合成

The Applications of Samarium Diiodide and Ytterbium Trifluoromethethanesulfonate in Organic Synthesis, the Applications of Bis Carbonate in Sythesis of Chloroformates

论文标题：二磺化钐及三氟甲磺酸镱在有机合成中的应用，双碳酸酯在氯甲酸酯合成中的应用

This paper also describes the physical and chemical properties of zeolite MAP.

本文着重考察了影响合成MAP沸石的因素，确定了MAP沸石合成的最佳范围，并对其物理化学性质进行了表征。

Highly ordered mesoporous Zr-Ce-SBA-15 silica with hexagonal-platelet morphology was synthesized through a hydrothermal route by using pluronic P123 as a template, tetraethyl orthosilicate as a silica source, zirconyl chloride and cerous nitrate as a precursor. The main strategy of this method was to utilize the acidity self-generated from the hydrolysis of inorganic salts in the aqueous solutions, where no addition of mineral acids was necessary.

以P123为模板剂，正硅酸乙酯为硅源，氯化氧锆和硝酸亚铈为无机前驱盐，在不外加无机酸的条件下，利用无机前驱盐自身水解产生的弱酸性环境，通过水热合成路线一步合成了具有大的径轴比、短孔道、六方板状形貌的Zr-Ce-SBA-15介孔材料。

Zyme all reached the highest during filling middle stage 14days after flowering , and decreased

粉合成酶、淀粉粒结合态合成酶和Q酶均是在灌浆中期(花后14 d)活性最高。

Lots of new production technologies to enhance the competitive power of products have worked out in China's companies such as technologies for producing vitamin C manufactured via two-step zymosis; synthesizing chemically vitamin E with the domestically produced key intermediates linalool, isophytol and trimethylphenol; preparing vitamin B2 gained by genetically engineered bacterium fermentation, and commercialized production of vitamin H, etc.

我国企业研究出许多维生素生产新工艺，提高了产品的竞争力，开发的新工艺有两步发酵法生产维生素C，化学合成维生素E的关键中间体芳樟醇、异植物醇和三甲基苯酚等原料国产化，基因工程菌发酵生产维生素B2，维生素H的工业合成等。

The results indicated that the treatment of increasing top dressing N applying ratio could increase endogenous hormones zeatin riboside ZR(subscript S, isopentenyl adenosine contents and decrease abscise acid contents in flag leaves, and improve photosynthate synthesis, which could increase sucrose contents in flag leaves and supply aplenty of carbon sources for starch synthesis in grains.

结果表明，氮肥后移的处理旗叶中ZR、iPAS含量的增加及ABA含量的减少，有利于光合产物的合成；蔗糖含量较高，为籽粒合成淀粉提供了充足的碳源物质。

METHODS: Mono-6-O-tosyl-β-CD and mono-6-formyl-β-CD were synthesized separately. Silylatedβ-CD was loaded onto polymer chain of PVA by acetalization to produce PVA containingβ-CD linear high polymer.

分别合成单6-对甲基苯磺酰β-环糊精酯和单6-甲酰基β-环糊精，利用缩醛化反应将醛基化β-环糊精固载到聚乙烯醇大分子链上，合成出聚乙烯醇固载β-环糊精的线性环糊精高分子。

The synthesis of celery ketone from butyl aldehyde and ethyl acetoacetate was improved with higher yield by using solid superbase(K2O/γ-Al2O3) for the first time.

在正丁醛和乙酰乙酸乙酯为原料合成芹菜酮的合成过程中，对其催化方法进行改进。

Production technology of synthesis of allantoin are reviewed, including glyoxal oxidation, electrochemical synthesis, calcium glyoxylate synthesis, dichloroacetic acid synthesis, acetochloral method, and oxidative decarboxylation.

评述了乙二醛氧化法、电化学法、乙醛酸钙法、尿素三氯乙醛合成法、尿酸二氯乙酸法和尿酸氧化脱羧法等合成尿囊素的各种工艺。

In this paper, the synthesis ways and applications of 4,5-dimethyl-l,3-dioxolen -2-one were introduced. An appropriate way synthesizing DMDO from acetoin via acylation, cyclization and dehydrochlorination was selected. The influences of various process conditions on the reaction were studied in detail, and the optimum process conditions were obtained by single factor experiments.

本文介绍了医药中间体4，5-二甲基-1，3-二氧杂环戊烯-2-酮的应用情况和合成路线，选择了适于工业化生产的工艺路线，即采用羟基丁酮为原料，经酰化、环合和脱氯化氢等步骤合成DMDO，并采用单因素试验法详细研究了各项工艺条件对反应结果的影响规律，确定了优化工艺条件。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失