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Originally limited to dialkylamino methylenation, the application of Mannich reaction has been expanded much further in recent years to a wide variety of monosubstituted amines, amine equivalents and amides. In addition, a variety of Aza-Mannich and Mannich-Michael methodologies have emerged.

最初该反应的应用范围仅局限于二烷基胺亚甲基化反应,近年来才得到了长足的发展,其研究范围扩展到单取代的胺、胺的类似物以及酰胺等化合物,并发展形成Aza-Mannich和Mannich-Michael等复合Mannich反应。

The same methods were used to study toluene dinitration, and the results indicated that the thermal runaway risks of these reactions were low too; prolonging dosing duration was helpful to the conversion of all nitrotoluene; decreasing the molar ratio of nitric acid to mononitrotoluene would make an insufficient conversion; among the given temperatures, rising reaction temperature couldn\'t markedly change the yield coefficient, but lead more heat generation and higher thermal runaway risk.

采用同样的方法对二段硝化反应进行研究,结果表明:二段硝化反应的热失控危险性也较低;延长加料时间,有利于反应完全;而随着硝酸与一硝基甲苯摩尔比的减小,硝化难以进行完全;在选定温度范围内升高温度,产物得率无显著变化,反而易导致放热加剧,增加体系的热失控危险。

Thepotential energy surface of these reactions were plotted, and the energy barrier of the reaction between THF and secondary oxonium ion was determined to be 182.0.116 kJ/mol.

本文进一步对四氢呋喃阳离子开环聚合反应过程中,氧鎓离子与水反应的机理进行了分析。

The appropriate conditions of polyaminating reaction was that oxycellulose chloride in 200mL DMSO was heated to 100℃with stirring,then was dropwised 10mL A2.3 and A3.4 separately,remaining the temperature for 12h,after pH was justed to 4-5,the products were obtained in 46%yield.

确定多胺化反应的较佳条件:在200mL DMSO搅拌加热至100℃,滴加A2.3和A3.4各10mL,维持温度反应12h,在酸性条件(pH:4-5)下生成,产率大约在46%左右。

At the same time, we found that the aggravation of patients' jointpain was correlate with the enhancement of lipid peroxidate reaction when the weather changed bed.

提示机体脂质过氧化物反应增强可能是气象变化引起某些RA息者出现关节不舒或疼痛加重反应的主要因素之一。

Their photostability were determined in DMF solutions under li...

在实验时间范围内,其光褪色反应遵循一级反应的规律,且光褪色速度很小。

Objective] The experiment aimed to determine the optimum ISSR-PCR reaction system of Picea crassifolia kom..

[目的]确定适应青海云杉ISSR-PCR反应的最佳反应体系。

Now, a convenient, efficient pinacol coupling of aldehydes mediated by zinc in good yields has been carried out in ammonia water in the presence of a little crown ether. Adding a small amount of crown ether was highly effective to enhance the yields of pinacol from 63% to 84%.

本文报道一种简便、有效的水相呐偶合反应,它是在含有少量冠醚的稀氨水溶液中,使用锌粉促进醛基化合物进行水相呐偶合反应,其中加入少量的冠醚有助于提高反应的产率,呐醇产率由63%提高到84%。

Nevertheless, the yield of pinacol was also strongly affected by the steric environment surrounding the carbonyl group. The pinacol coupling of aromatic aldehydes has been achieved with high yields under such a condition. However, the diastereose-lectivities of pinacols were not satisfying. Unfortunately, the ketones and most aliphatic aldehydes appeared inert under the same reaction conditions.

然而, 呐偶合反应的产率受到羰基周围环境的立体位阻影响较大,在此条件下,锌粉能有效地促进芳香族醛类化合物进行水相呐偶合反应,得到的呐醇产率高,但非对映异构体选择性差,而脂肪族醛类化合物得到的呐醇产率较低,在同样的条件下,酮类化合物不能顺利进行呐偶合反应。

Preliminary Study on Enzymatic Modification of Protein──Study on Plastein Reaction of Soybean Protein with Sesame Protein;2. Utilizing alkaline hydrolysate of rice protein as substrate,the effect of plastein reaction condition on the yield of plastein was studied.

以大米蛋白的碱性蛋白酶水解产物为原料,研究了反应条件对类蛋白反应产率的影响,采用正交试验优化了类蛋白反应的条件,并分析了最佳条件下类蛋白的氨基酸组成。

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