反应的

And when using benzene as solvent, amorphous phosphorus nitride imide were obtained, which were consisted of microtubes, hollow balls, solid balls and square frameworks. Through adjusting reaction time and temperature, the morphology of the samples was well controlled.

进一步引入苯作为反应的溶剂，在高压反应釜中在190-250℃反应得到了由微管、空心球、实心球和四方框组成的非晶HPN〓，并通过调节反应时间和温度使产物的形貌得到了很好的控制。

According to the electrophilic substitution of α-Allocryptopin by ICl, it can be suggested that there are competitions of n-donors (such as N and O atom occurred in alkaloid or solvent molecules) with the conjugated π system in alkaloid molecule for iodine monochloride when charge-transfer complexes are formed, which may block the formation of pre-reactive π-complex intermediate, and thus suppress the electrophilic substitution.

这一方法标记过程简便，标记产物富集于有机相，易于进一步纯化，其放射化学纯度接近95%，标记率超过70%；ICl与α-别隐品碱的亲电碘化反应结果表明，生物碱底物或溶剂分子中的N、O等n电子给体可能与亲电试剂形成电荷转移络合物，竞争芳香亲电取代反应π络合物反应前体的形成，从而抑制碘化反应的发生。

The experimental results show that the content of SiC in RBSC increases with carbon content while α-SiC is chosen as a filler. However, the residual carbon would appear in specimens when the carbon content exceeds 30% by weight. Using carbon felt, the reaction-formed SiC particles are small and uniform in size and distribution. However, when carbon felt is impregnated with phenol resin, the reaction-formed SiC is nonuniform in size and distribution. X-ray diffraction shows that the fabricated RBSC is composed of α-SiC,β-SiC, and free Si. The polytype of SiC is related to the reaction-heat during sintering.

结果表明：选用α-SiC+C粉的混合物作为生坯，SiC相的体积分数随生坯中wC的增加而增加，但过大的wC将使硅化后的试样出现残碳；选用碳毡作为生坯，反应烧结碳化硅的显微组织特点是C／Si反应生成的碳化硅颗粒均匀细小，并呈线状分布在游离硅中；浸渍过树脂的碳毡硅化处理后的显微组织特点是反应生成的碳化硅颗粒粗大且呈不均匀分布。X射线衍射结果也表明，反应烧结碳化硅陶瓷由游离Si、α-SiC、β-SiC组成，试样中不同晶型碳化硅的出现与C／Si反应的放热过程有关。

Some research and analysis on the reaction of 2,4-difluoronitrobenzene and nucleophilic reagent alcohol sodium (methyl alcohol ,ethyl alcohol, propyl alcohol, n-butyl alcohol, t-butyl alcohol, et hl) and the reaction choice of opposite -F in different solvent and conditions have done in this paper.

论文以2，4-二氟硝基苯为主要原料，研究了其与亲核试剂醇钠(甲醇、乙醇、丙醇、正丁醇、叔丁醇等)在不同溶剂中的反应情况，讨论了在几种代表性的溶剂——醇、四氢呋喃、苯、N，N-二甲基甲酰胺中亲核取代反应的情况，研究了温度、反应时间、亲核试剂、溶剂等条件对亲核取代反应的影响。

The anodic oxidation reactions of borohydride ion involves a novel and complex reaction system of three hydrogen valence states: protide H(superscript --protium H(superscript 0*-proton H(superscript +. Based on cyclic voltammetry and polarization studies, a multi-step mechanism for the oxidation of BH4-on Cu anode in NaOH solution was presented, and a kinetic expression containing the coverages of BH(superscript - subscript 4) and OH-adsorbed on the surface of Cu anode was deduced by the steady state approximation theory.

鉴于BH(上标-下标 4)阳极氧化反应涉及一个复杂的氢负离子H(上标-下标 4)－氢单原子H(上标 0*)－质子H之间价态转化的新颖反应体系，在循环伏安和极化实验研究基础上，提出了NaOH溶液中BH(上标-下标 4)在Cu电极上氧化反应的多步骤机理，导出了包含表面吸附态BH(上标-下标 4， ad)和OH覆盖率θ和θ的电极反应动力学方程。

The effects of molar ratio of linoleic acid and ethanol, temperature , and amount of ionic liquid on esterification reaction were studied and the optimal reaction conditions were obtained, that is, n :n = 4:1 , at refluence temperature, with the amount of ionic liquid equaling 42wt.

研究了环境友好的BF4离子液体催化亚油酸等高碳脂肪酸与无水乙醇酯化反应，考察了亚油酸与乙醇的摩尔比、反应温度、离子液体用量等条件对亚油酸酯化反应结果的影响，优化了反应的工艺条件。

The obtained activation barrier of β-scission of 1-butene is 217 kJmol^(-1) in the reverse reaction of ethene dimerization.

反应的逆过程也就是1-丁烯在酸性分子筛表面的1-丁基烷氧化合物发生B分裂反应，计算所得相应的l-丁烯B分裂反应的能垒为217kJmol^(-1)，远高于相应的乙烯二聚反应能垒。

Secondly,the synthesis of SIPE and the reaction conditions such as catalyst,anti-ether agent,temperature and water are researched to control the generation of diethylene glycol and the self-polymerization of SIPM by controlling the total quantum of distillate and the temperature of distillation column and reaction and the reliable synthetic conditions of SIPE are obtained.

其次，在此基础上，研究了三单体的中间体SIPE的合成工艺，研究了催化剂、抑醚剂、反应温度及水分等对合成反应的影响，同时提出了控制馏出物总量、控制分馏柱温度和控制反应温度等措施来控制二甘醇生成反应和SIPM自聚等副反应，得到了可靠的SIPE合成工艺。

Being combining with products distribution in styrene oxidation, we propose the styrene epoxidation carry out with Ti metallacyclo intermediates, And at the same time Ti-ZSM-5 have properties both catalytic epoxidation and acid-catalysis, namely the skeletal Ti can catalyze styrene epoxidation to styrene oxide and the skeletal Ti and Al can provide Lewis acid site to cause the rearrangement of styrene oxide to phenylacetaldehyde rapidly, the solvolysis to glycols and the cleavage of C=C double bond. Ti-ZSM-5 can also provide Bronsted acid site simultaneously, which is also catalytic center for the solvolysis to glycols.

同时结合Ti-ZSM-5催化选择性氧化苯乙烯反应的产物分布结果，提出苯乙烯环氧化反应可能是通过金属有机环机理进行；Ti-ZSM-5同时具有催化环氧化和酸催化两种功能，其骨架钛可催化苯乙烯环氧化生成环氧苯乙烷，而骨架钛和骨架铝等可提供Lewis酸位使环氧苯乙烷迅速发生重排生成苯乙醛从而使其成为反应的主要产物，同时还可发生加成以及碳碳键的裂解等副反应：Ti-ZSM-5也提供Bronsted酸位，它也是生成加成产物的活性中心。

During the low temperature plasma polymerization, different factors (reaction power, pulse duty factor, reaction time, bias voltage and pressure) were investigated to get the best film. The results of X-ray photoelectron spectroscopy and Fourier transformed infrared spectoscopy implied that polymer nano-film containing carboxyl or amido were deposited successfully by using allylamine or acrylic acid as a reagent, respectively.

低温等离子聚合过程中，研究了反应的功率、脉冲占空比、反应时间、偏压、反应室压强这五个因素对薄膜性质的影响，确定了最佳的工艺参数。X光电子能谱和傅立叶转换红外光谱分析结果表明，以丙烯胺和丙烯酸为反应物可以在样品表面分别得到含有羧基或氨基的有机薄膜。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失