反应的

The temperature and the addition of surfactant can accelerate conversion and selectivity of reaction. Under the conditions of 200℃、0.38MPa、0.06 mol/L、t=4h,the conversion of hexene is 86.32%.Selectivity of 2-hexene and 3-hexene is 30.46% and 57.86%.

结果表明，当表面活性剂的加入以及反应温度的升高，能明显提高反应的转化率和选择性，在200℃、0.38MPa、0.032 mol/L的反应条件下，反应4小时底物转化率为86.32%，3-己烯的选择性为57.86%，2-己烯的选择性为30.46%。

This paper focuses on the stability study of Rhizopus oryzae IFO4697 when used for the methanolysis of renewable oils for biodiesel production. The results showed that water content was important for achieving high catalytic activity and good stability of the biocatalyst. The optimum water content was found to be 5%-15%. Both particle size and desiccation methods showed no obvious effect on the stability of the biocatalyst. With GA cross-linking pretreatment, the stability of the biocatalyst could be improved significantly. When Rhizopus oryzae IFO4697 repeatedly used for next batch reaction, direct vacuum filtration was found to be a good way for the maintenance of good stability of the biocatalyst.

本实验对固定化全细胞Rhizopus oryzae IFO4697催化植物油脂合成生物柴油的稳定性进行了系统地研究，结果表明：反应体系水含量对于全细胞催化剂的反应活性和催化稳定性有重要影响， 5%~15%含水量适宜；研究范围内，载体粒度及干燥方式对稳定性影响不显著；经过戊二醛交联后，全细胞催化油脂甲醇解反应的稳定性显著提高， 1200 h反应后，仍然可以保持75%的生物柴油得率；真空抽滤直接回用的方式有利于稳定性的保持。

Recent developments of clean oxidation systems catalyzed by polyoxometalates are summarized in detail. The emphasis is on the epoxidation reaction of olefinic compounds, oxidation of alkanes and aromatic compounds with the comparatively ideal oxidants, hydrogen peroxide and molecular oxygen respectively.

文本总结了多金属氧酸盐在液相清洁催化氧化方面的进展，主要针对以过氧化氢和分子氧为氧化剂的烯烃类化合物的环氧化反应、烷烃和芳香族化合物的氧化反应，并详细探讨了此类氧化反应的反应机理。

Recent developments of clean oxidation systems catalyzed by polyoxometalates are summarized in detail. The emphasis is on the epoxidation reaction of olefinic compounds, oxidation of alkanes and aromatic compounds with the comparatively ideal oxidants, hydrogen peroxide and molecular oxygen respectively. The oxidation mechanisms are elucidated in detail.

文本总结了多金属氧酸盐在液相清洁催化氧化方面的进展，主要针对以过氧化氢和分子氧为氧化剂的烯烃类化合物的环氧化反应、烷烃和芳香族化合物的氧化反应，并详细探讨了此类氧化反应的反应机理。

Results:All dosage groups of Tou-Yu-Tong Pills could release chronic nerve injury caused by formaldehyde solution; remarkedly inhibit the pain of mice in the formalin test and prolong the latencies of paw-licking. It could significantly diminish pain caused by glacial acetic acid ,reduce the number of the writhing in mice.To the model of migraine ,Tou-Yu-Tong Pills can improve the content of 5-HT in brain tissue of mice ,and ruduce 5-HTAA.

结果 头愈痛丸对福尔马林致小鼠慢性神经性疼痛反应，能明显减少动物舔后足的时间，改善其伤害性疼痛行为反应；对冰醋酸致小鼠扭体反应，能显著延长扭体的潜伏期，减少扭体反应的次数；对小鼠偏头痛模型，能显著升高小鼠脑内5-HT的含量，且降低5-HIAA的趋势。

In the interfacial layer near to SiC, elements Pd and Ni preferentially diffused to SiC and resulted in the reaction products of Pd-Si phase, Ni-Si phase and graphite. In the reaction zone further away from the SiC, mainly elements Cr and V in the brazing filler participated in the interface reaction, and formed Cr-C, Cr-Si, Cr5Si3C. In the central part of the joint, the matrix was composed of Pd-Si, Ni-Si and V-Si phases, on which some blocky carbides V2C, Cr23C6 distributed scatteringly.

MPa。微观分析表明，在靠近SiC的界面反应层中，主要是Pd和Ni优先与SiC反应生成相应的Pd-Si相，Ni-Si相和石墨；接头中在离SiC稍远的区域，主要是Cr和V与母材扩散进入钎缝且未与Pd和Ni反应的C和Si发生反应，生成Cr-C， Cr-Si， Cr5Si3C 等相；钎缝中心区的基体由Pd-Si，Ni-Si和V-Si相组成，其上弥散分布着块状碳化物V2C和Cr23C6。

In range of 300℃～900℃, all the transition metal oxide catalysts could get high ammonia conversion, during the initial stages of the reaction, the SO〓 conversion is relatively low since the catalysts have not been sulfureted, but it increases gradually and attain constant with rising temperature and time continuance,〓 is better than other catalysts in reactivity and elemental sulfur selectivity; XRD indicates that, in the SO〓-SCR process, stable transition metal sulfide is generated which is very important to SO〓 reduction and transition metal sulfide probably is the active phase of catalyst, further the reduction of SO〓 by H〓 to H〓S is the limiting step of all process, then the activity is somewhat related to its lattice oxygen yet not so notable; XPS indicates that little sulfur on surface exists as S〓 in sulfate, showing that TiO〓 could restrain the generation of sulfate.

对于过渡金属氧化物催化剂的研究发现，在300℃～900℃范围内，不同的催化剂均可获得很高的NH〓转化率，反应初期由于催化剂还未硫化，所以SO〓的转化率较低，随着温度升高和反应时间的延续，SO〓的转化率逐渐升高并达到了稳定值；七种过渡金属氧化物中，以〓对于NH〓还原SO〓反应的活性和选择性最好；XRD结果表明在NH〓-SO〓反应后生成了稳定的硫化物相，硫化物对SO〓的还原过程具有重要作用，催化剂的活性相可能是过渡金属硫化物，而且在硫化物催化剂上进行的H〓还原SO〓生成H〓S的反应是整个过程的速率控制步骤，所以催化剂的活性与其自身的晶格氧的氧化还原能力有一定的联系，但关系不明显；XPS结果表明催化剂表面的硫大部分以过渡金属硫化物的形式存在，只生成少量的S〓，说明TiO〓催化剂能够较好的抑制硫酸盐的生成。

Adopted with the study mode of Reaction Times and the technique of Event-related Potentials, the paper compared the difference of the reaction times, accuracy rate,latency,amplitude of ERP components of athletes and undergraduate students during the process of choice reaction to stimuli which were presented at different field of vision, in order to explore the variety characteristics of brain nerve activity of spatial perception of athletes.

采用反应时研究范式和事件相关电位技术，通过比较运动员与普通大学生对不同视野刺激进行知觉选择反应的反应时间、反应准确率及所诱发的ERP成分的潜伏期和波幅的差异，来揭示对抗性项目运动员空间知觉的脑神经活动变化特点。

With change of calcium sulfate shape and reduce of compact degree of coat layer on phosphate rock, the velocity of second stage reaction of SSP is accelerated by active addition agent, and with intensification of mass transfer, the rate of first stage reaction of SSP is promoted by ultrasonic.

活化添加剂促进酸矿反应的重要途径是改变硫酸钙结晶的晶习，减弱硫酸钙对磷矿包裹的致密程度，特别表现为对第二阶段的反应十分有利，而超声波对酸矿反应的促进主要表现为提高第一阶段反应的传质过程强度。

Glycidyl benzoate,glycidyl propionate,glycidyl acetate were obtained respectly through a phase-transfer catalytic methodology using sodium benzoate, sodium propionate, sodium acetate and epichlorohydrin as raw materials, and pure products were obtained though vaccum distillation.β-cyclodextrin and glycidyl benzoate, glycidyl propionate, glycidyl acetate, reacted in organic solvent and goal product were

先以苯甲酸钠、乙酸钠、丙酸钠和环氧氯丙烷为原料在相转移催化剂的作用下分别合成了苯甲酸缩水甘油酯、乙酸缩水甘油酯和丙酸缩水酯，经过减压蒸馏，得到相应的纯品；β-环糊精和苯甲酸缩水甘油酯、乙酸缩水甘油酯、丙酸缩水甘油酯在有机溶剂中反应，经过硅胶色谱柱分离，得到了相应的产品，产品经过TLC、IR、1H NMR、MS表征，并研究了温度、反应时间、催化剂等几个因素对反应工艺的影响，结果表明温度和催化剂对反应的快慢有较大影响。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失