合成地

A facile method is presented for synthesis of malonaldehyde dianil from propargyl alcohol by oxidizing using chromium trioxide and addition reaction with aniline.

以丙炔醇为原料，经三氧化铬氧化生成丙炔醛后，直接与苯胺反应简便地合成了β-苯胺基丙烯醛缩苯胺。

In consideration of the competition of reactions between acetic acid, chloroacetic acid, dichloroacetic acid andchlorine, a competition factor was introduced for the improvement of fitting accuracy between calculated and experimental value of concentration.

结果表明，加入&竞争因子&的平行-连串宏观动力学模型能准确地反映己酸光氯化合成三氯乙酸的反应动力学规律。

Studing on samarium diiodide promoted asymmetric intramolecular reducing coupling reactions, we have made the resolution of the racemic biaryl dials by using enantiomeric N-tert-butanesulfinamine as the resolving reagent successfully and thus obtained a series of axially chiral biaryl dials with high enantiomeric excess.

中文摘要在二碘化钐促进的分子内不对称还原偶联反应中，我们不仅对联芳基二醛底物的合成路线进行了优化，还发现N-叔丁基亚磺酰胺辅基可以作为手性试剂，成功地对联芳基骨架二醛化合物进行拆分，得到高对映体过量的轴手性二醛类化合物。

The Nazarov cyclization, a powerful tool for the construction of five-membered carbocycles from divinyl ketones and related compounds, has attracted increasing attention in recent years due to its wide applications in the synthesis of complex natural and unnatural products.

Nazarov环合反应是通过二烯酮类物质和类似化合物构建五元碳环的有效方法。由于该方法广泛地应用于复杂天然和非天然产物的合成，近年来引起人们的广泛关注。

N-Butyl stearate was synthesized in high yield by esterification of n- butyl alcohol with stearic acid in the presence of ammonium ferric sulfate dodecahydrate.

在十二水合硫酸铁铵存在下，正丁醇和硬脂酸发生酯化反应，高收率地合成了硬脂酸正丁酯。

The stronge interaction between EMimBF4 and nitrobenzene, and its intermediates yielded in the process of electroreduction caused the selective reaction.

通过控制电位，可以选择性地合成氧化偶氮苯和偶氮苯；在EMimBF4中，硝基苯和水的浓度变化对电化学行为产生较大影响。

In Granards' reactionof fluorinated β-ketophosphonium salts we found differentGranard reagents give different reaction mechanisms andPhMgBr realized the enolate reaction of fluorinatedβ-keto-phosphonium salts.

在研究含氟β-酮基鏻盐的β位亲核加成反应中，我们利用含氟α-烷氧基-β-酮基鏻盐与有机锂试剂的亲核加成反应一锅法高度立体选择性地合成了E式或Z式三氟甲基的烯醚类化合物。

A reasonable explanation supported by solubility experiments was proposed. Based on these results, equimolar CTAB-SDS was used in oxidations of toluene derivatives by potassium permanganate.

此外，作为模板的表面活性剂能有效地控制CaCO_3一系列晶化过程，很少有关于SDS-非离子表面活性剂复配体系在反胶束溶液中合成CaCO_3的研究。

Some methods aiming at the two problems have been researched. First, the optimal number of ATE site can be calculated based on a cost model of DAT-ATE. Second, the problem of test schedule which is equitant with two-dimensional Bin-Packing problem is presented. Then a TCG denotation satisfied with T-admissible rule is more convenient for combinational optimization. With Simulated annealing algorithm, better test scheduling results can be achieved; but there is no great optimization space because the efficiency of scheduling is greater than 90%. Third, A novel test compression method——Multi-capture testing is proposed to compress the stimuli. And the ATPG results show that MC achieves high compression ratio which is greater than 90% in some large-scale circuits. MISR, widely used in LBIST, is employed to compress the responses. The aliasing analysis demonstrates that the fault coverage reduction is little due to the existence of aliasing. Fourth, an improved TIC (called S-TIC) aiming at structured test is proposed based on ARM's TIC. A MC scheduling algorithm is proposed to compute the SoC test time and combine MC vectors to SoC test vectors. The scheduling results shows that test time is greatly reduced when using the proper scheduling priority.

首先，给出了低成本ATE的成本模型，根据此模型得到最低测试成本时系统级测试调度的基本参数——测试Site数；其次，本文将DAT-Scan方式的SoC测试调度等价为两维BP问题，为有效地求解该问题，将该BP问题表示为TCG图并通过模拟退火算法解决其求解过于复杂的问题，调度的结果表明该方法在测试时间上有一定改善，并指出DAT-Scan测试调度效率已经大于90％，进一步优化的空间较小；第三，本文尝试通过测试压缩来解决激励所需的测试带宽，提出了Multi-capture结构并解决了MC测试过程中的&矢量&退化问题，MC测试的ATPG结果表明其测试压缩率很高（大电路接近90％）；第四，在激励获得很高压缩比的情况下，测试响应也需压缩，本文采用LBIST中常用的MISR作为MC测试的响应压缩电路，理论分析和实验结果都证明了MC测试的别名对故障覆盖率影响较小（小于2％），并对两类别名的成因做了具体分析；第五，在MC测试及其响应压缩的基础上，本文改进了ARM公司的测试控制器TIC使之适合于MC测试，为了解决MC测试矢量合成问题，本文抽取了MC测试模型，通过固定优先级的MC测试调度模拟将MC矢量合成为ATE矢量，并模拟出了总的MC测试时间。

A fully ethoxy-terminated polymethylsilsesquioxane has been prepared via a dehydration ethanolysis reaction between absolute ethanol and an ordered ladder-like HO-Me-T, which improved long-term storage stability of HO-Me-T. Meanwhile, EtO-Me-T can still participate in the cross-linking reaction with hydroxy-terminated PDMS in the presence of catalyst.

利用含端羟基的LPS与无水乙醇之间的催化脱水反应合成了一种乙氧基为末端基团的活性梯形聚甲基倍半硅氧烷，有效地改善该类聚合物的长期稳定性；同时，该乙氧基封端聚合物仍然具有活性，可以代替常用的正硅酸乙酯与羟基硅油进行交联反应。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失