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Chiral compounds Ⅰ for the first time was applied to allylation of acylhydrazones with allyltrichlorosilane and the results showed that the compound Ⅰ can contribute to the occurrence of the reaction.

首次将手性化合物Ⅰ应用于烯丙基三氯硅烷和酰腙的烯丙基化加成反应中,结果表明化合物Ⅰ能够促进该反应的发生。

Reaction (1) was examined with different kinds of acetal substrate(1) and vinyl ethyl ether, and the results indicated that the 1, 1,3-triethoxy compounds could be obtained in high yields of 88 and 97% respectively when the R groups of the acetal are phenyl and anisyl, while the yields amounted only to 55-75 % for R=a...

有证据表明这种催化反应也可能是通过正碳离子中间体进行的。本反应的产物1,1,3-三乙氧基化合物经乙酸/乙酸钠溶液水解可得反式α,β-不饱和醛。水解产率:芳香族产物大于90%,脂肪族产物大于75%。

Establishment of RAPD Reaction System of Aquilaria agallocha Roxb.

目的对影响沉香随机扩增多态性DNA反应的各因素进行优化,建立适用于沉香RAPD的最佳反应体系。

The response patterns were analyzed and categorized. The prolonged asystole was searched. Follow up was made at the outpatient clinic or by phone during October 2004. Two hundred forty-two patients (40.1%) had positive response. 172 patients (71.1%) with the mixed type, 60 patients (24.8%) with the vasodepressive type and only 10 patients (4.1%) with the cardioinhibitory type.

反应的型态皆加以分析及归类并寻找有长的心跳停止者而於2004年十月於门诊或电话做追踪。242位病人(40.1%)为阳性反应,其中172位(71.1%)为混合型,60位(24.8%)为血压下降型,而仅有10位(4.1%)为心跳抑制型。

Two kinds of products can be obtained in the addition reaction of benzaldoxime with propinol, in which 3-hydroxymethyl-dihydroisoxazol is the main product when reaction equilibrium is reached.

炔丙醇的两种取向对应着加成反应的两种产物,反应达到平衡后, 3-羟甲基二氢异噁唑为主要产物。

In this thesis, the three series of P, O and P, N bidentate ligands chelated palladium complexes £40-46} were designed and synthesized for Suziki cross-coupling reaction.

研究了它们对Suzuki偶联反应的催化作用,优化了这些催化剂在联苯类化合物合成中的反应条件。

Eighteen SSR primer pairs were designed and synthesized.The factors which affected on the SSR reaction of Toona ciliata var.

利用所合成的引物优化SSR反应体系,对影响SSR反应的各个因子进行了探讨。

The activation energies were highly pH-depended and decreased very sharply as the pH went up from 6. 0 to 11. 0 or down from 6. 0 to 2. 0.The stability of Gln residues in peptides or corn protein was the most at pH6. 0.At pH 6. 0, the rate constants of deamidation were the lowest, and their half-life and Arrhenius activation energies were the highest.

过酸或过碱都将增加脱酰胺反应的速率,动力学结果表明,pH6.0时最为稳定,表现为pH6.0时的脱酰胺反应速率常数最小、半衰期最长、活化能最大。

Solvent effect on the Diels-Alder reaction was analyzed with four different kinds of solvents: benzyl alcohol, cyclohexanone, toluent and decalin. The results show that the rate of the Diels-Alder reaction increased in more polar solvents and stereoselectivity of TCPD decreased.

在模拟计算基础之上,选择苯甲醇、环己酮、甲苯及十氢萘四种溶剂进行Diels-Alder反应的溶剂效应研究,考察温度、压力变化对反应速度、产物立体选择性的影响。

The two rate equations fitted the experimental data well,as was confirmed by the reaction of bis(4-carboxyphenyl)phenyl phosphine oxide with ethylene glycol under constant reaction temperatures of 180197℃ and at different ratios of diol to diacid,whose rate constant and activation energy were calculated.

将这两个速率方程应用于双苯基氧化膦与乙二醇的恒温自催化聚酯化反应,计算值与实验数据相一致,并计算得到了该反应的速率常数和活化能。

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