发烟硫酸

The influence of excess anhydrous hydrogen fluoride, the amount of oleum and its trickling rate, the time and temperature of heating hexafluorophosphoric acid, and refrigerants on the yield and the content of phosphorus pentafluoride was studied.

在此过程中，本文研究了无水氟化氢过量百分率、发烟硫酸用量及滴加速度、六氟磷酸的加热时间、加热温度以及冷凝介质等因素对五氟化磷产率和纯度的影响。

Difluorodiphenylsulfone and 4, 4"-difluorodiphenylketone are sulfonated by 50 % sulfuric acid. A new biphenol monomer containing six-membered ring imide is synthesized by reaction of 1, 4, 5, 8-naphthelenetetracarboxylic acid dianhydride with 3-aminophenol or 4-aminophenol sodium.

以50%发烟硫酸为磺化试剂，以4，4′-二氟二苯砜和4，4′-二氟二苯酮为原料反应得到双磺化的4，4′-二氟-3，3′-二磺酸钠-1，1′-二苯砜和4，4′-二氟-3，3′-二磺酸钠-1，1′-二苯酮。

Determination of total acidity, and calculation of free sulphur trioxide content of oleum.

发烟硫酸中游离三氧化硫成分的计算和总酸度的测定。

Sulfur trioxide in oleum was necessary for the reaction system.

对于甲烷液相部分氧化反应，发烟硫酸中游离的SO3是非常重要的影响因素。

Learn to calculate the concentration of sulphuric acid and oleum.

会对发烟硫酸浓度进行换算。

The paper discussed present processes of oleum production ,found the process using tube-shell evaporator is reliable.

国内外发烟硫酸生产方法很多，通过比较分析找出了管壳卧式蒸发器生产法是适合的生产工艺方案。

At present, although the iodine as a catalyst, oleum as the solvent liquid phase partial oxidation of methane research is not adequate, but the reaction has higher yield and the conversion rate of the industrialized good prospects to enlarge production.

目前，虽然以碘为催化剂、发烟硫酸为溶剂的甲烷液相部分氧化反应的研究尚不充分，但是该反应具有较高的转化率和收率，工业化放大生产的前景良好。

The alkylbenzene and alkylmethylbenzene are sulfonated by using 20% oleum as the sulfonating agent.

采用发烟硫酸对合成的系列烷基苯中间体进行磺化。

The development of novel catalysts is the key of the study. In some typical technologies developed up to now, [PtCl2] or HgSO4 is used as catalyst with oleum as solvent with higher conversion ratio and yield.

甲烷液相部分氧化反应制甲醇的研究中催化剂的开发是该研究的关键，迄今为止，已开发的该过程典型工艺是在发烟硫酸溶剂中，采用铂配合物[PtCl2]或HgSO4为催化剂进行的反应。

Based on this result, a new technology is suggested, that is by regulating the effective sulphonating contents of 1-amino-anthraquinone, adjusting the concentration of sulfuric acid to hydrolyze 1-amino-anthraquinone disulfonic acid conversing to 1-amino-anthraquinone -2-sulfonic acid, and briminating the hydrolyzed product in 100% sulfuric acid, 87% yield of Bromamino-acid was achieved, 10% higher than the conventional method prepared by "oleum method".

此新工艺，溴氨酸在产物中含量可达87％，比常规的发烟硫酸法生产溴氨酸提高了10％，质量和收率都接近或达到溶剂法生产的水平。 1，5-二硝基蒽醌和1，8-二硝基蒽醌是生产分散蓝56、分散蓝73等一系列分散染料重要中间体。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失