合成物

According to literature methods, the benzoic acid nitrogen mustard and its rare earth complexes were prepared. The structures were characterized by element analyses, IR, UV-vis and EPR spectra.

参照文献方法合成了苯甲酸氮芥及其稀土配合物，并通过元素分析、红外、电子光谱及电子顺磁共振光谱对配合物进行了表征。

We have developed a technique of random-primed tritium labeled DNA extension on the pachytene bivalents of rice-field eels.

采用随机引物，在黄鳝二价体上建立了氚标记引物原位DNA合成技术，并详细探索了该技术的实验条件。

Three new ternary copper complexes: 3.5H2O(1)、 2H2O (2) sand 1.5H2O(3)(phen=1, 10-phenanthroline, tatp=1, 4, 8, 9-tetranitrogen, dppz =dipyrido [3,2-a; 2,3-c]phenazine, Gly-L-Val=Gly-L-Valine), were synthesized characterized by elemental analysis, molar conductivity, IR and UV-Vis spectroscopes.

本文合成了3个新的三元铜配合物：3.5H2O(1)、2H2O(2)和1.5H2O(3)［Gly-L-Val=甘缬二肽，Phen=l，10-邻菲咯琳，TATP=l，4，8，9-四氮三联苯，DPPZ=二吡啶并［3，2-a；2，3-c］吩嗪］。通过元素分析、红外光谱、紫外－可见光谱以及摩尔电导率测定对这些配合物进行了表征。

Under the protection of purified water-free, oxygen-free argon, using Schlenk technique, the rare rarth organometallic complexes containing piperonal dimethyl acetal and dicyclopentadienyl and involving silylene-bridged fluorenyl have been synthesized.

合成了含胡椒醛二甲基缩醛基和二茂基稀土金属有机配合物。采用Schlenk技术，在干燥纯氩气保护下进行。将溴代胡椒醛二甲基缩醛基锂盐与二茂基一氯稀土（Ln：Yb，Dy，Pr，La，Sm）反应，形成5个新的文献未曾报道的稀土金属有机配合物。

The bioligical activities of all complexes were tested by means of modified pyrogallol autoxidation . The results indicates that V-SOD mimics present limited fine biological activities. This work opens up a new path for syntheizing new SOD mimics and studying the relationship between structure and biological activity of the mimics compounds.

利用改进的邻苯三酚自氧化法测定了所合成配合物的生物活性，结果显示钒的模型配合物具有较好的活性，为拓展研究SOD模型化学奠定了基础，开阔了思路。

Based on the summary of latest research results, the structure features, the synthesis methods and the mechanism as high density recordable optical recording media of metal porphyrin complexes are described.

本文在总结近年来最新研究成果的基础上，阐述了金属卟啉配合物的结构特点、合成方法和作为高密度可录光盘存储介质的作用机理，讨论了影响卟啉配合物性质和光存储性能的主要因素，并对未来的发展趋势作了展望。

The effects of operation parameters on separation of fatty acid methyl ester from rapeseed oil deodorizer distillate by molecular distillation were investigated for further utilization of RODD. The results indicated that the recovery of FAME was 41 g/(100 mL) when pressure was 5.2 Pa, evaporating temperature was 120℃, feed temperature was 70℃, wiper rolling speed was 150 r/min, feed rate was 120 mL/h. The biodiesel was analyzed by GC-TOFMS.

为了实现脱臭馏出物的清洁加工，运用分子蒸馏技术分离菜籽油脱臭馏出物中合成的生物柴油，考察了分子蒸馏的操作参数对生物柴油回收率的影响，研究结果表明：当系统压力为5.3 Pa，蒸发面温度120℃，进料温度70℃，刮膜转速150 r/min，进料速率120 mL/h时，生物柴油回收率达到41 g/100 mL。

The effects of operation parameters on separation of fatty acid methyl ester from rapeseed oil deodorizer distillate by molecular distillation were investigated for further utilization of RODD.

为了实现脱臭馏出物的清洁加工，运用分子蒸馏技术分离菜籽油脱臭馏出物中合成的生物柴油，考察了分子蒸馏的操作参数对生物柴油回收率的影响，研究结果表明：当系统压力为5.3 Pa，蒸发面温度120℃，进料温度70℃，刮膜转速150 r/m in，进料速率120 mL/h时，生物柴油回收率达到41 g/100 mL。

The recent progress in the studies of saccharide -metal complex is reviewed. Especially their synthesis based on saccharide ligand and application is described.

综述了近年来糖－金属配合物的最新研究进展，重点从糖基配体的角度介绍了各类糖－金属配合物的合成与应用研究。

Six Co complexes have been synthesized and their structures were confirmed by IR, UV spectroscope.

3以L~2、L~3、L~4、L~5、L~7、L~8、L~9为配体分别合成了它们的Co配合物，并测定配体及其配合物的红外光谱及紫外光谱，对它们的物理性质进行了初步的研究。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失