合成地

AlCl3-MEIC was prepared by reacting 1-methylimidazolium and ethyl chloride ,and the best situation of synthesis was confirmed.

2应用正交实验法确定了合成1—甲基—3—乙基氯化咪唑这种有机盐的最佳反应条件，并成功地合成了这种有机盐。

The first total synthesis of 3, 7, 11-trimethyl-10-oxododecanoic acid 14,a new sesquiterpene isolated from Caulerpa recemosa have been completedthrough eight steps starting from geraniol in a 18.5% overall yield.

以香叶醇为原料，经八步反应首次完成了倍半萜3，7，11-三甲基- 10-氧代-十二碳酸14天然产物的全合成，并对关键中间体24进行官能团改造，便利地合成了全反式法呢醇12。

The high-power system including main circuit, the charging and discharging circuit of synthetic circuit test system, and the principle of charging and discharging for current supply using electrolytic capacitor is presented. At the aspect of circuit breaker control, the advanced permanent magnetic actuator is used and analyzed in this paper, including the precision computation and using in synthetic circuit. The trigger circuit of voltage supply is designed, and the intelligent control is used to trigger the igniting gap. And the integraph based Rogowski coil is designed and employed the intelligent detection of breaking current.

强电系统介绍了合成回路试验系统的主电路及其充放电电路，讲述了电流源采用电解电容器的充放电原理；断路器控制方面，采用当前比较先进的永磁操动机构，并对永磁机构的原理、精度计算和在合成回路中的应用做了详细地分析；设计并制作了电压源点火回路，对球隙点火进行智能控制；在智能检测开断电流方面，设计并制作了与Rogowski线圈相配合的积分器。

Virtually Erythromycin Oxime is the common intermediate of some novel antibiotics such as Clarithromycin, Azithromycin and Dirithromycin.

其中红霉素肟不仅是合成罗红霉素的中间体，也是合成克拉霉素、阿奇霉素、地红霉素等的通用中间体。

To an asymmetric synthesis of (1), we applied a type of Roush addition in the first step to introduce the C4 stereocenter, and then the chair substance -122 are readily transformed into the title compound -aphanorphine using the same route as to the racemic target molecular.

aphanorphine分子的不对称合成是在第一步通过对甲氧基苯乙醛（119）发生Roush反应引入手性，得到手性高烯丙醇-122，然后利用与合成外消旋目标分子相同的方法，光学纯化合物-122经一系列转化可得到光学纯中间体化合物139；化合物139发生分子内傅—克反应的过程中，由C4位手性立体特异地控制C1位手性的生成，从而解决-aphanorphine分子中的手性问题。

Organosilane protective reagents widely used in the organic synthesis,especially in the synthesis of medicine、 pesticide and savageness production.

有机硅保护剂广泛地应用于有机合成中，特别是在医药、农药和天然产物的合成中大量的应用。

The key steps involved Friedel-Crafts reaction of o-cresol and the Wittig reaction for construction the skeleton of amine moiety,at the same time, using the synthesis of E,(7S)-7-methoxytetradec-4-enoic acid in chapter 2,and Johnson-Clainsen rearrangement as a key step for construction the fatty acid part,the corresponding acid was prepared in 23%and 50%overall yield,respectively.

随后将手性不饱和脂肪酸和氨片段进行酰胺化反应构筑了malyngamide M的基本骨架，再将Z-烯氯转化为E-烯氯完成了目标分子的全合成，高立体选择性地构筑了末端烯氯结构，为制备其它含有类似烯氯结构的malyngamides探索出行之有效的合成路线。

Chromium species in organic chromium catalyst is determined with plasma emission spectrography.

已酸铬是乙烯齐聚合成1-己烯的主催化剂，通过它与助催化剂的络合反应可以高选择性地合成1-己烯。

The synthesized monomer and fluorescent polymers were characterized by the methods of nuclear magnetic resonance (~1H NMR), mass spectrography, fourier transform infrared spectroscopy, ultra-violet-visible spectra and differential scanning calorimetry, respectively.

采用核磁(~1H NMR)，质谱，红外光谱，差示扫描量热法，可见紫外分光光度仪和荧光光谱等方法对合成的荧光分子以及荧光聚合物的结构和性能做了表征，系统地研究了所合成的荧光聚合物的荧光性能。

Besides, the derivatives were synthesized successfully by the similar acid binding agent system, such as tris(4-nitrophenyl) thiophosphate, tris(4-toluene)thiophosphate. The derivative of maleic anhydride was synthesized by the simple method, and its yield was above 90%.

采用类似的缚酸剂体系成功地合成了硫代磷酸三(4-硝基苯)酯、硫代磷酸三(4-甲基苯)酯，并用简单的方法合成了硫代磷酸三(4-氨基苯)酯的马来酸酐衍生物——硫代磷酸三(4-马来酸氨基苯)酯，产率达90％以上。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失