weakened.

XRD衍射测试表明:在0.1<x<0.3范围内,合金薄膜仍然保持氧化锌六角型纤锌矿结构,(002)衍射峰位随x的增大向大角度方向移动,在X≥0.3的范围内,合金薄膜的结构则为氧化锌和氧化镁的混合结构;室温光致发光谱表明:ZnMgO合金薄膜PL谱都是由较强的紫外发射带组成,且随着Mg含量的增加紫外发射峰位发生蓝移,同时可见发射增强。

The results indicate that the effect of alloying elements V and Cr on mechanical properties at room-temperature, creep behavior and microstructures are similar. With increasing contents of V and Cr, their mechanical properties produce little change, the creep resistant property decreases and microstructure grows, which is mainly due to their characteristics of β-stability element and smaller atomic radius compared with Ti. On the contrary, the effects of V and Cr on the thermal stability are quite different. With increasing V content or decreasing Cr content the thermal stability for the alloy becomes better, which may be due to the different solution characteristics of V and Cr element in titanium alloy that V belongs to isomorphous β-stability element and Cr belongs to eutectoid β-stability element.

结果表明:合金元素V和Cr对Ti40合金室温力学性能、蠕变行为和组织的影响具有相似性,即随V和Cr含量的降低,合金室温综合力学性能变化不明显、抗蠕变能力减弱、组织粗化:这与V和Cr同属于β稳定元素、且原子半径都小于Ti原子有关;而V和Cr对于热稳定性能的影响则完全相反,V含量的增加或Cr含量的降低含金热稳定性能优化,其主要原因可能与V属于同品型β稳定元素而Cr属于共析型β稳定元素有关。

The distortion of crystal lattice has been recovered by using heat treatment.

为使合金粉末的磁热性能达到试验用样机磁液体的要求,我们用热处理的方法恢复合金粉末的晶格扭曲,使合金粉末的磁热效应回升。

The investigation on rapidly solidified powders produced by ultrasonic gas atomization showed that the two kinds of dispersoids presented in Al-Cu-Fe and Al-Fe-V-Si alloys have simultaneously reformed in the new alloy, there is not any other dispersoid in the powders below 61μm.

对超音速气体雾化快速凝固的上述合金粉末进行的研究表明,新的合金中同时形成原来两个合金系中的析出相;在61 μm的粉末中,没有发现第三种析出相。

Nd and Y showed more evident effects than Gd and La due to lower temperature of eutectic reaction with aluminum. In order to investigate mechanism of the formation of the intercellular dispersoid which is being in debate and possibility of suppressing the dispersoid, a nucleation kinetic model which including unsteady nucleation and effect of alloy element was established.

Al-Fe-Mo-Si-Zr-Ti合金粉末具有四种凝固组织,初生Al〓〓,α-Al与Al〓共晶,胞晶及显微胞晶,合金元素Mo的加入,显著提高合金粉末凝固前的过冷度,使10~40μm粉末的凝固机制发生了变化,由导热控制型转变成溶质扩散控制型,从而基本上消除了该尺寸范围内粉末凝固组织中共晶成分和初生相,但对大于40μm的粉末,因共晶区富Zr核心的优先形成而使Mo的作用效果不明显。

The results show that, by the increment of the cathodic current density,the alloy electrodeposit was formed in displacemental solid solution, and that, with W content raised,lattice parameter expanded,and lattice distortion increased, whereas grain size decreased. All the morphologies of the deposits were presented in neat granular structure in the growth of electrocrystallization.

结果表明,随着电流密度的提高,合金沉积层中的W含量增大;形成置换固溶体的合金沉积层晶格参数涨大、晶格畸变度增大、而显微晶粒尺寸减小;合金沉积层的电结晶生长形态均呈现整齐的团粒状生长特征。

According to IS theory as well as die bond requirement in reality, Au/In was chosen by virtue of appropriate equilibrium diagram and high reaction rate from a variety of binary alloy systems as die bond media. To match CET of chip material of silicon, alloy 42 (Iron-Nickel) rather than copper—2 kinds of lead-frame materials in most common usage, was selected as substrate.

根据等温凝固原理和芯片焊接的实际需要,从多组二元合金中选出了共熔点低、反应速度快的金和铟作为焊接材料;并以硅片作为芯片,从目前最常用的框架材料—铜和铁镍四十二合金中,选出了与硅的热膨胀系数相近的铁镍四十二合金作为衬底材料。

The authers fetched the embryo calvarial peristeum tissue, got human osteoblast by enzyme-assimilating methods and tissue-block culture methods. We observed the morphological change, growth feature and osteogentic capability, of osteoblast during culture in vitro with phase contrast invert microscope, drew the growth curre and identified the cells by alkaline phosphatase dye. At same time, the morphology and bioactivity of 3-5th-generation osbeoblast and anabiotic cells was studied comparatively. 2. titanium particles were examined by scanning electron and the size was determined by semi-automated image analysis. The 3-5 th gereration of human osteoblast were cultured in medium with different concentration of particulates titanium alloy (1mg/ml, 0.1mg/ml, 0.01mg/ml). Cell growth and proliferation was detected by MTT method after 2、4、6 days that particles were added into medium and ALP activity was measured by kit after 4、7、10 days respectively. 3. With above same methods,the 3-5th generation of human osteoblasts were cultured for 3、6、9days after different concentration of particulates titanium alloy (1mg/ml, 0.1mg/ml, 0.01mg/ml) were added into the medium and OPG gene expression was quantified by RT-PCR.

1、取人胚胎颅骨骨膜,采有用酶消化法和组织培养法获取成骨细胞体外培养并传代,观察细胞形态,生物特点及成骨特性,并绘制生长曲线同时碱性磷酸酶染色鉴定成骨细胞以及比较冻存前3-5 代与冻存后成骨细胞的特点。2、电镜下观察钛合金颗粒的形态并测量其粒径,将不同浓度的钛合金颗粒(1mg/ml,0.1mg/ml,0.01mg/ml)与成骨细胞共同培养,分别于第2、4、6 天用MTT 法测量细胞增殖情况及4、7、10天用试剂盒检测碱性磷酸酶活性。3、分别将不同浓度的钛合金颗粒(1mg/ml,0.1mg/ml,0.01mg/ml)与成骨细胞基因培养3、6、9 天用RT-PCR 方法半定量测定骨保护素基因mRNA 的表达。

As the density of Al and Cu was quite difference,it was apt to delaminate and restrain the process of alloy by wet milling.The case was improved when dry milling,though it would be some reunite with the time of ball-milling prolonging.(2)The best technique parameters of high energy ball milling to prepare metastable powders of Cu-Al alloy were;the addition of Al powders was 1% in quality,the powders of Cu-Al were completely alloyed after high energy ball milling for 20 h.

1提出采用高能球磨制备Cu-Al合金粉的有效方法,认为由于Cu和Al的密度相差比较大,采用以液态酒精为过程控制剂的湿磨时,容易发生分层,抑制了合金化,采用干磨时,以硬脂酸为过程控制剂,虽然随球磨时间的延长会发生轻微的团聚,但能达到良好的合金化效果。

It's found that th e activation of alloy was improved with increasing the concentration,temperature and immersing time of alkaline solution,the reason is that the Zr-rich surface of alloy was conversed to Nirich surface because of the strong erodent action of alkaline solution,this catalyzes ...

实验发现:储氢合金电极的活化性能随碱液浓度增大、温度升高以及浸泡时间的延长得到改善,主要由于KOH的强腐蚀性使合金表面由富Zr层转化为富Ni层,为氢的吸附离解起到催化作用,总结出最佳KOH处理液的实验参数:6mol/L、80℃、浸泡 2 4h ,在此条件下合金电极循环两周即达最大放电容量。

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