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In the presence of SnCl2- C6H5Me3NBr and microwave irradiation, the mixture of tin-indium and propargyl bromide reacted quickly with aldehydes in aqueous media to produce the homopropargyl alcohols exclusively in high yields.

在SnCl2 和C6H5Me3NBr存在及微波照射下,锡-铟和炔丙基溴的混合物在水介质中与醛快速反应,生成高产率的单一的高炔丙醇。

Promoted by metal dysprosium, aldehydes and ketones could react smoothly with propargyl bromide to afford the corresponding homopropargylic alcohol s in good to excellent yields, and no allenic alcohols were found.

在金属镝的促进下,醛、酮可与炔丙基溴反应,高选择性高产率地得到相应的高炔丙醇,没有发现连二烯醇的存在。

A group of pyrylium salts with different substituents has been synthesized in this work. Their fluorescence life time, quantum yield and quenching constant by BVE have also been measured. It was found that a strong interaction was observed between BVE and pyrylium salt which contains an electron-withdrawing group, and contrary, the introduction of electron-repulsive groups to the pyrylium salt will decrease this effect. It indicated that these reactions possess the characteristic of electron transfer.

本工作合成了一组带不同取代基的氧鎓盐化合物,并对它们的荧光寿命、荧光量子产率以及用丁基乙烯基醚进行猝灭的荧光猝灭常数进行了测定,发现带拉电子基的氧鎓盐化合物和BVE间存在着较强的相互作用,相反,推电子基的引入则减弱了这种影响,表明反应具有电子转移性质。

METHODS: 124 patients with RA were assessed at baseline and after 10 years with inflammatory markers calprotectin, C-reactive protein (CRP, erythrocyte sedimentation rate, serological variables antibodies to cyclic citrullinated peptide (anti-CCP, IgA rheumatoid factor and IgM RF and radiographic and clinical assessments of joint damage hand radiographs and Rheumatoid Arthritis Articular Damage (RAAD score.

我们对患者在试验基线时和10年后分别进行了评估,测定其炎症标志物(钙卫蛋白、C反应蛋白CRP、红细胞沉降率ESR)水平,血清学变量(抗环瓜氨酸肽抗体Anti-CCP、IgA风湿因子RF、IgM风湿因子)水平,以及关节损害的放射影像学表现和临床表现(手部的X线片、风湿性关节炎关节损害RAAD评分)等。

The synthesis of water reducing agents from phenanthrene waste by sulfonation,condensation,neutralization and recondensation has been studied by the orthogonal test.

利用正交实验通过磺化、缩合、中和、再缩合反应对菲渣制取水泥减水剂进行了研究,优化了主要工艺条件,制备出的减水剂减水率可达17.5%。

Results EROD activities in liver of wild crucian from Zhangtan, Jiangjunyan, Fuyang and Wenyan (23.51±4.17, 16.79±7.39, 18.74±5.16, 18.65±8.86 nmol/) were significantly higher than that of Jiekou (7.84±2.42 nmol/g promin), and no difference was observed between the other sites and Jiekou. Three dose groups (0.25, 0.50, 1.00L/dish water sample extracts) were used in Ames test. Reversional mutation rate of TA98 colony exposed to extracts from Zhangtan was 2.21, 3.39, 6.95 without S9, and 2.70, 4.07, 6.23 with S9, respectively. The revesional mutation of TA100 colony was 2.55, 2.81, 5.36 without S9, and 1.73, 2.86, 4.14 with S9, respectively. Reversional mutation rate of TA98 colony exposed to 1.00L/dish extracts from Jiangjunyan with S9 was 2.22, and there was a dose-response relationship in reversional colony count. Ames tests of the other extracts were negative.

结果 樟潭、将军岩、富阳、闻堰点位野生鲫鱼肝EROD酶活性分别为(23.51±4.17),(16.79±7.39),(18.74±5.16),(18.65±8.86)nmol/,明显高于街口[(7.84±2.42)nmol/],其他点位与对照比较差异无统计学意义;樟潭水样浓集物在浓度为0.25,0.50,1.00 L/皿时在不加与加S9条件下,TA98回变菌落突变率MR值分别为2.21,3.39,6.95,2.70,4.07,6.23;TA100回变菌落MR值分别为2.55,2.81,5.36,1.73,2.86,4.14;Ames试验结果为明显阳性;将军岩水样浓集物在浓度为1.00 L/皿且加S9条件下TA98MR值为2.22,且在浓度为0.25,0.50,1.00 L/皿加S9条件下TA98回变菌落数呈剂量-反应关系,MR值分别为0.88,1.98,2.22;Ames试验结果为弱阳性;其他点位均为阴性。

Antibody to PE could block this function. In vivo PE could enhance murine splenocyte proliferation but not level of IL-2 production.

PE在体内能使小鼠脾淋巴细胞自发淋转率增高,对ConA刺激的增殖反应增强,但对淋巴细胞自发分泌IL-2和ConA诱导IL-2的产生水平无影响。

Results It showed that the sensitivity for pure tone,the discrimination score for speech and cognitive function were decreased,the threshold of stapedial reflex were elevated,the percentage of recruitment ear were increased,but the interpeak latency of ABR were normal,the wave latency of P300 were prolonged,but the amplitude were diminished obviously as compared with yonger group.

结果 与青年组相比,老年人纯音听敏度减退;言语识别率下降,中枢听觉认知功能减退,镫骨肌反射阈有不同程度提高、重振耳数随耳聋加重而增多;听性脑干反应各波间期无变化;P300认知电位波潜伏期延长,波辐下降。

Finally statistical analysis is conducted.Result: Orally taking Xuefu Zhuyu Tang and calming-wind medicines can ease stenocardia,improve ECG,enhance the stopped rate of nitroglycerin,better the heart contraction and dilation,regulate blood fat,promote blood rheology,lower CRP、ET、TXB2,raise NO、6-keto-PGF1αand so on,compired with the control group,it is obviously statically meaningful without obvius adverse reaction.

结果:血府逐瘀汤加治风活络药物内服治疗能有效地缓解心绞痛和临床症状;改善心电图;提高速效扩冠药的停减率;改善心脏的收缩及舒张功能;调节血脂;改善血液流变学;降低CRP、ET、TXB2的水平,升高NO、6-keto-PGF1α的水平等,与对照组相比,有显著的统计学意义,且未发现明显的不良反应。

Removal and recovery of nitrogen and phosphorus from wastewater by struvite crystallization,which has the advantages of high removal rate and rapid reaction rate.

采用磷酸铵镁沉淀法处理含氮磷的废水,具有氮磷去除率高,反应速度快的优点;同时,回收氮磷生成的磷酸铵镁是一种缓释肥,具有良好的经济效益。

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If you have any questions, you can contact me anytime.

如果有任何问题,你可以随时联系我。

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