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The formation mechanism of titanium nitride powders by reduction of carbon and nitridation was researched by method of continuous weighing.

用连续称重法研究了钛白粉被活性碳还原氮化合成氮化钛粉末的还原氮化反应机理,并进行了反应的热力学、反应产物的显微结构以及X-ray衍射分析。

Experimental results showed that, in this process, the optimal pH of the shortcut nitrification was 8.0~8.5; when the pH was less than 6,the nitrification is completely inhibited; when the pH was 6~7, at the end of aeration, the Nitrobacteria become the dominant bacteria because of the dropping of the free ammonia concentration. It is known to all, the activity of the Nitrobacteria and Nitrosomonas was affected by FA concentration, so nitrification was affected by FA concentration. According to the author's research results, the FA concentration which inhibit the Nitrobacteria was below 1.0mg/L,which inhibit the Nitrosomonas was above 10mg/L.

实验研究结果表明:本工艺中,短程硝化反应的最佳pH值在8.0~8.5之间,当pH小于6时,整个硝化反应都会受到抑制,当pH在6~7之间时,随着游离氨浓度的降低,在曝气后期,硝化菌将会占据优势;FA浓度对短程硝化反应的影响是通过对亚硝酸菌和硝酸菌的抑制来实现的,在本研究条件下,游离氨对亚硝酸菌的抑制浓度在10mg/L以上,对硝酸菌的抑制浓度在1.0mg/L以下;温度对短程硝化反应的影响是双重的,既影响微生物的生理活性,又影响FA浓度。

The dechlorination of the chlorinated hydrocarbon by electrolytic iron is based on the laws of redox reactions,the adsorption of the pollutants by tiny granular activated carbon among the iron filings ,the catalytic process of the tiny granular carbon,the destruction of the oxidational membrane on the iron surface by the active chloride ion and the effect of the tiny electric fields.

简述了氯代烃的主要物理性质和用途,认为铁屑腐蚀电池处理氯代烃污水是基于氧化还原反应、铁屑中活性炭微粒对氯代烃的吸附与对反应的催化、氯离子对氧化膜的破坏和微电池的电场效应等原理;简要总结了迄今利用铁屑去除氯代烃的室内实验和利用原位铁屑反应墙处理地下水中的氯代烃污染研究所取得的成果,认为这种反应墙是一种效果好、成本低、维护方便、有望投入商业运行的最佳方法,并指出了其存在的问

The transition states of the reaction between THF、 butylene oxide and secondary oxonium ion were acquired. By using frequency analysis and inner reactioncoordinate analysis the rationality of these transition states were affirmed.

分别对四氢呋喃和环氧丁烷,绘出了链增长反应的势能面曲线,得到四氢呋喃链增长反应的活化能为116.749kJ/mol;环氧丁烷链增长反应的活化能为92.672kJ/mol。

These two PESs may have two possible spin crossings at entrance and exit channels, respectively, and the minimum energy path is suggested to be 〓〓〓 H〓O.

OsO〓与甲烷的脱水反应机理此反应的极小能量反应路径只与四重态和二重态两个自旋态的势能面有关。

Moreover, nano-scale SiO〓 particle is as seed, styrene-acrylate-acrylic acid emulsion polymerization and soapless acrylic emulsion are studied from varying the level of SiO〓 particle and reaction temperature, particle size of these emulsions are determined and SiO〓 content of participating polymerization is also determined. Kinetic study is carried out in the presence of nano-scale SiO〓 particle.

此外用原位聚合法制备了纳米SiO〓/苯乙烯-丙烯酸酯复合乳液和无皂丙烯酸乳液,研究了不同SiO〓含量、反应温度等对聚合反应稳定性的影响,测定了所得乳胶粒的粒径,分析了在乳液中SiO〓含量,并进行了在SiO〓存在下乳液聚合反应的动力学研究。

Conductivity of Polyoxyethylene/Poly (2-vinyl pyridine)Blend and Compatibilizing Effect of Lithium Perchlorate;2. Graft terpolymerization of polyoxyethylene macromer with acrylates;3. Then multiblock copolymers was obtained by condensing polyoxyethylene and poly(2 vinylpyridine)with dichloromethane in the presence of potassium hydroxide.

甲基萘锂作为引发剂利用阴离子聚合得到 2 乙烯基吡啶的遥爪双羟基低聚物(P2VP),然后以二氯甲烷作偶联剂与聚环氧乙烷反应制备P2VP和PEO多嵌段共聚物,考察了反应时间对偶联反应的影响,并对共聚物进行了IR和1H NMR表征,由1H NMR谱的积分曲线得到了共聚物中PEO链段质量分数。

The influence of water content,molar ratio of methanol to oil,concentration of alkaline catalyst,reaction temperature and time different reaction factors to transesterification ,and methods such as water washing,acid washing,extraction and pressure reduced etc.

考察了原料油水分含量、醇油物质的量比、催化剂浓度、反应温度、反应时间等对转酯化反应的影响,以及水洗、酸洗、萃取、减压蒸馏等不同后处理方法对产品品质的影响。

This paper investigates the catalysis of D-72 strong acid cation exchange resin on the synthesis of acetals,and systematically discusses the influence of reaction factors on the catalysis reaction.

研究了强酸性阳离子交换树脂对缩醛合成反应的催化作用,系统地探讨了各反应因素对反应的影响,研究发现,D-72强酸性阳离子交换树脂具有较高的催化活性,并能重复使用。

It had already been used in preparing the immobilized catalyst for heterogeneous hydrogenation of olefins,[17] in desulfurization of simulated flue gas,[18] and particularly in the reactions between aldehydes or acetones and the compounds with active hydrogen, such as Henry reaction[19] and direct aldol reaction.

16它已被用于制备烯烃非均相加氢反应的固定相催化剂,[17]烟气脱硫,[18]并且特别地被用于醛或酮和含活泼氢的化合物之间的反应,例如Henry反应[19]和直接羟醛缩合。

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