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The extraction from star anise fruits was obtained by supercritical carbon dioxide extraction(SFE-CO_2) method at the pressure 16 MPa,temperature 35℃,flow rate 30 L/h meanwhile time 2 h,and the star anise oil was obtained by steam distillation.

用超临界CO2萃取(SFE-CO2)技术,在压力16 MPa、温度35℃、反应时间2 h及CO2流量30 L/h的条件下,对八角茴香的果实进行了萃取,得到八角茴香萃取物,并用水蒸气蒸馏法提取八角茴香精油。

The study has shown:(1) With increasing sediment depth and the woody giblets, the total organic carbon, the extraction of benzene , the total humic acids and the unhydrolyte are enhanced, while the hydrolyte is decreasing.(2) According to the GC-MS analysis, n-alkane,n-alkan-2-ones and n-alkanones are composed mainly of long-chains,such a result is thought to be characteristic of a herbaceous input from 2300a.B.P. n-alkanones exist in the samples may be considered as the evidence of microorganisms activity.(3) It is showed that the lipids is more sensitive to the climate change than the floristic. The proxy of the pollen spore of the peat stratum is different from the normal environment proxy. It is one of the main reasons that the sensitivity difference of the bog vegetation reacting to the climate isn't accordant with the log of the fat molecule fossil and biology fossil.(4) The transformation of the peat organic carbon is under the influence of temperature,acidity,organic material constituting, etc, and it showed the up-trend with the depth. In the short-term scale, the conversion of the peat organic carbon is effected by seasonal water,regional climate and vegetations; while in the long-term scale, it is controlled mainly by the climate.(5) According to the comparing the orderliness of organic compound,vegetation giblets with the depth to the characteristics of the peat molecule fossil with the section, in the development of this peatmire, 1500a B.P(210cm)is regard as the borderline of the late Holocene, the keynote of the front period is warm with several cold fluctuations, and the trend of the back period is dry and cold although there were several fluctuations.

研究表明:(1)随深度的增高及植物残体中木本残体的增多,总有机碳、苯萃取物、总腐植酸、不被水解物含量逐渐增高,而易水解物含量减少;(2)GC- MS分析显示,正构烷烃,直链烷基2-酮和正烷醇均以长链组分为主,揭示了该泥炭柱剖面2347a.B.P的母源输入以草本植物为主;甲基酮类和短链正烷醇的存在是微生物活性很大的生物证据;(3)通过有机分子标志物与孢粉、植物残体等指标的对比研究表明:脂类化合物对气候变化的反映要比植物种灵敏得多,不同沼泽植物对气候变化的敏感性的差异是脂类分子化石记录与生物大化石结果很难一致的主要原因之一;(4)泥炭有机碳的转化受到温度、酸度、有机物质组成等很多因素的影响,短时间尺度,泥炭有机碳的转化受季节性降水、地方气候和植被等因素的影响;长时间尺度,泥炭地有机碳的转化,受气候条件控制;(5)总结泥炭分子化石特征、泥炭有机质各组分含量及植物残体组成随深度的变异规律,分析结果显示该泥炭地层形成过程中,1500a B.P(210cm)可作为划分前后晚全新世的界线,前期的基调是气候偏暖,但又有几次偏干冷气候的反复,后期气候以干冷为主,其间虽有几次上升波动,但整体趋势不变。

The results showed that extracts from the hexane layer have the best abilities to inhibit the growth of the aforementioned tumor cells.

实验结果显示,经分配萃取后的Hexane萃取物作用於三株细胞株具有良好抑制生长的能力。

The results show that the inhibition included both reversible and irreversible process. The optimal solvent for extracting FAS inhibitors is 50% ethanol.

结果表明,边茶萃取物对FAS有可逆和不可逆抑制双重作用,最佳萃取溶剂为50%的乙醇,在常温下5 h即可达到最佳萃取效果。

The yield of essential oil by supercritical CO2 extraction was increased 55% than steam distillation. The oil is a light yellow liquid with high purity and strong flavoring of D. kaki fruit.

用超临界CO2萃取柿叶精油比水蒸气法蒸馏的柿叶精油得率提高了55%,萃取物纯度高,有浓郁的柿果香味,色淡黄。

ObjectiveTo study the optimal technology of supercriticalCO2 fluid extraction(SFECO2) on Lycopodium japonicum Thunb.and validate the drug action of extract.

目的考察超临界CO2 流体萃取伸筋草有效成分的最佳工艺,进一步验证萃取物的药效。

The antioxidation effects of the thyme extract were also investigated in this experiment.

探讨了萃取压力、时间、温度等因素对萃取收率的影响,并将萃取物进行了抗氧化实验。

The first part of this research was to investigate anti-oxidant abilities of Boehmeria nivea leaf and root. Different extraction methods, drying conditions as well as far infrared were applied to measure their effects on anti-oxidant abilities of Boehmeria nivea leaf and root. Results showed that 95% ethanol extracts of fresh leaves and roots demonstrate the highest anti-oxidant components(total contents of phenol compounds and flavonoids)and scavenging abilities free radical scavengingABTS(2,2'-azinobis[3-ethylbenzothiazoline-6- sulfonic acid]and DPPH (α,α-diphenyl-β-picrylhydrazyl) free radical , followed by hot water and cold water extraction.

本研究第一部份拟针对苎麻叶与根探讨其抗氧化能力,并以不同萃取方法、不同乾燥处理方式及经远红外线照射对其抗氧化能力之影响,研究结果显示,在不同萃取方法中,新鲜苎麻叶与根皆以95%乙醇萃取物的抗氧化成分及抗氧化能力清除ABTS(2,2'-azinobis[3-ethylben-zothiazo-line-6

Results of acute treatments of oral glucose tolerance test showed that the plasma glucose levels of the diabetic Wistar rats administered, both of guava fruit water or alcohol extracts, with 200 or 400 mg/kg BW were lower than the control group (fed with equal volume of saline solution) after 30 minutes gavages. It is considered that the extracts containing protein, lipid and diet fiber may defer the stomach and small intestines to get empty and interfere or delay the sugar absorption and then increase the glucose utilization in diabetic rats.

结果显示糖尿病鼠不论灌食番石榴果实之水及乙醇萃取物粗萃物200或400 mg/kg BW的剂量,於OGTT第30分钟后的血浆葡萄糖值均比糖尿病控制组显著降低,推测原因可能与番石榴粗萃物所含的蛋白质,脂肪及膳食纤维延缓胃和小肠的排空,具有干扰或减缓葡萄糖的吸收,因而促进体内组织细胞对血液中葡萄糖的利用有关。

A study based on the separation of tall oil with supercritical carbon dioxide extraction was carried out. The author found the optimum extractive condition of the acid of tall oil at the feasible temperature, pressure, flux of carbon dioxide and time, analyzed the acid and confirmed their composition.

以工业妥尔油为原料,通过超临界二氧化碳萃取方法,在适宜的温度、压力、二氧化碳流量和时间等条件下,进行了塔尔油主要成分的分离;确定了最优化萃取工艺条件;对萃取物的主要成分进行了分析;从萃余物中提取出粗植物甾醇,粗植物甾醇经进一步的精制得到高纯度的β-谷甾醇。

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