取物

It is existed competitiveness inhibition of 6APA, non-competitiveness inhibition of PAA and substrate inhibition of Penicillin on the hydrolysis of benzylpenicillin to 6APA and PAA by an immobilized penicillin amidase. The heat conductive coefficients were determined on the vacuum elevation liquid membrane concentration. The thermodynamics and kinetics of PAA extraction were studied on the organic solvent extraction of the above solution.

研究证明固定化青霉素酰化酶裂解反应是典型的底物、产物抑制酶反应，其反应动力学数据表明，青霉素、苯乙酸以及6APA对反应分别存在底物抑制、非竞争性抑制和竞争性抑制；真空升膜浓缩适应热敏性以及粘度不大的物系，对于6APA水溶液的真空升膜浓缩过程研究得到了浓缩实验的传热系数；浓缩液萃取主要是提取出其中的苯乙酸，本文测定了不同温度以及溶剂条件下的苯乙酸溶解度，并观测了苯乙酸萃取动力学。

Batch extractive distillation is used to separate azeotrope or the mixture of which the relative volatility is close to 1.0. For it has both advantages of batch distillation and extractive distillation, batch extractive distillation is becoming increasingly important to the production of small scale and high value products like fine chemicals and pharmaceuticals.

间歇萃取精馏是分离共沸物或近沸物的一种方法，由于它结合了间歇和萃取的优点，特别适用于化工、制药、溶剂回收、天然产物提取等产量小，品种多的行业，因此间歇萃取精馏近年来已成为非常活跃的研究和开发领域。

Meanwhile, experiment with the ternary mixture of methanol, butyl methyl ether and 1-chlorobytane showed that the system was not ternary azeotrope and can be separated by combination of extractive and rectification using water as extractive solvent.

针对甲醇、甲基正丁醚和正氯丁烷三元混合物，研究了该物系的性质，得到该物系不是三元共沸物的结论，并用水作萃取剂，通过实验验证了利用萃取和精馏耦合的方法分离该物系的可行性。

A total of 614 sediment samples at an interval of about 1.5 m from all 5 sites of the Integrated Ocean Drilling Program Expedition 311 on Cascadia Margin, northwestern Pacific were analyzed using a Beckman Coulter LS230 Particle Analyzer. The grainsize data were then plotted against depth and compared with other potential proxies of gas hydrateoccurrence such as soupy/mousselike fabrics in sedimentary textures, gas hydrate concentration derived from LWD data using Archie's relation, IR core images and the recovered samples of gas hydratebearing sediments.

对取自IODP 311航次（东北太平洋Cascadia大陆边缘）所有5个站位、采样间距约为1.5 m的614件沉积物样品，利用Beckman Coulter LS230激光粒度仪进行了沉积物粒度分析，获得了沉积物粒度随深度变化特征，进而与水合物层位的替代指标进行了位置对比，这些指标包括特殊沉积构造（soupy和mousselike构造）、测井数据推算出来的水合物饱和度、岩芯红外图像和实际钻取的含水合物沉积物等。

A total of 614 sediment samples at an interval of about 1.5m from all 5 sites of the Integrated Ocean Drilling Program Expedition 311 on Cascadia Margin, northwestern Pacific were analyzed using a Beckman Coulter LS-230 Particle Analyzer. The grain-size data were then plotted against depth and compared with other potential proxies of gas hydrate-occurrence such as soupy/mousse-like fabrics in sedimentary textures, gas hydrate concentration S(subscript h derived from LWD data using Archie's relation, IR core images and the recovered samples of gas hydrate-bearing sediments.

对取自IODP311航次（东北太平洋Cascadia大陆边缘）所有5个站位、采样间距约为1.5m的614件沉积物样品，利用Beckman Coulter LS-30激光粒度仪进行了沉积物粒度分析，获得了沉积物粒度随深度变化特征，进而与水合物层位的替代指标进行了位置对比，这些指标包括特珠沉积构造（soupy和mousse-like构造）、测井数据推算出来的水合物饱和度S(下标 h、岩芯红外图像和实际钻取的含水合物沉积物等。

The effects of ,, and temperature on the distribution ratio have been investigated. The composition of the extracted species is determined by the methods of slope ratio, continuous variation,extraction isotherm curves and their chemical analyses. The extraction is found to proceed according to the reaction:AuCl_4 ~-+DEOTA_(0)TAuCl3 .DEOTA_...

着重研究了盐酸浓度、氯离子浓度、氢离子浓度和温度诸因素对萃取的影响；对有机相中金的反萃行为也进行了初探；通过斜率法、等摩尔系列法、萃取等温线法确定了配合物的组成；推定了DEOTA在盐酸体系中萃取金的机理为配位取代反应；计算了萃取反应的表观平衡常数和配合物的稳定常数。

The allograft was harvested at 6h posttransplantation. Scrambled ODN group: The donor kidney was stored for 6h in ECs containing 1 u M Liposome/scrambled ODN complexes under hypothermal and hypoxia condition, then the donor kidney was transplanted into a SD recipient, and at 6h posttransplantation the allograft was harvested.

五、试验分四组：(1) Control组假手术组，Wister大鼠麻醉后，开腹后，即将伤口缝合，6h后切取左肾；(2) ECs组供肾经ECs(不含脂质体/ODN复合物)低温缺氧保存6h，移植到受体大鼠6h后切取移植肾；(3)deeoy onN组供肾经含1 pM的deeoy onN脂质体复合物的ECs 低温缺氧保存6h，移植到受体大鼠6h切取移植肾；(4)sc~。

Lithium metaborate melting technology was used to make the quick analysis flow sheets of rock samples by Inductively Coupled Plasma Atoms Emission Spectrometry.

应用偏硼酸锂熔融技术建立岩石样品电感耦合等离子体原子发射光谱法的快速分析流程，并针对含锂硼酸盐熔融物较难溶解的特点，通过熔剂与样品混匀方式实验、熔融体形成龟裂条件实验和浸取液条件实验，研究三者与熔融物浸取时间的关系，从而选择一个适合ICP-AES分析技术的最佳熔融和浸取条件。

Extractive distillation and liquid-liquid extraction are effective separation processes to deal with the separation of close boiling compounds or azeotropes systems. The selection of appropriate solvents is the key.

化工生产中常遇到欲分离组分之间的相对挥发度接近1或形成共沸物的难分离物系，萃取精馏和液液萃取是常用且有效的方法，其中萃取剂的选择是关键。

In an acetate buffer of pH 6.0,and in the presence of CTMAB,a stable complex,having the mole ratio of 1 to 3,was formed between cobalt ion and nitroso R salt,which was concentrated on C18 solid phase extraction column,achieving a concentration multiplication of 100 times.

研究了用亚硝基R盐离子对固相萃取光度法测定钴，在pH 6.0的HOAc-NH4OAc缓冲介质中，溴化十六烷基三甲基铵存在下，亚硝基R盐与钴反应生成3∶1稳定络合物，该络合物可用C18固相萃取小柱富集，富集倍数达100倍，小柱上富集的络合物用乙醇洗脱后用光度法测定，钴的质量浓度在0.05~5.0 mg.L-1内符合比耳定律。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。