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The direct incorporation of U-13C glucose was estimated by the intensity increase of m/z to F(F was parent fragment, and n was the carbon number in the fragment), while the total isotope incorporation from the added 13C could be calculated according to the abundance ratio increment summation from m/z (Fa+1) through (Fa was the fragment containing all original skeleton carbons, and T was the carbon number in the amino acid molecule). The 13C enrichment in the target compound was expressed as atom percentage excess, and that of D-amino acid needed to be corrected by the coefficient of hydrolysis-induced racemization. The 13C enrichment reflected the carbon turnover velocity of individual amino acid enantiomers, and was powerful to investigate the dynamics of soil amino acids.

外加葡萄糖直接合成氨基酸的比例可利用质谱碎片的相对强度变化来评价(n为质谱碎片F中含有的碳原子数目);而源于葡萄糖的13C同位素在氨基酸分子中的富集程度是所有同位素峰相对强度变化的总和。13C在目标化合物中的富集比例用原子百分超评价,D氨-基酸的APE还需进一步利用水解诱导的外消旋化系数校正。13C在目标化合物中的富集程度可反映各氨基酸手性异构体的碳循环速率大小,是研究土壤氨基酸动态变化的有力工具。

Alternatiely, the induction of anergy results in markedly less S6 kinase 1 Thr(421)/Ser(424) phosphorylation and CD71 surface expression.

换之,无能可导致明显地S6激酶1在421位苏氨酸/424位丝氨酸磷酸化和CD71胞膜表达的减少。

In the asymmetric hydrogenation of ethyl pyruvate catalyzed by 0 5% Rh/PVP TiO 2, the chiral modifier cinchonidine not only induces the enantioselectivity, but also accelerates the reaction rate greatly.

研究了辛可尼定作手性修饰剂修饰的负载型纳米铑簇合物催化剂(0 5 %Rh/PVP TiO2 )催化丙酮酸乙酯不对称氢化反应,在该反应中手性修饰剂辛可尼定不仅具有对产物生成的手性诱导作用,而且对反应具有明显加速作用;在优化反应条件后,反应的TOF和对映选择性分别可以达到 5 8 0min-1和

A new spectrophotometric method for the determination of chromium has been developed. In HCl medium, the chromium oxidizes hydroxylammonium chloride to form nitrite, which produces a pink azo dye when reacting with p-aminobenzene sulfonic acid and α-naphthylamine.

基于铬在稀盐酸介质中氧化盐酸羟胺产生亚硝酸根,而亚硝酸根与对氨基苯磺酸重氮化后可与α-萘胺偶联产生粉红色偶氮染料,提出了分光光度法测定铬的新方法。

The existance of vesicles was demonstrated by negatively staining TEM, freeze-fracture TEM, bromphenol blue entrapment, and quasi-elastic lightscattering experiments.

应用电镜(负染色制样和冰冻复型制样)、凝胶色谱、DSC、激光光散射等手段,证实了十一烯酸钠与十烷基三甲基溴化铵的混合溶液,在摩尔组成比α=9∶1--1∶9时经超声皆可制得单室囊泡。

The diastereo-selective lactones 57~58 was obtained by the polyfluoroalkyl -lactonization of S--2-methyl-4-pentenoic acid under the reaction conditions mentioned above.

以S--2-甲基-4-戊烯酸进行上述内酯化反应,可得到具有立体选择性的产物57a,57b,58a,58b。

The optimal conditions were as follows: molar ratio of lauric acid to phytosterols 1.4:1, reaction temperature 120℃, SDS 1.5% and reaction time 4 hours. Under this condition, the yield of esterification reached 87.9%. After three steps of purification the content of phytosterol ester is about 93.1%. The product was determined as phytosterol laurate with FT-IR.

在酸醇摩尔比1.4:1,反应温度120℃,SDS用量1.5%反应时间4h的最优条件下植物甾醇酯化率可达到87.9%;反应所得的植物甾醇酯粗产品经3步提纯后纯度可达93.1%;对提纯过的产品进行红外光谱分析确定反应产物为植物甾醇酯。

Ceramic bearings can produce oxidation-ho, silicon carbide, silicon nitride and so on, diameter from 3mm-50mm, precision Machinable P0, P6, P5 level; its performance characteristics are: high temperature, oil-free self-lubricating, acid, alkali and salt corrosion , wear resistance, low noise, insulating diamagnetic, since high-speed operation; metal nano-ceramic bearing its production process for a new generation of high content of nano-particles in the heat and pressure infiltration of metal surface is activated to fill the cracks and pits the metal so that 3-5 micron metal surface is more smooth solid surface, greatly reduce the friction, improve Chennai base metals, and greatly increased the life span of bearings, and its characteristics are: long life (as an ordinary stainless steel bearings 2 -- 10-fold), low noise (as an ordinary stainless steel bearings, 70%), wear-resisting, acid, alkali, salt corrosion, high temperature, load large; ceramic bearing and metal nano-ceramic bearing design and development to meet the needs of the market for high-speed, low - noise, high load, the demand for corrosion-resistant; Machinery Production Department to produce aircraft rod end joint bearing, linear guide bearings, the fuel tank of earrings, plastic bearing, non-standard side bearing components, glass door hardware, such as high-precision control products; and provide CNC machining.

陶瓷轴承可生产氧化镐、碳化硅、氮化硅等,内径从3mm-50mm,精度可加工P0、P6、P5级;其性能特点为:耐高温、无油自润滑、耐酸、碱、盐腐蚀、耐磨、低噪音、绝缘抗磁、起高速运转;金属纳米陶瓷轴承其生产工艺为新一代的高含量纳米级微粒在热和压力的作用下被激活渗入金属表面,填补金属缝隙和凹坑,使金属表面3-5微米表面更光滑坚固,大大降低其摩擦力,提高金属的奈酸碱性,并大大提高了轴承的寿命,其特性为:长寿命(为普通不锈钢轴承的2-10倍)、低噪音(为普通不锈钢轴承的70%)、耐磨、耐酸、碱、盐腐蚀、耐高温、负载大;陶瓷轴承与金属纳米陶瓷轴承的设计开发以满足市场对高转速、低噪音、高负载、耐腐蚀的需求;机械生产部以生产机杆端关节轴承、直线导轨轴承、油缸耳环、塑料轴承、非标端轴承零部件、玻璃门控五金等高精度产品;并对外提供数控加工。

Base played a crucial role in this reaction: in the Pd2/L1 catalyzed α-arylation of ethyl malonate, K3PO4 is the base of choice; in the α-arylation of ethyl acetoacetate, K2CO3 is the most effective base.

在这类催化反应中,碱的选择具有重要的影响:以K3PO4为碱, Pd2/L1催化体系在丙二酸二乙酯的α-芳基化中,富电子溴代芳烃显示较好的活性; Pd2/L1催化的乙酰乙酸乙酯α-芳基化时,以 K2CO3为碱,催化体系显示较好的活性,这个催化体系可控制反应得到α-芳基乙酰乙酸乙酯,而不是脱乙酰基的产物。

Base played a crucial role in this reaction: in the Pd2/L1 catalyzed α-arylation of ethy malonate, K3PO4 is the base of choice; in the α-arylation of ethyl acetoacetate, K2CO3 is the most effectiv base.

在这类催化反应中,碱的选择具有重要的影响:以K3PO4为碱,Pd2/L1催化体系在丙二酸二乙酯的α-芳基化中,富电子溴代芳烃显示较好的活性;Pd2/L1催化的乙酰乙酸乙酯α-芳基化时,以K2CO3为碱,催化体系显示较好的活性,这个催化体系可控制反应得到α-芳基乙酰乙酸乙酯,而不是脱乙酰基的产物。

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For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降,而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

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Lao Qiu is the Chairman of China Qiuyang Translation Group and the head master of the Confucius School. He has committed himself to the research and promotion of the classics of China.

老秋先生为中国秋阳翻译集团的董事长和孔子商学院的院长,致力于国学的研究和推广。