反应的

When the nucleophile was alkanol, the reaction proceeded smoothly in the room temperature to give 6- alkoxyl pyrazolo[3,4-d]pyrimidin-4(5H)-ones.

并分离出了部分反应中间提胍，提出可能的反应机理，对这种反应的选择性进行了解析。

This article analyzed nucleophilic substitution mechanism of amidation reaction which was the key step in new process, the effect factors such as catalyst type, catalyst volume, solvent and temperature were also involved.

其中酰胺化反应是关键步骤，文章分析了该反应的亲核取代机理及催化剂种类、催化剂用量、溶剂、温度等条件对反应的影响。

This process can be carried out in an atomically economic way from the viewpoints of both material and energy utilization, which could significantly improve the efficiency of the process.

加氢和脱氢耦合法可将加氢反应的放热用于脱氢反应的供热，减小了过程的热效应，可有效避免反应器的局部过热或过冷；脱氢反应释放的氢可用于加氢反应，整个过程无氢消耗，具有能量和原子的经济性，显著地提高了整个过程的效率。

The results obtained by the proposed method in the bilirubin calibrator and control Sample were in good agreement with the target values.

为减少间接胆红素在DB测定中的反应，常规分析采用反应Indn后中止反应的方法。

Stable Vitamin K 3 is synthesized by addition reaction of raw materials of niacinamide, chlorhydric acid and menadione sodium bisulfite at 25℃.

以烟酰胺、盐酸为原料，在 2 5℃反应得烟酰胺盐酸盐溶液，而后与亚硫酸氢钠甲萘醌发生加成反应，反应的物料配比为：n ∶ n ∶ n =1∶1.2 ∶1.2 5 ，得到稳定的复合维生素K3 ，收率 95 %。

In acetic acid and using cobaltous acetate as catalyst m-chlorobenzoic acid was synthesized by the reaction of m-chlorotoluene with oxygen.

在醋酸溶液中，醋酸钴为催化剂，以间氯甲苯、氧气为原料合成间氯苯甲酸，分别研究了反应温度、反应时间、原料配比、催化剂的用量等条件对合成反应的影响，确定了最佳工艺条件。

In this catalyst system, the Knoevenagel condensations of a series of aromatic aldehydes with malononitrile or ethyl cyanoacetate were programmed and a mechanism was postulated as well. When aromatic aldehydes reacted with ethyl cyanoacetate, the corresponding alkenes proved to be E-isomers by 1H NMR.

在该反应体系中考察了一系列芳香醛和丙二氰、氰基乙酸乙酯的缩合反应，并推测了Knoevenagel缩合反应的机理，芳香醛与氰基乙酸乙酯缩合产物经1H NMR检测为E式烯烃。

The related reaction conditions and factors such as catalysis of some catalysts etc were discussed. In the procedures, 2-pentylidene cyclopentanone intermediate, which could be isomerizated into a 2-pentyl cyclopentenone under acidic conditions, was effectively prepared in the presence of a phase transfer promotor.

讨论了正戊醛和环戊酮在碱性条件下缩合生成2-亚戊基环戊酮的反应温度、碱浓度、相转移催化剂等因素对反应的影响。2-亚戊基环戊酮中间体化合物能在酸催化剂作用下，异构成2-戊基环戊烯酮，其中酸浓度和溶剂等参数对反应影响明显。

After this research work, we know that: HMCM-22 is a better catalyst of selecting naphthalene alkylation; Surface modification of zeolite Y is effective, but the effect of zeolite 3 is not evident and surface modification doesn"t suits mordenite; Surface modification doesn"t affect the frameworks and inner environments of zeolites, but only reduces diameter of orifice and overlays surface acidities; t-butanol is not suitable for alkylating agent of the reaction using modified zeolites as catalyst; Solvents with smaller molecular size are advantageous for naphthalene alkylation reaction using modified zeolites as catalyst, such as cyclohexane is better than decalin.

通过本论文的研究，我们知道：HMCM-22是萘择形烷基化反应较好的沸石之一；Y沸石的外表面改性效果较好，β沸石则效果不明显，而丝光沸石则不适于外表面改性；外表面改性不改变沸石的骨架结构和孔道内部环境，仅减小孔口直径和覆盖外表面酸性位；叔丁醇不适于作外表面改性沸石催化的反应的烷基化试剂，其反应活性很低，且选择性无明显提升；分子较小的溶剂更适于外表面改性沸石催化的反应，环己烷就明显好于十氢萘。

The sodium dithiobenzoic acid was oxidized with potassium ferricyanide to obtain di disulfide.The influences of raw materials mole ratio,stirring method and reaction time on the yield were studied with orthogonal test.

用铁氰化钾溶液氧化二硫代苯甲酸钠，得双二硫代苯甲酰，采用正交实验探讨了4，4'-偶氮双(4-氰基戊酸)与双二硫代苯甲酰反应的投料比、搅拌方式、反应时间对反应收率的影响。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失