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The main object of this research is to investigate synthesis of Cu23Cl Cu and CuO nanoparticles through electrospinning and heat-treated method The research is mainly focused on preparative parameter and the change of heat-treated temperature to form the nanoparticles inlaid in silicon fibers the shape and color change are dicussed First of all to prepare the Polyvinyl butyral and silica dioxide complex nanofiber by electrospinning and then to investigate different heat-treated temperature and reactive time to being an influence on the products The results detected by SEM XRD TEM EDS FTIR combined sol-gel process and electrospinning can prepare Polyvinyl butyral and silica complex nanofiber The experimental result is found when heat-treated temperature is 100~4750C it can produce Cu23Cl nanoparticles; Above 4750C~ 4900C it can produce Cu nanoparticles; Above 450~7000C it can produce CuO nanoparticles And the viscosity is lain between 20~40cp and the sol-gel process time is 3hr it can produce the thinner fibers The average diameter of the fibers are 107 88±21 01nm;Due to the nanoparticles inlaid in the silica fibers the thinner fibers can be inlaid the smaller nanoparticles so this is the result that the experiment is expected To calcine the complex fibers is to produce surface silica fibers contain Cu23Cl Cu and CuO nanoparticles due to surface plasma resonance it make the color of the fibers become yellowish green from light white green turn into the red nuclear finally As the experimental result to utilize sol-gel process combine electrospinning can produce porous silica fibers contain Cu23Cl Cu and CuO nanoparticles

本研究旨在探讨「利用放电纺丝和热处理法来合成Cu23Cl、Cu和CuO奈米粒」之研究,实验著重在制备参数与热处理温度变化对所形成的奈米粒镶嵌在二氧化矽纤维中的形态与颜色变化探讨。首先,利用放电纺丝法制备出聚乙烯醇缩丁醛及二氧化矽之奈米纤维,比较不同的热处理温度与反应时间的改变对产物生成产生影响,进而研究不同热处理温度和时间对生成奈米粒的影响。产物经由SEM、XRD、TEM、EDS和FTIR等仪器分析结果显示,结合溶胶-凝胶法(sol-gel process)和放电纺丝法可产生聚乙烯醇缩丁醛及二氧化矽复合奈米纤维。实验结果发现,若热处理温度在100~4750C下可得到Cu23Cl奈米粒,475~4900C 可得Cu奈米粒,450~7000C以上可得 CuO奈米粒。而黏度介於20~40cp间和溶胶-凝胶时间为3hr时,可产生直径比较细的纤维,纤维直径为107 88±21 01nm;且由於奈米金属颗粒镶嵌在二氧化矽纤维中,直径比较细的纤维,可以得到比较小的奈米金属颗粒,这与实验预期相符。而锻烧此复合物产生多孔的二氧化矽纤维并包含Cu23Cl、Cu和CuO奈米微粒时,由於表面电浆子共震关系,而使纤维颜色由淡白黄绿色变成黄绿色,再变红褐色。由实验结果得知,利用溶胶-凝胶法(sol-gel process)结合放电纺丝法和不同热处理温度,可产生Cu23Cl、Cu和CuO奈米粒镶嵌在二氧化矽纤维。

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Therefore, it has the important scientific research value in studying the relationship between the changing of the parameters (including the temperature, the humidity, the grain radius and so on) and the electricity and radioactivity of the medium. Applied the count statistics and the numeral value analysis, the paper analyzes, concludes and contrasts the data sufficiently through the experimentation, and acquires the following results that the resistivity and the polarizability both have the negative relationship with the temperature variety of medium from 0℃ to 200 ℃. The parallactic poalarizability is consistent with the temperature variety in the plan as well as the section, but their trends are exactly opposite. Power supply voltage has no considerable influence to the resistivity and polarizability by using duality variance analysis, however, the detecting depth and the plan position influence them greatly. Different AB/2 interval that increases by degree does not influence variance and the average value of the resistivity and the polarizability remarkably. By using the least double multiplication, the relationship of temperature-time-the influence radius of the fire source is carried up by the mathematic drawing up. After discussing their correl ation, I educe the influence radius of the fire source and carry out the 'trend analysis and forecast to the spacial changing of the temperature and the parallactic polarizability in the end.

本文通过试验并应用数理统计和数值分析等相关理论对所得到的试验数据进行了分析、归纳和对比,得出了介质温度变化在0-200℃内视电阻率和视极化率与温度均表现为负相关性;视极化率与温度在剖面和平面上的变化形态具有很好的一致性,但变化趋势相反;由二元方差分析可得供电电压对视电阻率和视极化率无显著影响,但探测深度和平面位置对视电阻率和视极化率有显著影响;通过假设检验可证不同AB/2递增间隔,对视电阻率和视极化率的方差和平均数影响都无显著性差异;应用最小二乘法对温度——时间——火源影响半径之间的关系进行了数学拟合,讨论了它们之间的相互关系,得出了火源影响的有效半径,太原理工大学硕士研究生学位论文并对温度和视极化率的空间变化作了趋势分析和预测。

Based on these observations, we hypothesised that (1) the length of the breeding season, food resources and predation are critical for the evolution of passerine reproductive patterns in alpine meadows;(2) that alpine meadow passerines used single-investment and accumulative-investment strategies;(3) that the typical clutch size was actually the most efficient for reproductive purposes;(4) and that the transition from neonate to fledgling passerines is a relatively fixed process as compensatory growth does not appear to occur;(5) and that growth period is volatile.

高寒草甸雀形目鸟类受适合繁殖季节长度、食物资源和捕食压力的影响,或选择逐步投资对策,或选择一次投资对策;每个种群的常见窝卵数就是最适窝卵数;雏鸟的发育模式相对固定,不存在补偿性生长,但是生长期长度是可变化的。

She returned her eyes to Roy and to the transformable puzzle block one of the ship's child-care specialists had handed him.

她转身看着罗伊和一位托儿所老师交给他的那个可变化的谜题方块。

Interlayer oxidized zone can be divided accurately by Fe_2O_3, Fe_2O_3/FeO and U parameters. We can correct the field macroscopic color zoning by combining the macroscopic zoning and microscopic zoning. Univalent major elements components(Al_2O_3, SiO_2, K_2O, Na_2O) show remarkable activity at the process of interlayer oxidizing, their contents are variable and mingled in different zones and it can't be used in zoning. But we can speculate the developmental degree of interlayer oxidized zone and uranium mineralization according to the concentration trends and variation characteristics of sensitivity group, activity group and their ratios .(3)The comparatively steady elements such as lithiphile elements, sulfophile elements and high field strength elements change regularly at the process of interlayer oxidation except some radioactive elements. Trace elements and rare earth elements commonly enrich in thin rock clast such as mudstone, in which the enriched elements species are more than those in the whole rock, which indicate that the regeneration action in caulking matter are more deep than that in whole rock at the process of interlayer oxidation, and the reallocate intention of trace elements in main minerlized rock in Tuha basin are more intensive than that in Yili basin at the process of deposition ,diagenesis and later changes .

根据化学蚀变参数PC值和分离迁移位等将常量元素组分分为敏感组分组、活动组分组、次活动组分组和惰性组分组,不同组分可分别用于讨论层间氧化带低温地球化学中不同问题;敏感组分(变价元素组分Fe_2O_3、FeO)和U在层间氧化带中迁移富集规律明显,Fe_2O_3/FeOFe~(3+/Fe~(2+)比值具分带判别能力,配合U含量对层间氧化带进行较准确的分带,可克服野外宏观颜色分带偏差:提出Fe~(3+)/Fe~(2+)分带判别值在不同盆地、不同地段不同,除受氧化作用控制外,流体酸碱度不同也是重要因素的观点,对找矿实践有实际指导意义;活动组分(Al_2O_3、SiO_2、K_2O、Na_2O)在层间氧化作用过程中具有较明显的活动性,其含量值变化跳跃,在不同分带相互交织,不具分带指示意义;但利用敏感组分、活动组分及其比值在层间氧化带中的变化特征可推测层间氧化带发育的完善程度及其含矿性;次活动组分组(CaO、MgO、MnO_2)含量低,变化规律性差;惰性组分组(TiO_2、P_2O_5)含量低,活动稳定,可用来反映沉积物源特征。

Can also change the speed, such as "slow is slow tortoise", and that the last-place, winning only Oh!

可变化速度,例如「很慢很慢的乌龟」,那最后一个到位子的人,才算赢喔!

To secure hand-finished waistbands, tailor ed buttonhole facings, and bindings use a variation of this hem stitch, picking up the machine stitches instead of the folded edge.

为了使手工整修的腰带、西装纽洞贴边牢固,卷边针法可变化,挑起机缝线迹而不是折边。

To secure hand-finished waistbands, tailored buttonhole facings, and bindings use a variation of this hem stitch, picking up the machine stitches instead of the folded edge.

为了使手工整修的腰带、西装纽洞贴边牢固,卷边针法可变化,挑起机缝线迹而不是折边。

To secure hand-finished waistbands, tailored buttonhole facings, and bindings use a variation of this hem stitch , picking up the machine stitch es instead of the folded edge.

为了使手工整修的腰带、西装纽洞贴边牢固,卷边针法可变化,挑起机缝线迹而不是折边。

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In the United States, chronic alcoholism and hepatitis C are the most common ones.

在美国,慢性酒精中毒,肝炎是最常见的。

If you have any questions, you can contact me anytime.

如果有任何问题,你可以随时联系我。

Very pretty, but the airport looks more fascinating The other party wisecracked.

很漂亮,不过停机坪更迷人。那人俏皮地答道。