合成物

In a DMF solution of CuCl〓-ethanolamine-acetic acid (1: 2: 2), 27 formed a highly oxidized heterocyclic compound 2-hydroxymethyl-naphtho [1, 2-a] oxazole (30) by the carbon-nitrogen coupling and carbon-oxygen coupling with the ligand of ethanolamine, which brings a chance to develop a novel approach to this heterocyclic compound via one-pot reaction of phenols under mild condition.

在氯化铜—乙醇胺—乙酸（1：2：2）的DMF溶液中，27与配体乙醇胺发生碳氮偶合与碳氧偶合，生成深度氧化的杂环化合物：2-羟甲基-萘并[1，2-a]〓唑（30）。这可望为酚类一锅化直接转化为30及其类似物提供一种简便的新合成路线。

Methods K-ras gene point mutation and its style at codon 12 of Patu 8988 cell were detected by using PCR-SSP and sequence analysis.

方法顺序特异引物聚合酶链反应法和基因测序检测Patu8988细胞K-ras点突变形式，根据点突变形式设计并合成硫代反义寡核苷酸（K-ras mutation ASODN）作用Patu 8988，通过噻唑蓝比色法检测细胞生长情况；流式细胞术检测K-ras蛋白表达和细胞凋亡；逆转录-聚合酶链反应检测K-ras mRNA表达水平；以Patu8988细胞建立裸鼠胰腺癌模型观察K-ras mutation ASODN在体内的抗肿瘤效果。

Next, the relaxation of TAPP-Co-NO was investigated on isolated aorta pectoralis circle in the rabbit.

合成并结构表征 meso -5，10，15，20-四钴卟啉-NO配合物作为NO供体。

Hexachlorocyclophosphazene was prepared using phosphorous pentachloride and ammonium chloride as raw material, hccp was mixed with Montmorillonite which aimed to decrease MMT.'s hydrophilicity. Solid state reserve cell of Mg│reformed MMT.│polymer gel containing water│graphite was assembled, and cell performance was tested. XRD and IR results show: When mass percentage lower than 9.1%, hccp mixed with MMT to form homophase, hccp phase was observed in the mixture when percentage higher than 9.1%, for hccp specific diffraction peak appears in XRD data, and 1220cm-1 which was assigned to P=N double bond 's expand vibration appears in IR data.

合成了六氯环三磷腈，并用六氯环三磷腈与蒙脱石混合对其改性，期望能减小蒙脱石的吸水性能；组装电池Mg |改性蒙脱石|含水凝胶|石墨片，并测试电池的性能。X射线粉末衍射数据和红外光谱数据表明：蒙脱石容纳六氯环三磷腈的质量分数在4.8%-9.1%之间，可与蒙脱石形成单一物相，但混合质量分数大于9.1%时，改性蒙脱石出现六氯环三磷腈的特征衍射峰，和1220 cm-1的六氯环三磷腈P=N双键的特征伸缩振动峰，证明为蒙脱石与六氯环三磷腈的两相混合。

The aim of this thesis is to prepare rutile TiO2 nanorods under the hydrothermal condition and to investigate the correlation between the preparation parameters and the photocatalytic activity of as-prepared TiO2 samples. The initial sols for TiO2 were prepared by the hydrolysis and condensation of Ti precursor, titanium n-butoxide 〔Ti4, TNB〕 in DI-water with hydrogen chloride as a peptizer.

中文摘要本研究的主要目的是制备以水热法制备金红石相二氧化钛奈米棒并探讨其制备条件与光催化活性的相关性，以四丁基氧化钛为前驱物，在盐酸的催化下，经由水热处理来合成金红石相的二氧化钛奈米粒，并藉由XRD鉴定其结晶相，TEM来观察其外观形貌及其颗粒大小，氮气吸附法来分析其比表面积。

These products include sodium percarbonate, percarbamide, 4Na 2SO 4·2H 2O 2·NaCl adduct, tertiary amine oxides, hydrazine hydrate, dihydroxy benzene, quaternary ammonium salt hydrogen peroxide and methylethyl ketone oxime.

介绍了近期国外过氧化氢在部分化学品合成中应用研究新进展，产品包括过碳酸钠、过碳酰胺、4Na2 SO4·2H2 O2 ·NaCl加合物、叔胺氧化物、水合肼、二羟基苯、季铵盐过氧化氢和甲乙酮肟。

Inorganic chemistry ; hydrogen peroxide ; review ; sodium percarbonate ; percarbamide ; 4Na 2SO 4·2H 2O 2·NaCl adduct ; tertiary amine oxides ; hydrazine hydrate ; dihydroxy benzene ; quaternary ammonium salts hydrogen peroxide ; methylethyl ketone oxim

无机化学；过氧化氢；综述；过碳酸钠；过碳酰胺； 4Na2SO4·2H2O2·NaCl加合物；叔胺氧化物；水合肼；二羟基苯；季铵盐过氧化氢；甲乙酮肟；合成；催化剂；质量；安定性；收率

Four new solid complexes of rare earth with phenoxyacetic acid and 1,10 phenanthroline were synthesized ,and their composition,solubility and molar conductance were studied.

合成了钕、钇、镝、镥等稀土·苯氧乙酸·邻菲罗啉三元配合物。用化学分析法研究了它们的组成以及它们在不同溶剂中的溶解性能和摩尔电导等物理性质。

Two solid complexes of terbium with phenylacetic acid(L1) and phenyl-hydroxylacetic acid(L2) were synthesized by solid state reaction at low temperature,and the complexes were characterized by chemical analysis.

以两种不同结构的羧酸苯乙酸和苯基羟基乙酸与氯化铽为原料，采用低温固相反应合成了两种羧酸铽配合物。

Four series and sixteen solid complexes of rare earth chloride with 1-naphthoic acid (L_1),benzoic acid (L_2),phenylacetic acid (L_3) and Mandelic acid (L_4) have been synthesized by method of solid state reaction at low temperature,and then these complexes were characterized by chemical analysis methods.

本文采用低温固相合成法，以稀土氯化物、1—萘甲酸(HL_1)、苯甲酸(HL_2)、苯乙酸(HL_3)、苯羟乙酸(HL_4)为原料，以六次甲基四胺为质子受体，合成并表征了四个系列十六种固态配合物。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失