变晶

Fig. 5 Composition of chromium spinels and diagram of Cr2O3 of chromium spinels and Al2O3 of orthopyroxene b

第4 期陈世忠等：铬尖晶石和石榴石的相变表现不同行为，Cr 和Mg 强烈分配在固态中，Al 强

For the available of individual endothermic peak of crystal structure transition at low temperature and the enthalpy change of pure pentaerythritol in different system, the concentration in mixtures and complex coating systems could be determined.

利用在较低的温度下复杂体系中季戊四醇的晶型转变吸热峰独立存在的特点，根据其在不同混合体系中的焓变，确定该组分在混合体系及涂料中的质量百分数。

After fired at 1600℃, with the increase of zircon addition the bulk density of the samples increases while apparent porosity decreases. When zircon addition is 4%, the strength is the best, and the photomicrograph of the sample exhibits a densely packed microstructure, with larger and better developed grains of periclase and spinel. Meanwhile, the direct bonding of solid phases is reinforced.

在1600℃热处理下，随着w(ZrSiO4)的增加，试样的体积密度增大，显气孔率变小，试样力学强度在w(ZrSiO4)为4%时达到最大值。w(ZrSiO4)为4%的试样整体显微结构致密，固相直接结合程度提高；并且方镁石和尖晶石晶粒的晶粒尺寸粗大，晶粒发育比较完整。

The effect of fine particles on the flow behavior of polycrystalline ice under stress has been studied.

研究了应力下微粒对多晶冰流变行为的影响。

A petrographic analysis combined with electron microprobe analysis and SEM shows that black opaque matters, whose composition is mostly of microcrystalline silicate and magnetite, are widely found running reticulately through mineral particles, crystals and cleavage cracks in association with metasomatic alteration in the mafic-ultramafic xenoliths and their host rocks.

经岩相学和电子探针及扫描电镜分析发现，伴随交代蚀变，寄主岩和各类镁铁-超镁铁质包体岩石中，普遍发育沿粒间和矿物晶体裂隙或解理纹贯入或穿插的黑色不透明物质，主要由微晶硅酸盐矿物和磁铁矿组成。

Combined crystallization kinetics analysis obtained via rheometry and morphological observation of crystals growth performed on POM, two different mechanisms of shear-enhanced crystallization for PP/ grafted MWCNTs composites were suggested:(1) at low temperature, strong heterogeneous nucleation plays a dominant role on the. crystallization behavior, which would be saturated at a higher filler content, and the effect of shear-enhanced crystallization was weak;(2) at high temperature, the effect of heterogeneous nucleation was substantially depressed, and the crystallization of the composite was obviously accelerated by pre-shear and the thread-like crystallites were generated earlier than the spherulites.

结合流变测试结果和热台偏光显微镜观察的结晶形貌发展过程，对于PP／G—MWCNTs体系得到了两个不同的剪切影响机理：(1)在低温条件下，强烈的异相成核作用对结晶行为的影响占主导优势，而剪切作用对结晶的影响十分微弱，同时，在填料含量较高是，异相成核作用具有饱和性；(2)在高温条件下，异相成核作用被抑制，复合体系的结晶主要受到预剪切作用的影响，并且纤维状晶体较球晶更易生成。

Finally roud and flat elliptic cross-section samples with uniform shape, smooth surface and unidirectional crystals have been successfully obtained.

最终在等截面送料、变截面送料的条件下分别抽拉出了成形良好，表面光洁，具有单向柱状晶组织的圆形截面、扁椭圆形截面的样件。

And the PLA/Chitosan/ACP barriers with additional 2 wt% chitosan still maintain 56.58 % antibacterial ability after eightieth day. The different composition of PLA/Chitosan/ACP composites was prepared by water washing solidification from NMP/water/lactic acid consolvent. After storing at room temperature for 48 hours and taking it out to obtain a shapable composites. To investigate the influence of ratio of composition with the shapable property of composites, it was analyzed by Rheometer, TGA, AFM, XRD. The result of the different APC content had different effect both water content and yield stress of composite materials. The yield stress decreased with ACP content while increases. It was derived that ions, released from ACP interact with amide groups of chitosan to form water-absorbing ionic clusters through chelating or electrostatic attraction.

另外，以聚乳酸/几丁聚醣作为基材并添加不同比例的非晶型磷酸钙，经过水洗固化后可得白色片状沉淀物，於室温下静置48小时后，复合材之体积呈现膨胀且具有可塑形之特性，以热重分析仪与流变仪分析样品之含水率与屈伏应力，结果显示不同ACP含量对复合材含水率与屈伏应力具有消长变化，而PLA/Chitosan/ACP之可塑程度与其所吸收之水份多寡有关，推测可能机制为ACP磷酸钙盐解离后之金属离子与几丁聚醣之胺基透过螯合作用或静电吸引之交互作用，形成具吸水性之离子团簇分散於疏水性之聚乳酸基材中。

Liquid-crystalline compounds with sulfur, reported in recent years,readily form smectic phases and exhibit broad-range mesophases.

近年文献中出现的含硫的液晶化合物具有易形成近晶相和相变温度宽等特点。

It was iound in the experiment that the glass fiber made crystal peak temperature raise 8~9 ℃, Crystal original taper to be large, spherocrystal size small, it -acted the function of hetero-geneous nucleation for polypropylene . High density polyethylene has plasticizing efficancy and combined effect of hetero-geoeous nu...

试验表明PP/GF/HDPE复合物的结晶峰温度升高8～9℃，结晶起始斜率变大，球晶几何尺寸明显减小，复合物中的玻璃纤维起到异相成核作用，高密度聚乙烯对聚丙烯有增塑作用并对异相成核具有协同效应。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。