合成

After that, we introduced a new approach to synthesis of valiolamine, by a series of reaction to the carbon-carbon double bond from the substrate of valienamine, including epoxidation, hydrogenolysis and so on, and obtained the aim product finally.

在完成上述合成路线后，本文通过提出了一条全新的合成伏格列波糖重要中间体valiolamine的路线，即采用对底物valienamine中的碳-碳双键进行环氧化、氢解等一系列反应，成功地制备出所需的中间体，研究全新的合成伏格列波糖的路线，研究结果证实：该新路线已经被打通。

A series of the ligands including 6-bromo-piperonal dimethyl acetal, bis (9-fluorenyl) silane, and the dimer of indene have been synthesized and characterized.

合成了溴代胡椒醛二甲基缩醛基配体，合成了手性配体甲基苯基双芴基硅烷，合成了茚的二聚体，对其进行表征，培养单晶并测定了晶体结构。

It was known that pyridine and Triton-x100 had a bad effect on the cell growth and lycopene production were studied. The results indicated that pyridine and triton-x100 inhibited cell growth and lycopene synthesis;β-ionone increased cell growth and lycopene synthesis when the concentration was 0.05 ml/L, but when the concentration became higher, there would be a decrease on the lycopene output; span-20 increased cell growth and lycopene synthesis effectively when the concentration reached 2.0ml/L, and the lycopene yield became 2.4×10~(-2) mg/L which was 3-fold than control.

研究了培养基中加入不同浓度的小分子效应物吡啶、Triton-x100、Span-20、β-紫罗酮、异烟肼对番茄红素产量的提高作用，结果显示培养基中加入很低浓度的吡啶(0.1ml／L)就会对菌体产生很强的毒害作用；triton-x100对类胡萝卜素的合成也有很强的抑制作用，试验的浓度为0.2ml／L到5ml／L，结果发现它对菌体的生长和番茄红素的合成都有抑制作用；β-紫罗酮在浓度为0.05ml／L时有很小的促进作用，而浓度升高就有了比较强的抑制效果；span-20在液体培养基中的加量为2.0ml／L时，对番茄红素的合成有很强的促进效果，产量达到了2.4×10~(-2)mg／L，比原始菌株产量提高了2倍，而浓度进一步增大就产生了很强的抑制效果。

In the part of preparing HMT, the thesis did research on the preparing process of using isobutylene , 2,3-dimethyl-butene-l , 2,3-dimethyl-butene-2 as the materials respectively .

在中间体合成部分，本文分别对新己烯、2，3—二甲基—丁烯—1、2，3—二甲基—丁烯—2为原料合成HMT的工艺进行了研究，然后利用GC-MS对三种原料合成HMT的主要副产物分别进行了分析。

In the part of preparing HMT, the thesis did research on the preparing process of using isobutylene , 2,3-dimethyl-butene-l , 2,3-dimethyl-butene-2 as the materials respectively .Then using GC-MS , the main outgrowths in each reaction systems were analyzed.

在中间体合成部分，本文分别对新己烯、2，3—二甲基—丁烯—1、2，3—二甲基—丁烯—2为原料合成HMT的工艺进行了研究，然后利用GC-MS对三种原料合成HMT的主要副产物分别进行了分析。

ABSTRACT This paper demonstrated that supplementing valine, isoleucine and leucine in synthetic media had different effects on biosynthesis of multi-components of biotechspiramycin.

在合成培养基中分别添加缬氨酸、异亮氨酸与亮氨酸考察其对必特螺旋霉素生物合成的影响，证明Val、Ile及Leu对必特螺旋霉素多组分的合成有着不同的调节作用。

Recent developments in the synthesis,modification and catalytic properties of titanium silicalite molecular sieve are reviewed,including the developments in the synthesis of TS-1 with hydrothermal and isomorphous replacement methods,the modification of TS-1,as well as applications in catalytic oxidation and acid catalysis systems.

本文重点综述了近年来钛硅分子筛催化材料的合成、改性及其催化应用的研究进展，包括钛硅分子筛（TS-1）的水热合成方法和同晶取代合成法、改性、成型与负载以及钛硅分子筛催化氧化功能和酸催化功能的研究。

Firstly, through analysis for the synthetic mechanism of lactide and according to improve the condition of synthetic process the factors related were studied in detail.

首先，从改善合成丙交酯反应的条件入手，通过对丙交酯合成反应的机理分析，对反应过程中催化剂用量、种类、脱水温度、时间、压力、解聚温度、时间、压力等做了详细的研究，得出最佳的合成条件和工艺过程。

This paper reviewed the recent development of synthesis of propyl lactide,discussed the effects of different synthesis techniques and various catalyst system s for the preparation of propyi lactide on the yield and discussed the prospect of propyl lactide synthesis.

介绍了丙交酯合成研究的最新进展，比较了不同催化体系和不同合成工艺对丙交酯收率的影响，并对丙交酯合成的发展前景进行了展望。

It is evident that LiCoO〓 and LiMn〓O〓 fine powder with high phase purity can be obtained by this method in～10 minutes.

本文首次用微波合成法制备了LiCoO〓和LiMn〓O〓，并对合成工艺、微波合成机理以及材料的结构和电化学性能进行了研究。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失