可酸化的

The results show that a MgSnO3·H2O conversion film is formed by treatment in the stannate solution at 90℃, and the immersion test and potentiodynamic polarization show that the corrosion resistance of the AZ91D alloy is improved to some extent.

结果表明：锡酸盐转化处理后合金表面形成了以MgSnO3·H2O为主要成分的转化膜，可对合金起到一定的防护作用；转化膜由细小的球形颗粒密积而成，颗粒之间存在间隙，它可以为化学镀镍的前处理过程提供良好的吸附条件；转化膜上的化学镀镍层组织致密、无缺陷， MgSnO3·H2O转化膜在镀镍层与基体之间起到过渡作用，镀层的磷含量达到9%，与基体结合良好；在3.5% NaCl (pH=7)溶液中的动电位极化测试表明，镀镍以后的合金在阳极极化过程中发生了明显的钝化，耐腐蚀性能进一步提高，对基体起到了较好的防护作用。

With the observation of the outward appearances, it can be known roughly that if the sample was added with adulterations. Since the beeswax dissolves in the benzene but the adulterations, such as gypsum, starch and so on do not, these can be determined. By the verification of acid value and alcohol dissolve ability, the acid or non acid added can be determined. By the change of saponification value, the ester or non ester added can be determined. By the carbonification degree in the concentrated sulphuric acid, the mineral wax, such as paraffin wax added can be determined.

通过样品外观的观察初步定性是否掺有杂质；利用纯蜂蜡在苯中溶解，而掺入的石膏、面粉和淀粉等杂质在苯中不溶而定量鉴定这类杂质；由酸值变化和乙醇溶解物的量，测定掺入的硬脂酸等酸性物质或其它的非酸性物质；由皂化值变化，定量测定掺入的动物脂等酯类物质或其它的非酯类物质；根据蜂蜡中的烃类在浓硫酸中可被炭化，加入的石蜡等矿物蜡不被炭化来测定此类掺杂物。

They suggested that radicals with a double bond 13 to the carbon bearing the peroxy groups (which can only arise from acids containing more than two double bonds) cyclize to form peroxides with five-membered rings.

他们认为连接过氧基的碳原子有一个双键的游离基(只有多于两个双键的酸可形成)环化形成五元环的过氧化物。

The results showed that pectinase activity can retained up to 95.2% when prepared with 4.0% sodium alginate, 0.20 % glutaric acid, 0.10 mol/L CaCl2, 0.50 mL pectinase. The recovery activity of the immobilized pectinase was more than 76% after repeated 10 times.

结果表明，以4.0%的海藻酸钠为载体、0.20%的戊二醛为交联剂、0.10mol/L的CaCl2为凝聚剂、用酶量为0.50mL时所得的固定化果胶酶活力保存率可达95.2%，回收使用10次以后，酶的活力回收率为76.1%。

TyPe II collagen induced arthritisln the rat ank1e joint andoVathumin as antigen induced arthritis WA in the rabbit knee joint wereestab1ish2 Qualitative evaluation of me in skin, muscle, synovium, cedilagearound joint and blood was performed by OMA3 The CIA rats were treated on day 7 after hind paw swelling and erythemaAnimals were injected intravenously with ase at a dose of 10mg/kg,tWenty minuots 1ater, one ankle of the rats random1y assigned was exPosedlaser irradiation at l00J/cm fOr l000 seconds, and another ankle wasM grouP wihout laser The other two groups is unmanipulatedcontrol group and untreated CIA group Bimaleolar ankle widthmeasuremellts were taken in all animals every tWo days using amicrometer The histopathology of the ank1e Joint was assessed at day 21after disease onset4 The pro1iferating cell nuclear antigen WCNA of CIA treated by PDT andthe HMME group without laser was doterdrined by immunohistochemiStry5 The AfA rabbits were treated on day 7 after knee swelling and erythemaThe theraPy invo1ved lntravenous injection of l0mg/kg HMME, fOl1owedby 20 minues period in dim light, and transdermal light treatment with\l00 J/cm2 fOr l000 seconds The inner sides of the treated Anees wereirradiated at first, and then the outer side did 24 hours later, the synovialtissue of the Anees joint were removed and in situ cel1 aPoptosis wasdetCCted With tednal deoxync1eotidyl transferase-mediated dUTP nickend labelingR6suIt8:l The pathologic changes of CIA and AIA include subsynovial inflammation,opovial hyPerplasia, pannus formation, cartilage and bone destructionresemble RA.2 The studies demonstrated that there are different uptake of HMME withinskin, muscle, synovium, cartilage and b1ood, and the synovium cou1draPidly uPtake more ase than skin and cartilage at the firSt 30 minuesaller intravenous injection of HMME3 The bimaleolar anke width had no different among PDT treated group,H group withollt 1aser and untreated CIA group But hlstologicalevaluation showed statiStical1y significallt reductions in synovialhyperplasia, pannus formation and cart1lage reosion, bone destruction andtotal score in PDT treated group4 Image analysis showed that the ratlo bforeen the areas of the coufltedobect to that of the entire area in PDTtreated grOup is lower than that in conirol group, but the integrated oPticaldensity had no different between the two groups5 Imape analysis showed that the ratio between the area of the countedobject to that of the e

治疗组在大鼠出现踝关节红肿后1周，炎症达到高峰时进行PDT治疗。随机治疗大鼠一侧的踝关节，另。2。一一侧作单纯HMME 对照。治疗方法是大鼠麻醉后尾静脉注入 HMME10ngkg，20分钟后踝关节照光，激光波长627.sum，功率密度 100mwcm'，照射时间1000秒，能量密度100）／。治疗后避光喂养72 小时。隔日一次测量大鼠的踝关节左右横径，治疗后两周取关节进行病理d 观察。 4。大鼠CIA模型用上述方法进行PDT治疗后，治疗组和单纯HMME 组用兔疫组化SP法检测石蜡切片的核增殖抗原。 5。兔AIA模型在关节炎出现第七天进行PDT治疗，随机治疗一侧膝关节，另一侧作自身对照。兔耳静脉注入I'arrainrelomg／Kg，20分钟后，膝关节用金蒸气激光照射，激光能量密度100）儿旷。24 ／J'时后取膝关节滑膜作病理检查，并用脱氧核昔酸末端转移酶介导的缺口末端标记法原位检测凋亡细胞。结果： 1。模型观察：CIA大鼠炎症高峰期滑膜下炎细胞浸润明显，滑膜细胞明显增殖，炎症达到高峰后二周，血管缀形成，并侵蚀和破坏软骨和骨， CIA模型病理改变与人类RA相似。兔AIA模型膝关节滑膜病理可见滑膜细胞增生，滑膜下炎细胞浸润，也与人类RA滑膜改变相似。 2。关节周围组织中光敏剂含量的测定结果表明，各组织对HMME 的吸收速度和吸收量不同，荧光值一时间曲线不同，滑膜组织比皮肤和软骨对 HMME的吸收多，在 2 0分钟时即有明显差异。 3.PDT对CIA模型的治疗结果表明：PDT治疗后关节炎组、单纯 HMME组和治疗组踝关节左右横径统计学检验差异没有显著性，但病理评分PDT治疗组滑膜增生、血管资形成及软骨破坏、骨破坏和总分比关节炎对照组和HMME对照组好，统计学检验差异有显著性。。3＿军医进修学院硕士学位论文中文摘要 4.PDT治疗组PCNA阳性细胞较对照组少，图像分析结果表明面密度（阳性染色的面积总和与统计视野面积的比值）治疗组小于对照组，统计学检验差异有显著性。。 5.PDT治疗组凋亡阳性细胞较对照组明显增多，图像分析结果单位视野内阳性细胞数和面密度PDT治疗组高于对照组，统计学检验差异有显著性。凋亡细胞核直径PDT治疗组较小，与对照组相比，统计学检验差异有显著性。结论：二。CIA、AIA的病理改变类似人类RA，可作为研究RA病因、发病机制、检查及治疗方法的模型。 2。各组织对HMME的吸收速度和吸收量不同，滑膜组织比皮。

The negatively charged sulfonic acid groups was readily introduced through the reaction of the terminal anhydride groups of the anhydride-terminated hyperbranched poly precursor with the amino groups of sulfanilic acid before chemical imidization.

研究表明，在聚合过程的聚酰胺酸阶段，采用过量的邻苯二甲酸酐或苯胺对超支化聚酰亚胺的端氨基或端酸酐基团进行的封端改性切实可行，改性反应可进行地相当彻底。

The methods of extracting and refining tellurium presently were mainly soda roasting,autoclaving in general basic solution,sulfating roasting,oxidative leaching in acid solution, solvent extraction ,emulsion liquid membrane,microbial method,electrorefining,vacuum distillation and zone melting etc.

目前分离提纯碲的方法主要有苏打粉焙烧法、碱性高压浸出法、硫酸化焙烧法、氧化酸浸法、萃取法、液膜法、微生物法、电解精炼法、真空蒸馏法、区熔精炼法等，其中电解精炼法得到的碲的纯度达到99.99%，真空蒸馏碲的纯度达到99.999%，区熔精炼碲的纯度可达99.999995%，本文综述了以上分离提纯碲的方法。

In fact, we had obtained polythiophene films with high quality in BF3 ethyl ether, a kind of solvated Lewis acid. The electric conductivity of the polythiophene film is a bout 100 Scm-1. and the tensile strength is as high as 140 MPa, which is forty percent higher than that of aluminum.

事实上，我们已经从一种Lewis酸催化下的低电位聚合体系—噻吩/三氟化硼乙醚溶液中得到了高质量的聚噻吩薄膜，在降低了的聚合电位下得到的聚合物具有优异的力学及电学性能：拉伸强度达140MPa(比金属铝高40%)，电导率则可达100Scm-1。

In fact, we had obtained polythiophene films with high quality in BF〓-ethyl ether, a kind of solvated Lewis acid. The electric conductivity of the polythiophene film is about 100Scm〓, and the tensile strength is as high as 140Mpa, which is forty percent higher than that of aluminum.

事实上，我们已经从一种Lewis酸催化下的低电位聚合体系-噻吩/三氟化硼乙醚溶液中得到了高质量的聚噻吩薄膜，在降低了的聚合电位下得到的聚合物具有优异的力学及电学性能：拉伸强度达140MPa（比金属铝高40％），电导率则可达100Scm〓。

This paper presents a description of the brief synthesis of hexanoic acid 2-ethyl ester by new methods and its application. It takes two steps and 4.5 h to complete the synthesis of it.

己酸二乙氨基乙醇酯(DA 6)由美国科学家于20世纪90年代初首先发现的一种新型植物生长调节剂，具有高活性，低毒无污染、可与其它农化物质兼容的特点，它的合成与应用研究正日益受到人们的重视[1～7]。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。