合成物

Numbers of secretory granules, oplasmic reticulums, mitochondrias in ACTH cells all changed distinctly. GTH cytoplast were full of big and small, high density electron secretory granules.STH cells were in activity synthesis and secretion, secretory granules were from fusion to release. TSH cells cytoplast evacuated secretory granules, electron density decreased and vacuofes appeared.

ACTH细胞分泌物颗粒数量、内质网及线粒体均发生明显变化；GTH细胞胞质中充满电子密度较高的大、小两种分泌颗粒；STH细胞处于活跃的合成和分泌状态，分泌颗粒呈现出由融合到释放的状态；TSH细胞胞质中分泌颗粒排空，且电子密度降低，出现大空泡。

The original crystal configuration of KGM was destroyed, and the molecular structure was disordered. The glass transition temperature T(subscript g of TKGM was only 13.14℃, and there's an obvious melting decalescence peak at 102℃, the difference between decomposed temperature and melting temperature is above 200℃. This means that TKGM has a good thermoplasticization property.

结果表明：合成了KGM和乙酸乙烯酯、丙烯酸甲酯的接枝共聚物；KGM原有的结晶结构被破坏，分子结构呈现无序化；玻璃化转变温度T(下标 g仅为13.14℃，且在102.5℃处有明显的熔融吸热峰，分解和熔融温差达200℃以上，具有较好的热塑加工性能。

A dominant B2CN crystal with orthorhombic structure was synthesized using deliquescent Ca3B2N4 catalyst by high pressure and high temperature. This crystal is a white photoluminescence material with blue-violet luminescence characteristic.

采用乱层石墨结构B2CN为前驱物，在高温高压下获得了六方B2CN晶体；采用Ca3B2N4触媒；在压力为3~6 GPa；温度为800~1600 ℃范围内测定了立方B(CxN1-x)的P-T相图；合成出了立方B(CxN1-x)(x=0.1~0.4)化合物。

Seeking secondary metabolites with biological activity to the harmful organisms from plants, after separation, depuration or taking as the template to the new artificial synthetic pesticide has become the classic of the contemporary pesticide research.

从植物中寻找对有害生物有生物活性的次生代谢物，经分离、提纯或作为人工合成新农药品种的模板已成为当代农药研究的经典。

All the compounds are characterized by IR and elemental analysis.we design and prepare a bipyridinium supramolecular compound and six coordination compounds, which are also characterized by IR, elemental analysis and X-ray structure analysis. According to X-ray structure analysis, hydrogen bonds and n-n stocking interactions participate in the architecture of three-dimensional framework [H2L1 (NO3)2 (H2O)2]n; one-dimensional zigzag coordination polymer [Hgl21.5CH3OH]n; binuclear metallamacrocycle (HgI2L2)2 3H2O; helical double-stranded one-dimensional coordination polymer [Co2(L2)2-2CH3OH]n; double-stranded one-dimensional coordination polymer [Co2(L3)2-CH3OH-CH3CN]n; and three-dimensional compound [Cu(C5H4NCOO)2(H2O)2]-H2O with hydrogen bonds, three-dimensional coordination polymer {[Cd(C5H6NCOO)2H2O]-DMF}n, which are indirectly obtained from the precursor ligand L3 through metal ion induced the hydrolysis of diamide and self-assembled with the hydrolyzate.

我们首次合成了一个双吡啶鎓超分子化合物和六个过渡金属配合物，并通过IR谱，元素分析和X-ray晶体衍射分析对它们进行了表征。X-ray晶体结构分析表明：超分子化合物[H_2L1·(NO_3)_2·(H_2O)_2]_n是由多种氢键和芳香环间的π-π堆积作用构建的三维无限结构；[HgI_2(L1)·1.5CH_3OH]_n是一维锯齿状配位聚合物；(HgI_2L2)_2·3H_2O是双核金属大环化合物；[Co_2(L2)_2·2CH_3OH]_n是具有一维双螺旋结构的配位聚合物；[Co_2(L3)_2·CH_3OH·CH_3CN]_n为一维双链结构的配位聚合物；以及由非直线形配体L3在金属离子Cu和Cd的诱导作用下发生水解，并且金属离子与水解产物——异烟酸根离子自组装，形成了三维氢键超分子化合物[Cu(C_5H_4NCOO)_2(H_2O)_2]·H_2O和三维配位聚合物{[Cd(C_5H_6NCOO)_2H_2O]·DMF}_n。

A new type of difunctional initiator (benzyl dibromide, ethyl dibromoacetate) was proposed in this paper and used to synthesize poly based triblock copolymers such as PSt-PBA-PSt, PMMA-PBA-PMMA.

本论文提出一种新型ATRP双官能团引发剂(如α，α-二溴化苄、α，α-二溴乙酸乙酯)，并用聚合反应速度法、GPC法、核磁分析法进行双官能度的验证，并通过两步聚合合成以聚丙烯酸酯为中间嵌段、苯乙烯或甲基丙烯酸甲酯为两端嵌段的ABA型三嵌段共聚物。

Two bispyrazolylimine nickel complexes [bis-N-(phenyl-1,3,5-dimethylpyrazolylmethylene) phenylimine nickel dibromide] (Cat.1) and [bis-4-methoxy-N-(phenyl-1,3,5-dimethylpyrazolylmethylene) phenylimine nickel dibromide] (Cat.2) were synthesized.

合成了两种双吡唑亚胺镍配合物：双－N-（苯基－1-3，5-二甲基吡唑基亚甲基）苯基亚胺二溴化镍Cat.1）和双－4-甲氧基－N-（苯基－1-3，5-二甲基吡唑基亚甲基）苯基亚胺二溴化镍

We synthesized the dienophile 62 from L-malic acid and then heated together with diene 73 afforded the cycloaddition product.

我们由L-苹果酸出发合成了亲双烯体62，并实现了底物诱导的Diels-Alder反应。

The polymer carriers,the immobilization of rare earth compounds,the properties of polymer-supported rare earth metal complex es and their catalytic characteristics in the polymerization of diene was reviewed with 25 references.

对聚合物载体的合成、稀土金属化合物的固定和聚合物载体－稀土金属络合物的性质及其催化双烯烃聚合的特征进行了论述。

It was found that the synthesized polymer of BDME can dissolve the low boiling point impregnant system which could settle the problem both the diffluence of BMI and the consistence of BMI and EP.

结果表明：合成的BDME共聚物可溶于低沸点溶剂体系，解决了双马来酰亚胺聚合物的溶解以及与环氧树脂共混时的相容性问题。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。