合成

To improve the cyano reactivity, cyano-terminated PPENs were prepared by the end-capping reaction of PPEN-OL with CBN; benzonitrile terminated polys were also prepared by the polycondensation of excess 4,4'-oxydianiline with 1,2-dihydro-2-(4-carboxyphenyl)-4-[4-(4-carboxyphenoxyl)phenyl]-phthalazinone, followed by end-capping with CBA. The polymers synthesized exhibited good solubility in NMP, DMAc and DMF, and were crosslinked to afford phenyl-s-triazine-containing polymers under the similar conditions.

为提高氰基活性，以对氯苯腈为原料，对PPEN-OL进行封端，设计合成了含氰端基的聚芳醚腈；以含二氮杂萘酮联苯结构二酸单体与4，4'-二氨基二苯醚为原料，经Yamazaki膦酰化缩聚，并用对氰基苯甲酸进行封端，合成了含氰端基的聚芳醚酰胺。

Three ways leads to the synthesis of fenclorin, one way discussed here has 3 steps. Stepl :benzonitrile using as raw material goes though dry hydrogen chloride and becomes a-imino phenylmethyl ether after meet carbinol.

解草啶的合成主要有三条路线，本文选取合成路线是以苯甲腈为原料，经三步反应而成：1、苯甲腈在干燥的氯化氢通入，与甲醇形成亚氨基苯甲醚，通入氨气后置换甲氧基得到苯基脒盐酸盐(收率76.18%)。2、苯基脒盐酸盐在碱性条件下与丙二酸二乙酯环合而得嘧啶醇(收率84.39%)。3、嘧啶醇在三氯氧磷中羟基被氯化得到产品解草啶(收率87.29%)。

In this thesis, a series of benzamides and thioureas derivatives have been designed and prepared. By reasonable photoreaction conditions, a series of benzophenone and quinazoline compounds have been synthesized and structurally determined by NMR, MS and X-ray crystallography, respectively.

本文设计并合成了一系列苯甲酰胺和硫脲衍生物，通过选择合理的光反应条件，合成了一系列二苯甲酮和喹唑啉类化合物，应用核磁、质谱以及X-射线衍射技术对这些化合物的结构进行表征。

K-MnO/γ-Al2O3 and Cu/SiO2-C15.2 exhibited higher activity and selectivity for continuous hydrogenation of methyl benzoate to benzyl alcohol, the conversion of methyl benzoate was 89.2% and the selectivity of benzyl alcohol reached 84.1%.

以K-MnO/γ-Al2O3和Cu/SiO2为催化剂，利用固定床串联反应器实现了苯甲酸甲酯连续加氢合成无氯苯甲醇反应过程。K-MnO/γ-Al2O3和Cu/SiO2催化剂对于苯甲酸甲酯连续加氢合成苯甲醇具有良好的加氢活性，反应转化率可达89.2%，苯甲醇的选择性为84.1%。

The synthesis of benzyl chloroformate was studied.

对氯甲酸苄酯的合成进行了研究，介绍了其在多钛合成中的应用。

The result showed that benzyl erucate was synthetized and identified on its structure.

结果表明，采用微型合成法能够在60~70min合成芥酸苯甲酯。

Influence of the reaction condition for the yield of benzyl propionate was investigated. The traditional process was improved,and the reaction condition was optimized.

讨论了各种反应条件对合成丙酸苄酯的产率的影响，并对传统合成方法进行了改进。

With its unique molecular structure and outstanding bio-activities, qinghaosu has been proven as a worthy subject for in-depth studies with profound influence, not only for pharmacy, but also for phytochemistry, biogenetic synthesis and organic synthetic chemistry, chemical biology, etc. A great amount of work has been done in the last 30 years, with a lot more issues to be explored. Researchers need to seize the opportunity and make more achievements.

青蒿素以其独特的分子结构和杰出的生物活性显示出它是一有深远影响的研究对象，不仅对于药学，而且对于植物化学、生源合成、有机合成化学、化学生物学等学科都是一个可以大有作为的课题。30年来国内外已做了不少工作，但是还有更多的问题有待探索，机不可失，时不再来，期待着在綻放青蒿素的故土上结出更多的果实。

The progress of recent research on the lignin biosynthesis is introduced in this paper.

本文介绍了木质素生物合成途径，重点综述了调控木质素合成的手段及限速酶研究方面的最新进展，并提出存在的问题及展望。

In this paper,the progress,especially combining gene engineering of mutational biosynthesis is reviewed.

本文综述了突变生物合成技术在微生物药物领域的应用，特别是结合基因技术进行突变生物合成研究的新进展。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。