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Used the PERCA method union tubular mobile technology basically to determine the free radical production of the ozone ethene reaction, the result has been consistent with the literature value.

采用PERCA方法结合管式流动技术测定了臭氧乙烯反应生成的自由基的产率,结果与文献值基本一致。

Results: six patients with vagal reflection were cured by intravenous atropine, 2 with pericardial hemorrhage were treated by pericardiocentesis, 1 patient developed hypotension due to occlusion of the mitral valve orifice by the catheter was corrected by shortening the duration of the catheter in left ventricle, the blood pressure of 1 patient with rapid atrial flutter was elevated by intravenous cedilanid, the blood pressure of 1 patient with hypotension of unknown origin was elevated by vasopressor and atropine.

结果:其中迷走神经反射6例,经静脉注射阿托品纠正;心包出血2例,心包穿刺抽液血压至正常;球囊导管阻塞二尖瓣口1例,缩短导管停留在左心室时间,可以避免低血压反应;快速心房颤动1例,使用西地兰减慢心室率,血压回升;原因不明1例,经使用升压药及阿托品后血压改善。

The molecular structure was clarified by IR, which revealed the existence of ether bonds. The content of tartaric acid and unreacted maleic acid were detected by spectrophotometer. The effect of some factors on the yield of ESA and scale inhibition efficiency of PESA was investigated.

利用红外光谱表征了该产物结构,表明分子链中含有醚键;利用紫外-可见分光光度法测得体系内副产物酒石酸和未反应的马来酸的含量,并系统地研究了各因素对中间产物环氧琥珀酸钠的产率和最终产物聚环氧琥珀酸钠阻垢性能的影响。

The paper introduced three processes to prepare isochroman from β-phenethyl alcohol and polyformaldehyde:HCl catalysis,AlCl_3 catalysis and toluene-p-sulfonic acid catalysis,and discussed its reaction mechanism,using toluene-p-sulfonic acid catalysis method to prepare isochroman ,the yield is 46%,purity is 96%.

用β-苯乙醇和多聚甲醛为原料,进行了HC l催化法,三氯化铝催化法和对甲苯磺酸催化法的合成路线的实验,并对其反应机理进行了探讨,应用对甲苯磺酸催化法合成异色满的合成路线,得率46%,纯度96%。

A method using α methylstyrene as raw material to prepare β methylene phenethyl alcohol,a new rose flavor ,by chlorination,esterification and saponification was studied.

对α 甲基苯乙烯经氯代、酯化、皂化合成新型玫瑰香料β亚甲基苯乙醇的方法进行了研究,选择PTC1作为相转移催化剂,当m∶m (NaAc·3H2 O)∶m (PTC1 )=1 。0 0 0∶0 30 0∶0 0 2 4时,80℃下反应 6h ,产率为 67 3%。

This research utilizes the method of organic synthesis to put different amount of aminophenol into hydroxybenzoic acid or caffeic acid so as to produce a series of high yield of polyhydroxy benzamides (1~40).Through the following different activity tests, discussing the applied value of cosmetics.Ⅰ.

摘要 本研究主要利用有机合成方法,将具有不同数量及在不同位置之羟基取代之安息香酸及咖啡酸分别与胺基苯酚化合物进行醯胺化反应,得到一系列高产率之多酚醯胺类衍生物(1~40),经由下列不同活性测试方法,探讨其化菻~上的应用价值。

By comparing the body weight, immune organs index and response of lymphocytes to ConA, to analyze the effect of QKL on immunological system of normal mouse. Delayed type hypersensitivity mouse model was established by stimulation with dinitrofluorobenzene. By comparing spleen index and swelling rate of pathogenetic ear, to illuminate the immunoregulation of QKL in vivo. Polymicrobial sepsis mouse model was induced by cecal ligation and puncture. The cumulative survival rate was observed in QKL and NS groups. Results: QKL had no influence on body weight and spleen index of normal mouse, but it could significantly decrease thymus index and inhibit the immune response of lymphocytes to ConA.

连续皮下注射QKL 5 d,通过检测小鼠体重、免疫器官指数和淋巴细胞对ConA刺激的反应,分析QKL对正常小鼠免疫功能的影响;采用二硝基氟苯诱发小鼠耳朵肿胀,发生接触性皮炎,建立DTH模型,通过比较QKL与NS对照对小鼠脾脏指数和发病耳肿胀抑制率评价QKL体内对小鼠的免疫调节功能;采用盲肠结扎穿孔术后引起的多细菌性腹膜炎,建立小鼠脓毒症模型,通过观察QKL对小鼠存活状况的影响,评价QKL的免疫调节作用。

The efficacy measure was the Hamilton Depression Rating Scale, 17 items at 0, 1st, 2nd, 3rd, and 4th week. Side effects were classified prescriptively.

分 别在治疗前及第 1 , 2 , 3 , 4 周末以汉密尔顿抑郁量表( 17 项, HAMD )总分减分率评价疗效,并通过心电图、血液检查和描述性记录不良反应。

Long-term complications were as follows: postradiation proctitis and cystisis was 8.33%(5/60). Viginal stenosis, uterine hydropsand was 5%(3/60).Conclusion It is a good method to treat middle and advanced cervical cancer with 3DCRT plus pelvis radiotherapy. It can be easily endured with its convenient operation, short-cycled irradiation and therapy; it is particularly suitable for patients who could not be treated by endovascular.

采用盆腔野加后程三维适形放射治疗对中晚期宫颈癌有较好的局控率与生存率,毒副反应轻,患者易耐受,且操作易行,照射时间及治疗周期短,尤其适合无法进行腔内治疗患者,值得临床进一步研究、应用。

To pronuclear formation rate after oocyte in vitro maturation 18 hours and parthenogenticactivation, oocytes derived from SM is significantly higher than oocytes from PM,oocytes derived from IM is significantly lower that of oocytes detrived from PM and SM.

对于孤雌刺激反应而言,无论是何种类型的卵母细胞成熟18小时后,自发成熟卵母细胞激活后形成原核的比率高于被动成熟的卵母细胞,诱导成熟的卵母细胞的原核形成率显著低于自发和/或被动成熟的卵母细胞。

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