合成

The second route firstly studied the tautomerization of the key intermediate from spirostane to cholestane 3-O-substituted kryptogenin,then formed a direct access used Zn/KI/HOAc reduction,which supplied a better synthetic method of MPD and other furostanol saponins.

第二条路线则首先研究了由螺甾到胆甾结构的关键中间体3-O-substituted kryptogenin的异构化现象，建立起以Zn/KI/HOAc还原反应直接合成该中间体的过程，这提供了一个更好的合成甲基原薯蓣皂苷及其他呋甾皂苷的方法。

The effects of feeding way of phosphorus pentoxide, ratio of C8H174OH to P2O5, reaction temperature and time on the synthesized isooctanol polyethenoxy ether phosphate were investigated. Its optimum synthesis technology conditions were as follows: feeding at batches while stirring tempestuously at 45℃, the ratio of nC8H17(EO4OH:n(P2O5)=2:1, esterifying at 70℃ for 4h, and add given volume of water at 70℃ for hydrolysing 2h.

研究五氧化磷的投料方式、反应物的用量比、反应温度和反应时间等因素对合成的异辛醇聚氧乙烯醚C8H17(EO4OH磷酸酯性能的影响，得到优化的异辛醇聚氧乙烯醚磷酸酯的合成工艺条件：在强烈搅拌下，分批投入P2O5，加料时的温度不超过45℃，nC8：H17(EO4OH：n(P2O5)=2：1，酯化温度为70℃，酯化时间为4h，在温度70℃时加入定量的水再水解2h。

It meets the need of tenseness of modern English.

复合形容词可由几个词合成，也可由短语、甚至句子合成。

Terpene synthases is one of most important regulatory enzymes in biosynthetic pathway of terpenoids, specially in regulation of terpene biodiversity.

萜类合成酶是萜烯生物合成途径中的重要调控酶之一，特别是在萜烯化合物多样性的调控上具有重要作用。

It has offered the information of the boiling points of the chemical compounds, and it is helpful to reutilize them after their separation by rectification. The results showed that the main compounds of the heavy cut of terpineol were longifolene and βcaryophyllene. They are from the raw material, terpinene oil.

松油醇的合成工艺方法主要有两种：一种是一步法，即松节油在酸催化作用下直接进行水合反应生成松油醇；另一种是二步法，即松节油首先在酸催化作用下水合成萜二醇，再经稀酸催化脱水生产松油醇。

ESCA results show that silica is coated on surface of the polymeric microspheres. SEM analysis reveals that when water was used as a solvent, uniform silica coating on the surface of organic microsphere can be obtained, and when the reactive time is 10 minutes, an uniform coating layer can be prepared. But when tetrachloroethylene was used as a reactive solvent, an inhomogeneous silica coating is found on the organic microspheres.

由化学分析电子光谱仪纵深分析可以得到，矽的前驱物是藉由披覆方式附著在有机微球表面；SEM分析发现以水为溶剂所合成出之披覆有二氧化矽的有机微球表面呈现均匀披覆效果，并且当反应时间为10min时表面均匀披覆效果最好；而以四氯乙烯为溶剂的系统所合成之微球则呈现不均匀披覆。

The results of the dissertation were concluded as follows:(1) It is essential to deposit a basic additive on the Mo-based catalysts for the synthesis of CH_3SH. The potassium-doped Mo-based catalysts exhibit the highest activity than that of the catalysts doped with the otherⅠA andⅡA group basic promoters. H_2-TPR and LRS characterizations suggest that the addition of a base leads to the transformation of octahedrally coordinated Mo to tetrahedrally coordinated Mo, thus leads to the split of low temperature reduction peaks. The interaction between the basic components and Mo lead to the formation of B-Mo interface phase, which are closely correlated with the formation of CH_3SH.(2) It has been found that Fe, Co, Ni and Te have evident promoting effects for the K-Mo/SiO_2 catalysts.

主要结果归纳如下：(1)在Mo基催化剂中，必须添加碱才具有可观的合成甲硫醇活性，在IA和IIA族元素中，K是最佳的碱促进剂，当K/Mo摩尔比为2，前驱体为K_2CO_3，采用共浸法制备的K-Mo催化剂活性最高。H_2-TPR和LRS表征显示，碱的加入导致表面八面体钼氧物种向四面体转化，催化剂的低温还原峰发生分裂，碱助剂与钼之间存在强相互作用形成了B-Mo"界面相"，该物种与合成甲硫醇密切相关。

In this thesis, synthetic process route for natrexone hydrochloride was studied from the laboratory aspect. The target compound, natrexone hydrochloride, was synthesized via preparing intermediate, methylnaltrexone, using thebaine as starting material.

本论文从试验方面研究了由蒂巴因出发，中间合成甲基纳曲酮中间体，最后制备盐酸纳曲酮的合成工艺路线。

The gas phase reaction is attributed to aluminium vaporizing and Fe〓O〓 decomposing to release oxygen at higher temperature of the thermite reaction.

自行设计了一套用于弯管一次合成的自动化设备，在国内外首次用SHS—重力法合成出φ108～325mm的整体内衬陶瓷弯管。

The chapter 3 focuses on the design and synthesis of new thiazole derivatives.

论文第四章是噻唑衍生物的固相合成，设计并开发了用组合化学方法合成噻唑衍生物的新方法。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失