合成的

The azo derivatives were hydrolyzed on the condition of alky to get end products. The structures of azo derivatives of 4-ASA and intermediate products were characterized by melting point, TLC, MS, FT-IR, 1H-NMR and 13C-NMR spectra properties in details.

本课题探索了一条4-ASA偶氮化合物的多步合成工艺，得到了目标产物三个，对合成的目标产物和中间产物用熔点、薄层色谱法、MS、FT-IR、1H-NMR和13C-NMR进行了详细的表征，确定了它们的结构。

On the other hand, the amidase activity and esterase activity of papain were determined at different temperatures.

一方面，通过比较常温溶液体系、低温溶液体系以及低温固液体系中的肽合成产率，发现低温和固液共存是动力学控制肽键合成的两个有利因素：另一方面，通过对木瓜蛋白酶催化水解动力学的研究，分别测定了该酶在不同温度下的酯酶活性和酰胺酶活性。

CA-CTSs including N,O-carboxymethyl chitosan,N,O-1-carboxyethyl chitosan (N,O-1-CEC),N,O-2-carboxyethyl chltosan(N,O-2-CEC),N-carboxymethyl chitosan and N-1-carboxyethyl chitosan(N-1-CEC) are quaternized using active quaternary salts prepared in laboratory.5 series including 25 kinds amphoteric chitosans characterized with polymeric ampholyte,in which 24 kinds are synthesized firstly,are obtained, 2-Hydroxypropyl dimethylbenzyl ammonium N,O-(1-carboxyethyl) chitosan chloride (GDMBA-N,O-1-CEC) is hydrolyzed into serial low molecular weight GDMBA-N, O-1-CEC with acid as catalyst and microwave as assistant instrumentality innovately.

以合成的活性季铵盐改性了N，O-羧甲基壳聚糖、N，O-1-羧乙基壳聚糖(N，O-1-CEC)、N，O-2-羧乙基壳聚糖(N，O-2-CEC)、N-羧甲基壳聚糖和N-1-羧乙基壳聚糖(N-1-CEC)等羧烷基壳聚糖，得到5个系列25种具有两性高分子电解质特征的新季铵化羧烷基壳聚糖，其中24种为首次合成；创新提出以微波辅助酸催化的方法催化2-羟丙基二甲基苄基-N，O-(1-羧乙基)壳聚糖氯化铵(GDMBA-N，O-1-CEC)水解，得到了低分子量的GDMBA-N，O-1-CEC。

The structures and composition of the Y-shaped copolymer were well characterized by means of NMR, IR and GPC measurement.

然后用合成的引发剂引发了GMA的ATRP反应合成了P(TCE-10-HD)-b-PGMA，并且证明这种聚合方法是简便可行的。

Dehydroepiandrosterone and its sulphate DHEAS are the most abundant circulating sex steroid hormones in women, providing a large precursor reservoir for the intracellular production of androgens and oestrogens in non-reproductive tissues.

脱氢表雄酮和硫酸盐脱氢表雄酮是女性体内最丰富的循环性类固醇激素，作为雄激素和雌激素合成的前提储存，用于在非生殖组织的胞内合成雄激素和雌激素。

Dehydroepiandrosterone and its sulphate DHEAS are the most abundant circulating sex steroid hormones in women, proiding a large precursor reseroir for the intracellular production of androgens and oestrogens in non-reproductie tissues.

脱氢表雄酮和硫酸盐脱氢表雄酮是女性体内最丰富的循环性类固醇激素，作为雄激素和雌激素合成的前提储存，用于在非生殖组织的胞内合成雄激素和雌激素。

It occurs at the carbon-carbon triple bond in a highl regioselective manner. Therefore, the reaction not only expanded the synthetic applications of Diels-Alder reaction but also provided a facile and efficient synthetic procedure for the synthesis of 4-functionalized quinoline derivatives.

上述反应实现不仅扩展了Diles-Alder反应在有机合成的应用，同时喹啉类化合物4-位上官能化的二硫缩烯酮基团也为其4-位取代打开了大门，为合成各种4-取代喹啉类化合物开辟了一个简洁高效的方法。

"Bio2 is a synthetic ecosystem, but so is California by now," said Burgess.

&生物圈二号是一种合成的生态系统，而现在的加利福尼亚也是一种合成的生态系统。&

"Bio2 is a synthetic ecosystem, but so is California by now," said Burgess.

&生物圈2号是一种人工合成的生态系统，而现在的加利福尼亚也是一种合成的生态系统。&

The methods of IR and others were carried on in order toverify the structural formula of XN. The validation of analytical procedures wasconducted according to quality standard of XN in supplement of ChinesePharmacopoeia in 2002. The results show that the structural formula of XN isright and XN can be analysed in accordance with the quality specification of ChP.The results of three lots repeat tests show that the optimal process for XN wasrepeated excellently and quality of products is stable and controllable.

所合成的烟酸占替诺经红外分光光度法等波谱测定，证明其结构正确；经检验方法学验证，确证该产品适用于按《中国药典》质量标准检验；经三批次重复验证试验，结果表明优选的烟酸占替诺合成工艺重现性好，所得产品质量可控，收率为91.1%，接近文献报道的最高收率。

In the negative and interrogative forms, of course, this is identical to the non-emphatic forms.

。但是，在否定句或疑问句里，这种带有"do"的方法表达的效果却没有什么强调的意思。

Go down on one's knees;kneel down

屈膝跪下。。。下跪祈祷