可酸化的

The process of preparing sterilizing granule capable of generating chorine dioxide in one package includes the following steps: preparing activating agent; mixing inorganic salt and nickel acetate, re-crystallization, sieving and deactivation; sieving and deactivating solid acid; mixing with inorganic salt; mixing sodium chlorite and cobaltous chloride, re-crystallization, sieving and deactivation; and mixing the activating agent with sodium chlorite.

一种可发生二氧化氯的一元包装消毒颗粒制备方法，其特征是制备活化剂：将无机盐加入醋酸镍，经过重结晶后，筛分、钝化处理；将固体酸进行筛分、钝化处理；然后与无机盐进行混合；在亚氯酸钠中加入氯化亚钴后，经过重结晶、筛分、钝化处理；将上述活化剂和亚氯酸钠均匀混合即成。

The quaternary ammonium salt of quinoline synthesized by alkyl halide and quinolin etc.,can be used as corrosion inhibiter during acidizing treatment of oil well when it is compounded with organic amine,suitable solvent and surfactant.

以烷基卤化物与喹啉等原料合成的喹啉季铵盐，当其与有机胺、适当溶剂、表面活性剂复配后，可作为油井酸化作业的酸化缓蚀剂。

Phytin was extracted with diluted hydrochloric acid, after precipitating the effluent and transforming the precipitate with sodium hydroxide, sodium phytate solution was produced.

采用化学沉淀法由菲汀制取植酸和植酸钠。菲汀经酸浸、沉淀、加碱使沉淀转化可制得植酸钠溶液。植酸钠溶液经减压浓缩、乙醇结晶可制得针状的植酸钠晶体，或经离子交换树脂酸化、浓缩可得浓度为70%的植酸

The saponification and membrane extraction process is a combination of the above processes.

采用皂化萃取工艺，可提高Nd3+的利用率，并可根据皂化率任意控制游离酸浓度。

In part one, the reactions of some active fluorine-containing compounds such as 2, 2-dihydropolyfluoroalkanoic acids and ethyl 2-hydropolyfluoroalkenoates were studied and various fluorine-containing heterocyclic compounds were synthesized. Using 2, 2-dihydropolyfluoroalkanoic acids as the starting material, 4-fluoroalkyl quinolin-2-ols, 2- [ -1-hydropolyfluoro-1-alkenyl] -4H-3, 1-benzoxazin-4-ones, 1-aryl -4, 9-dihydro-3-fluoro-alkyl-1H-pyrazo [3, 4-b] quinolin-4-ones, 5-fluoroalkyl-12H-quin olino [2, 1-b] quinazolin-12-ones, 4-fluoroalkyl-1, 3-dihydro-1, 5-benzodiazepin-2-ones and 4-fluoroalkyl-2H-pyrido [1, 2-a] pyrimidin-2-ones were synthesized through its condensation reaction with anilines, anthranilic acid, N'-aryl-o-aminobenzamides, o-nitro aniline, o-amino pyridine and their derivatives and the subsequent transformations. 5-Fluoroalkyl isoxazolidines, 3-fluoro-3-fluoroalkylisoxazolidino [4, 3-c] quinolin-4-ones, 3-fluoroalkylisoxazolino [4, 3-c] quinolin-4-ones and 2-aryl-3per fluoroacylindoles were synthesized by inter-and intramolecular 1, 3-dipolar cycloaddition of fluorine-containing olefins and nitrones.

第二部分，我们研究了α，α-二氟苄基卤类化合物的亚磺化脱卤反应、产物的转化及全氟烷基亚磺酸盐与芳环化合物的全氟烷基化反应，发现全氟苄基碘或溴及α，α一二氟苄基溴在保险粉等亚磺化脱卤试剂引发下可生成相应的亚磺酸盐；全氟苄基亚磺酸盐与氯气或溴反应可生成全氟苄基磺酰氯或磺酰溴；在烯烃存在下，全氟苄基碘则与烯烃发生加成反应，生成相应的1：1加成产物；在三价醋酸锰的作用下，部分芳香化合物如茴香醚，二甲氧基苯，吡啶，喹啉等可以和过量的全氟烷基亚磺酸盐发生双全氟烷基化反应，反应表现出一定的区域选择性，产率良好。

The main steps include as follows: CO2 is led into the mother liquor of sodium meta-aluminate to carry out carbon content decomposing; the primary separation between the aluminum and the gallium is realized by primary carbonatation to filter out sodium hydroxide; secondary carbonatation is carried out on the filtrate to obtain the deposit of the complex salt of gallium and aluminum; a sodium carbonate crystal is obtained after the filtered filtrate is condensed and vaporized; the deposit of the complex salt of gallium and aluminum is dissolved in the mother liquor of sodium meta-aluminate; the processes are repeated until the proportion of gallium and aluminum in the complex salt of gallium and aluminum is larger than 1/340; then the complex salt of gallium and aluminum is added into the NaOH liquor and electrolyzed, thus obtaining the metal gallium with a purity larger than 99.9 percent which reaches the level of 3; simultaneously, the byproducts of the aluminum hydroxide and the sodium carbonate during the process of carbonatation by steps are obtained.

主要步骤包括：向铝酸钠母液中通入CO 2 进行碳分分解，一次碳酸化实现铝镓的初次分离；过滤出氢氧化钠，滤液进行二次碳酸化获得镓铝复盐沉淀，过滤后滤液经浓缩蒸发获得碳酸钠晶体，铝镓复盐沉淀溶解在偏铝酸钠母液中，重复上述过程直至铝镓复盐中的镓铝比例大于1/340，将其加入到NaOH溶液中，电解可获得纯度＞99.9％的金属镓，达到3N级水平同时在分步碳酸化的过程中获得氢氧化铝和碳酸钠副产品。

The composition comprises: 35 to 65 wt % of an anionic detergent or surfactant selected from alkyl benzene sulphonic acids, alpha olefine sulfonates, long chain fatty acid sulphates, higher fatty acids, as well as the alkali metal and alkaline earth metal salts thereof, and natural detersive agents, and mixtures of any of these; 3 to 15 wt % of a non-ionic detergent or surfactant selected from alkoxylated alkyl phenols and alkoxylated fatty alcohols; 5 to 10 wt % of a water-swellable cellulose derivative or a salt thereof, wherein the cellulose derivative exhibits a viscosity of at least about 1500 cps, measured in a 1 % aqueous solution at 25 DEG C with a Brookfield viscometer having spindle 3, speed 30rpm, factor 40 for viscosities of 2500-3500 cps; 6 to 20 wt % of a solubility regulator selected from alkali metal and alkaline earth metal chlorides, carbonates and sulphates, aluminosilicates and starch; and 0 to 20 wt % of a fragrance or perfume in solid, liquid or microencapsulated form.

该组合物包含：a35―65％重量的阴离子洗涤剂，其选自烷基苯磺酸、α－链烯烃磺酸盐、长链脂肪酸硫酸盐、高级脂肪酸以及其碱金属和碱土金属盐和天然的去污剂，和任何这些组分的混合物；b）3―15％重量的非离子洗涤剂，选自烷氧基化烷基酚和烷氧基化脂肪醇；c）5～10％重量的水可溶涨的纤维素衍生物或它们的盐，其中纤维素衍生物按1％水溶液在25℃下用Brookfield粘度计（3号转轴，转速30rpm，2500―3500cps粘度的因子是40测定；具有粘度至少约1500cps；d）6―20%重量的溶解性调节剂，选自碱金属和碱土金属氯化物、碳酸盐和硫酸盐、硅铝酸盐和淀粉；和e）0～20％重量的为固体、液体或微囊包封形式的香精。

Isoamyl isovalerate was synthesized through esterification reaction by using isovaleric acid and isoamyl alcohol as raw materials and nano-H4SiW12O40/SiO2 as catalyst, the influencing factors in the reaction were studied, and the results showed that the esterification rate could reach 98.6 % under the conditions of the ratio of alcohol-acid 1.4∶1, the use level of catalyst 5 %, and the reaction time 1.5 h.

以纳米复合钨硅杂多酸为催化剂，异戊酸和异戊醇为原料，通过酯化反应合成苹果油，对酯化反应的影响因素进行了研究，结果表明，在醇酸物质的量比为1.4∶1，催化剂用量5%，反应时间1.5h的条件下，酯化率可达98.6%。

For TRO there are a little surfacatants whose effect are not good.In this paper,content of sulfonates and composition of alkyl are decided through right design ;under control reaction conditions different alkylbenzene sulfonates are synthesized;Polyreaction catalyst is developed .non-straight high carbon olefine are made through C9-C12 Polyreaction technolgy;clear composition alkylkenzene is sulfanated in falling-film reactor by SO,product can be adjusted,recipe of the surfacate can be used for super-low interfacialtension with Daqing oil -10-3-10-4mN/m,and stablity is good too.According to method issued by Daqing Develop and Explore Research institute,EOR is over 20% in natural core .

本文研究通过烷基苯磺酸盐组成的正确设计，确定了磺酸盐的当量范围和烷基碳数组成和分布；通过对烷基化条件控制，设计合成了不同碳数的直链和支链烷基苯及烷基二甲苯，并用于制备了相应的烷基苯磺酸盐；研制出了新型的烯烃叠合络合催化剂，采用C_9、C_(12)支链烯烃叠合工艺合成了更高碳数的支链烯烃，并进一步合成出相应的烷基苯和烷基二甲苯；以SO_3为磺化剂，通过对磺化条件的选择和控制，采用已知组成的烷基苯混合物进行膜式磺化反应，使合成工艺得以简化；所得磺酸盐组成确定并且可控，最终配方可与大庆原油形成超低界面张力，达10~3～10~(-4)mN/m数量级，且稳定性良好；以合成的烷基苯磺酸盐为主体形成了三元复合驱配方，室内驱油模拟实验表明，按照大庆研究院对复合驱体系活性剂的评价方法，在天然岩芯上的驱油效率在20％以上。

Our data are showed that apoptosis parameters including DNA fragmentation, nuclear morphological change and sub-G1 fraction, appeared after 24 h by 5 μM rottlerin treatment. Furthermore, rottlerin caused a decrease in 72% of ODC protein expression and an increase in threonine, rather than serine and tyrosine dephosphorylation on ODC enzyme compared with the control after incubation for 10 h. To determine whether ODC could down-regulate rottlerin-induced apoptosis, HL60 cells were stably transfected with ODC cDNA. HL60-ODC cells exhibited a 2.5-fold increase in ODC protein compared with vector only (HL60-pcDNA3) or HL60 cells.

在我们筛选天然化合物实验中，发现rottlerin抑制鸟胺酸去羧化活性最具成效，之前的研究人员已知蛋白激Cd调节鸟胺酸去羧化的活性，因此在人类白血病HL60细胞处理rottlerin的实验中发现加入rottlerin二十四小时后，细胞进行计划性死亡，并可侦测到DNA片段、细胞核浓缩及sub-G1提增；而细胞处理药物十小时后与控制组细胞比较，观察到鸟胺酸去羧化的蛋白表现与活性下降50﹪以上；除此以外，测定鸟胺酸去羧化去磷酸化的情况，发现於酥胺酸位置有显著差异，而丝胺酸和酪胺酸位置并无差异。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。