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High reaction performance and decoking ability were obtained in gas-phase oxidative cracking of decalin , as compared with its pyrolysis reaction.

十氢萘气相氧化裂解与传统的热裂解工艺相比,O2的存在降低了十氢萘 GOC反应的活化能,使反应在较低温度下具有高的反应性能;O2同时起到消除积炭的作用,提高体系的抗积炭能力。

The Schiff base transitional metal complexes of various structures and their metallomicelles as peroxidase models for the phenol and phenolic derivant oxidation have been investigated. Some results are obtained from the studies:(1) the Schiff base transitional metal complexes have high catalytic activity for the phenol and phenolic derivant oxidation, and the structure of the complexes has a great effect on its catalytic activity;(2)a novel kinetic mathematical model for the complexes and their metallomicelles catalyzing the phenolic derivant oxidation has been established;(3) the feasibility and mechanism for the phenolic derivant oxidation catalyzed by the metallomicelle(as the mimetic model of peroxidase)have been discussed.

研究了冠醚Schiff碱金属配合物作为过氧化物酶的模拟模型对酚类物质氧化反应的催化作用,取得如下结果:(1)几种冠醚Schiff碱金属配合物对催化酚类物质氧化具有良好的催化活性,其中配体结构对其催化活性有较大的影响;(2)建立了金属配合物与表面活性剂形成的金属胶束催化酚类物质氧化反应的动力学数学模型;(3)探讨了金属胶束模拟过氧化物酶催化酚类氧化反应的可行性及其机理。

The kinetic behaviors of ethylene homo- olymerization and ethylene / l-hexene co-polymerization , catalyzed by the metallocene catalyst PS-DVB-MC in an 0.5 L stainless steel reactor , were studied. The effects of polymerization conditions on ethylene polymerization , such as concentration of catalyst , temperature of polymerization , pressure of ethylene , molar ratio of AI / Z r , etc ., were also investigated . Some leading results were as follows : the activity of the catalyst PS–DVB- MC for ethylene homo-polymerization was high ( 1.053 x 107 gPE / mol Zr·h ), but the molar ratio of AI / Zr was low ( 350:1 ); the catalytic ability for ethyleneα-olefin ( such as l hexene etc .) co-olymerization was great , and the corresponding activity come up to a maximum of 1.753 x 107 gPE / mol Zr·h while concenlration of l-hexene was 0.080 mol / L ; the molecular weight of polyethylene was about 180,000 , meanwhile the molecular weight distribution was narrow ( 2.19 ); the bulk density of polyethylene and ethylene / l-hexene co -polymer were 0.25 and 0.34 respectively .

采用0.5L高压不锈钢反应釜,对催化剂PS–DVB-MC催化乙烯均聚和乙烯/ l-己烯共聚合的动力学行为进行了研究,详细考察了催化剂浓度、反应温度、压力、Al/ Zr比、1-己烯浓度等因素对乙烯聚合反应的影响,得到如下主要结论:催化剂PS-DVB-MC具有催化乙烯均聚的高活性(1.053×107g PE / mo1 zr.hr),低Al / Zr比( 350:1 );具有良好的催化乙烯与α-烯烃(如1-己烯等)共聚的能力,在1-己烯浓度为0.080 mol / L时,催化活性达到最大(1.783×107 g PE / molZr.hr);乙烯均聚产物的分子量在18万左右,分子量分布窄( 2.19 )。

The result indicates that the intracortical synaptic input was unchanged, but the thalamocortical synaptic input was depressed by sensory stimulation and this depression recovered with a time course that matched that of the recovery of sensory responsiveness.

结果表明,电刺激诱导出的皮层—皮层突触反应不受持续的触须刺激的影响,而电刺激诱导出的丘脑—皮层突触反应则由于持续的触须刺激而减小,而且突触反应的恢复时程与皮层细胞适应恢复的时程类似。

The relative stabilities and probable proton transfer in isolated and monohydrated 2-hydroxyimidazole molecules have been studied in gas phase using ab initio (MP2/6-31+G *) method.

采用从头算方法在MP2/6-31+G*水平上研究了2-羟基咪唑分子在孤立分子和一水合物的异构体的相对稳定性和可能的质子迁移反应,分析了一个水分子的参与对2-羟基咪唑分子异构体的相对稳定性和质子迁移速率的影响,采用Monte Carlo模拟方法研究了反应体系在水溶液中反应的溶剂化效应。

Four different ionic liquids, BF4, BF and PF6 were investigated, arid PF6 showed the best effect when used as the reaction media, giving the highest yield in the shortest reaction time. Promoted by KF in PF6, N-aryl or N-alkyl monosubstituted sulfonamides could react with various activated halides and unactivated primary halides smoothly. Reactions were performed at 85℃ for 2~10 hours, and thirteen N-alkylation products were obtained with 70%~97% yields. Moreover, the ionic liquid recovered could be reused for three times with no appreciable decrease in yield and reaction rate.

结果表明,以PF6为反应介质时显示出了最好的效果,反应的时间最短,收率最高。N-芳基或N-烷基单取代的磺酰胺和各类不同结构的活化的卤代烃和未活化的一级卤代烃在PF6中KF作用下,85℃反应2~10h,以70%~97%的优良收率得到了13个N-烷基化产物,而且离子液体回收使用3次后效果未降低。

The key problem for limb , skin or other composite tissues transplantation is to control posttransplantation rejection , which encumbers long term functional survival of transplanted organ and tissues .

作为皮肤复合组织移植的受者,术后出现排斥反应的几率很高,排斥反应发生的程度和频率将直接影响移植组织能否长期存活及功能能否及时恢复,而免疫抑制剂的个体化用药是否合理又直接影响术后免疫排斥反应发生的频率和程度,因此为受者&量体裁衣&制定免疫抑制剂术后个体化给药方案,是保证移植组织或器官有功能性的长期存活的关键因素之一。

The vibration energy or the electronic and vibration entropy of the gaseous molecules are approximately used as the energy or entropy of the solid. In this approximation, thermodynamic functions 、、 and hydrogen isotopes equilibrium pressure of the hydrogenating reaction have been calculated .Then we can fit the relations between temperature and equilibrium pressure.

在ZrH2的E和S的过程中,以气态分子总能量中的振动能EV代替该分子处于固态时的振动能量E,以电子和振动熵SEV代替分子处于固态熵的近似方法,计算了不同温度下金属Zr与氢同位素反应的,和以及氢化反应平衡压力,并导出了氢化反应平衡压力与温度的关系。

Some prescribes about the test method of alkali aggregate and alkali-aggregate reaction have been shown in the regulations of geologic reconnoitering and the test method of the hydraulic concrete.

中国已建的混凝土大坝中,有些也含有一定量的碱活性骨料,但由于采用了低标号水泥和大量的活性混合材,因此至今未发生碱骨料破坏反应;但也有个别工程,虽经碱骨料反应的检测,并采用了一定的抑制措施,但运行20年后,在大坝溢流面混凝土中出现了碱骨料反应的微观和宏观裂缝破坏。

There are three different nucleophilic reagent respectively reaction with m-dinitrobenzene ramification at distint alkaline term:With the nitrobenzene 、 m-nirtobenzenesulfone sodium salt 、 2.4-dinitro chlorobenzene 、 m-dinitrobenzene for bottom thing, benzyl cyanide、 benzyl chloride、 benzyl chloropyridine、is a nucleophilic reagent reaction for under the different term proceeds a series reaction. At the same time ,discuss about the impact factor to nucleophilicity such as the number of attract electron group、 ability of attract electron and the nucleophilic substitution reaction part.

设计了三类不同的亲核试剂分别与活化芳环在不同的碱性条件下发生反应:以苄基氰、苄基氯化吡啶为亲核试剂,以硝基苯、间二硝基苯、间硝基苯磺酸钠、2,4-二硝基苄基氯为底物进行亲核取代反应;并且对亲核试剂的体积效应、溶剂效应对亲核性影响,底物上吸电子基团的数目、吸电子能力对亲电性的影响,以及亲核取代反应的发生部位受哪些因素影响进行探讨。

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She gently rebuff ed him, but agreed that they could be friends

她婉言拒绝了,但同意作为朋友相处。

If in the penal farm, you were sure to be criticized.

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