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Hydrastine(97.7%) was obtained with extracted rate 65%by extracting the Goldenseal with mixed Solvent;Berberine hydrochloride (99.9%) was obtained by adding hydrochloride acid to alcohol (alcohol∶H 2O=1∶1) solution of the extract and Hydrastine (99.5%) was gained by CLC method with the yield 1%.

原药材用混合溶剂直接提取分离,可得到含北美黄连碱 97.7%的结晶体,提取率达 6 5%;提取物经醇水溶解、酸化,可直接获得小檗碱盐酸盐结晶,纯度达到 99.9%;用柱色谱法,可得到 99.5%的北美黄连碱,收率约 1

The exact of petroleum ether was the acaricidal active site of Eungenia caryophyllata. 3.Isolation, purification and identification of compounds with acaricidal activity in Eugenia Caryphyllata: The exact of petroleum ether was separated into 6 parts by silica gel column chromatography with gradually increasing polarity of petroleum ether: ethyl acetate. The part C was demonstrated to be the most effective part by acaricidal activity test in vitro,and the time for it to kill all experimental mites was about 20 min.

丁香杀螨活性成分的追踪分离、纯化与结构鉴定:采用硅胶柱层析法,以石油醚:乙酸乙酯溶剂系统梯度洗脱,对丁香石油醚提取物进行分离,得到A~F 等6 段混合物,离体杀螨试验发现,C 段混合物具有突出的杀螨活性,50%浓度平均15min可杀死全部供试螨虫。

The ionomer membrane under the conditions of 20℃ and 0.05 MPa shows better permeaselectivities that the permeability coefficient of CO_2 and CO_2/ N_2 separation factor are 223 Barrer and 65.70, respectively, while CO_2 / CH_4 separation factor is only 14.70. An obvious increase in P_(CO_2) with decreasing pressure difference exhibits a characteristic of facilitated CO_2 transport, which is not disappear and almost unchange after two months. There is no this behavior for N_2 and CH_4. Hence, P_(CO_2) and α_(CO_2/N_2) and α_(CO_2/CH_4) can be enhanced simultaneously.

该离聚体膜显示出良好的CO_2渗透性能,在20℃和0.05MPa压差下,CO_2渗透系数P_(CO_2)和CO_2/N_2分离系数αCO_2/N_2分别高达223 Barrer和65.70.P_(CO_2)和αCO_2/N_2随CO_2压差的降低而明显增大,显示出促进输送特征,这一行为即使在膜放置2个月之后并不消失,渗透分离性能变化不大。N_2和CH_4无此性能,因此在气体压差较低时,P_(CO_2)和αCO_2/N_2、αCO_2/CH_4可同时提高。

The ionomer membrane under the conditions of 20℃ and 0.05 MPa shows better permeaselectivities that the permeability coefficient of CO_2 and CO_2/ N_2 separation factor are 223 Barrer and 65.70, respectively, while CO_2 / CH_4 separation factor is only 14.70. An obvious increase in P_(CO_2) with decreasing pressure difference exhibits a characteristic of facilitated CO_2 transport, which is not disappear and almost unchange after two months. There is no this behavior for N_2 and CH_4. Hence, P_(CO_2) and α_(CO_2/N_2) and α_(CO_2/CH_4) can be enhanced simultaneously.

该离聚体膜显示出良好的CO_2渗透性能,在20℃和0.05MPa压差下,CO_2渗透系数P_(CO_2)和CO_2/N_2分离系数αCO_2/N_2分别高达223 Barrer和65.70.P_(CO_2)和αCO_2/N_2随CO_2压差的降低而(来源:e2b2A2bBC论文网www.abclunwen.com)明显增大,显示出促进输送特征,这一行为即使在膜放置2个月之后并不消失,渗透分离性能变化不大。N_2和CH_4无此性能,因此在气体压差较低时,P_(CO_2)和αCO_2/N_2、αCO_2/CH_4可同时提高。

According to the experiment results, the proposed system could be used in chromatographic separation.

对苯和萘的分离结果表明,电动流动分析系统可用于样品的色谱分离。

It was demonstrated that the sulphonated phase could be used to prepare columns for the separation of alkaline drugs, symmetric peaks were obtained for them and base-line separation was realized.

在磺酸型的固定相上,则成功地分离了一些碱性药物,得到了较好的对称峰型,这些药物间可达到基线分离。

By using acetonitrile-water (pH=3.85) as the mobile phase, with a flow rate of 1.0mLmin^(-1), detected at 294nm, washed by gradientelution, the mian alkaloids can be separated in HPLC. The figure was applied to qualitative analysis, and quality control of alkaloids in thesium chinese turcz.in some extent.

在流动相为乙腈-水(pH=3.85),流速为1.0mLmin1,检测波长为294nm的条件下,进行梯度洗脱,在HPLC图谱上百蕊草提取液中主要生物碱可得到理想分离,图谱可为定性分析提供依据,并可在一定程度上进行百蕊草生物碱物质的质量控制。

Studied in the paper are the performance, separation efficiency and pressure loss of a uniflow square shaped cyclone separator which can be directly and easily installed on the water wall of a circulating fluidized bed boiler.

对可与循环流化床水冷壁直接结合而易于布置的下排气方形旋风分离器的性能指标:分离效率、压降等进行了研究。

18 Days after perithecia appearance was the best time to isolate ascospores, although there were differences between crosses. The highest survival percentage of ascospores could reach up to 85. 5% during this period.

观察发现,虽然不同杂交组合间有一定差异,分离稻瘟病菌子囊孢子的适宜时期,一般在子囊壳开始出现后7~18天之间;在此期间分离出的子囊孢子成活率最高可达85.5%。

Results We isolated 2 strains of Bdellovibrio sp.(5#-12 and 5#-sh06) from sea mud of Shenzhen bay. Both strains grew between 20℃ and 35℃, with 25℃ and 30℃ as optimal temperature for 5#-12 and 5#-sh06, respectively. They grew between pH 6.1 and 8.6, and the opti℃mal pH for both was 7.2. Lysis experiments on 58 strains of pathogens were conducted and the results showed that 5#-12 and 5#-sh06 lysed 46 and 48 strains, corresponding to 79.3% and 82.8% of lysis abilities. Taken both two Bdellovibrio strains together, they lysed 96.6%(56 strains) of tested pathogens and 100% of tested vibrios (39 strains).

从深圳湾海泥中分离出2株蛭弧菌,分别命名为5#-12和5#-sh06,它们可在20℃~35℃范围内生长,最适温度分别是25℃和30℃;生长pH范围6.1~8.6,最适pH均为7.2;2株蛭弧菌可分别裂解46和48株试验菌,各占总试验菌株数(58)的79.3%和82.8%;联合2株蛭弧菌,可裂解56株试验菌,占总试验菌株数的96.6%;同时,它们一起能将所有试验弧菌裂解。

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I am accused of being overreligious," she said in her quiet, frank manner,"but that does not prevent me thinking the children very cruel who obstinately commit such suicide.""

客人们在卡罗利娜·埃凯家里,举止就文雅一些,因为卡罗利娜的母亲治家很严厉。

Designed by French fashion house Herm è s, this elegant uniform was manufactured in our home, Hong Kong, and was the first without a hat.

由著名品牌 Herm è s 设计,这件高贵的制服是香港本土制造,是我们第一套不配帽子的制服。

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不要 '夸大' 你的业绩或成果,条件或者技能。