反磁性的

To adopt antiphase evaporation transonic method and high speed agitation method to prepare Semustine Magnetic Liposome, to carry out the exosyndrome with TEM, image analysis system and energy spectrometer, to test the envelopment rate of semustine in the liposome.

采用反相蒸发超声法加高速搅拌制备纳米司莫司汀磁性脂质体，用透射电镜、图像分析系统和能谱仪对其进行表征，HPLC法检验脂质体中司莫司汀的包封率。

The Fe3O4 magnetic nanoparticle is a good carrier to prepare medical magnetic liposome. The adoption of antiphase evaporation transonic method and high speed agitation method can prepare nanometer Fe3O4 magnetic liposome.

Fe3O4纳米粒子是制备医用磁性脂质体的良好载体，采用反相蒸发超声法加高速搅拌可制备纳米级Fe3O4磁性脂质体。

The austenite of the alloys possesses strong ferromagnetism, while martensite showes the characteristics of paramagnetism.

奥氏体具有强的铁磁性，而马氏体表现为顺磁或反铁磁性。

Result 1 Magnetic nanoparticles, magnetic nanoparticles modified with antisense oligodeoxynucleotide of human telomerase reverse transcriptase induced HL-60 tumor cells to apoptosis, we could see typical morphologic change of apoptosis cells: karyopyknosis, chromation"s condensing and aggregation in nuclear, forming crescent-shaped or annulus structures to lean on edge of cell nucleus"s membrane and posing apoptosis body by Atomic Force Microscope, Fluorescence microscope, transmission electron Microscope 2 There was a significant difference compared with control group(p.01), inhibition ratio had significant positive correlation with medication dosage and time ;during 0.8-8μM dosage amplitude, inhibition ratio accrescenced by dosages increasing. However, the inhibition ratio would decrease when dosage over 8-80μM.

结果 1 磁性纳米粒子、修饰有端粒酶反义寡核苷酸的磁性纳米粒子诱导HL-60细胞发生凋亡，原子力显微镜、光学显微镜、荧光显微镜和透射电镜下均观察到HL-60细胞呈现典型的凋亡细胞的形态变化：细胞核固缩，核内染色质浓缩、凝聚、形成新月形或环状结构紧靠在细胞核膜边缘，并形成凋亡小体。2 磁性纳米粒子、修饰有端粒酶反义寡聚脱氧核苷酸的磁性纳米粒子对HL-60肿瘤细胞的生长和增殖有明显的抑制作用，与对照组相比有显著性差异(p＜0.01)，在剂量为0.8-8μmol／L范围内，抑制率随剂量的增加而增加，当剂量超过8μmol／L时，抑制率反而下降；3 磁性纳米粒子、修饰有端粒酶反义寡聚脱氧核苷酸的磁性纳米粒子可增强p53基因的表达活性，引起DNA降解损伤，反向调节细胞周期活动，促使细胞从G0期进入G1期，抑制肿瘤细胞的生长。4 修饰有端粒酶反义寡聚脱氧核苷酸的量子点能通过内吞作用进入HL-60肿瘤细胞的细胞核，可以在细胞内进行定位和促进HL-60肿瘤细胞的凋亡。

Theoretical analysis shows that Faraday magnetooptical effect has the anisotropy, and Faraday rotation is depend not only linearly on the magnetization Min paramagnetic and ferromagnetic media or the sublatbee's magnetization Mi in ferrimagnetie and antiferromagnetie media, but also on the high-order terms of M or Mi.

理论分析表明，法拉第磁光效应具有各向异性特性；法拉第旋转不仅与顺磁性和铁磁性介质中的磁化强度M或反铁磁性和亚铁磁性介质中的次晶格磁化强度Mi的线性项有关，而且还应与M或Mi的高次项有关。

Preparation of polymeric nanocapsules by radiation induced miniemulsion polymerization (1) Polystyrene nanocapsules with liquid core were prepared by ~(60)Coγ-ray radiation induced miniemulsion polymerization, in which N-vinyl pyrrolidone was used as polar monomer.

本文首先通过辐射引发细乳液聚合制备了聚苯乙烯纳米微胶囊，并从热力学与动力学两方面研究了影响纳米微胶囊形貌的因素；之后使用反相乳液聚合制备了磁性复合微球和磁性复合空心微球，并研究了有关影响因素。

The main contributions of this thesis are:(1) Seven mononuclear complexes of tetradentate ligand NTB have been obtained using N〓 or SCN〓 as the additional ligand;(2) Seventeen binuclear complexes of Fe , Zn , Co , Cu have been designed and the complexes of Co , Cu exhibit antiferromagnetic properties;(3) Changing the bridged-ligand such as PO〓, CO〓, o-phth, mai, Ag (CN 〓, Au 〓, etc , fourteen tetranuclear complexes of polypridine ligand have been synthesized;(4) Two antiferromagnetic 1D chain complexes of KH〓pdc ligand have been prepared from hydrothermal reactions; in addition, one ferromagnetic 1D chain copper complex of tpdp which is bridged by oxalate has been obtained.

本论文的主要贡献为：(1)合成了配体NTB的七个新型单核配合物；(2)合成了十七个铁、锌、钴及铜系列混桥双核配合物，其中双核钴和双核铜配合物为反铁磁偶合；(3)选用多吡啶配体tpdp和TPA，改变桥联配体，合成了十个四核配合物；(4)选择配体KH〓pdc，采用水热合成方法得到了反铁磁性一维链状锰、铜配合物；以草酸根为桥联配体，合成了配体tpdp的一维链状铜配合物，该化合物为铁磁偶合，文献较少报道。

Compound 6 is a sheet of dimmers, in which two Mn ions are bridged by two EO azides and the dimers are linked by the single EE bridges into a sheet.

磁性分析表明配合物6的二维层内单EE叠氮桥和双EO叠氮桥分别传递反铁磁和铁磁相互作用，但整体表现反铁磁相互作用。

Their formulas are presented as following:( 1 ) [Co2C6H2(COO44]n ( 2 ){[Co2(C2O4)C6H2(COO4(H2O)4] -4H2O-(NH2CH2COOH)}n ( 3 ){[Co(H2O)6][Co(H2O)4C6H2(COO4] . 4H2O}n These coordination polymers have been characterized by IR,UV-VIS-NIR spectroscopes. The variable temperature magnetic susceptibilities(1.5-300K)of complex (1) and (2) have been measured and studied. Complex (1) and (2) exhibit the anti-ferromagnetic property. The spin-transition phenomenon of complex (2) takes place at 17K.

经X-光衍射测定，确定了它们的结构，分子式如下：(1)[Co_2C_6H_2(COO_4_4]_n (2){[Co_2(C_2O_4)C_6H_2(COO_4(H_2O)_4]·4H_2O·(NH_2CH_2COOH)}_n (3){[Co(H_2O)_6][Co(H_2O)_4C_6H_2(COO_4]·4H_2O}_n 研究了上述三种配位聚合物的红外，紫外—可见—近红外光谱，测定了化合物(1)和(2)在1.5—300K温度范围内的变温磁矩，对它们的磁性研究表明，化合物(1)和(2)均呈反铁磁性，并且化合物(2)在17K发生了自旋转换现象。

For the chemical shifts of the carbons that lay in the conjugated sketeton we obtained a good linear relationship between the calculated and experimental data as well as their antimagnetic contribution σ_d and electronic density ρ.

对于固定在π骨架上的碳原子，其化学位移计算值与实验结果有很好的线性关系，并且它们的反磁性贡献σ_d和电荷密度ρ之间也有较好的线性关系。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。