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Low density silicon nitride with about 55% porosity and globed macropores was prepared by reaction-bonded raw silicon powder and adding 30% in mass pore-forming agent of benzoic acid ball-like particles.

以硅粉为原料,添加质量分数为30%的成孔剂球形颗粒,反应烧结制备了气孔率为55%,具有球形宏观孔的低密度多孔氮化硅陶瓷。

Ti-MWW is more attractive by a comparison with those conventional titanosilicates (TS-1,Ti-MCM-41,et al ) in the epoxidation of linear functionalized alkenes, on which the epoxidation of allyl alcohol to glycidol is one of the most industrial promising processes for benign reaction conditions, high yields of the product and environment friendly.

Ti-MWW 对线性官能烯烃的环氧化具有优良的催化性能,特别是对烯丙醇环氧化制缩水甘油的过程,其反应条件温和,产率高,且对环境友好而最具有工业应用前景。

Results After 50 mmol·L-1 Taurine was added to the spleen lymphocyte suspension containing 0.1 mmol·L-1 glycolaldehyde, the cellular DNA damage rates were markedly decreased (P.01) and the migration distances of DNA were significantly reduced (P.01) as compared with positive control group, and Taurine reduced the carbonyl compound contents in a reactive system in a dose-dependent manner.

结果:在0.1 mmol·L-1乙醇醛溶液中加入50 mmol·L-1牛磺酸后,小鼠脾淋巴细胞DNA的损伤率较阳性对照组明显降低(P.01),彗星实验的迁移距离也显著缩短(P.01),牛磺酸呈剂量依赖性明显降低反应体系中乙醇醛的含量。

Methods: PNS was got by extracting panax notognseng with general method of alcohol circumfluence, purified with organic solvents, and separated with D101 macroreticular resin. The hematolysis rate and the immunocompetence of biology of PNS were determined by hemolysis test and experiment of splenocyte proliferation respectively.

乙醇回流法提取PNS粗提物,经有机溶剂除杂后,通过大孔树脂柱层析分离纯化;溶血性试验测定PNS作用后红细胞的溶血率;脾淋巴细胞增殖反应测定PNS的生物免疫活性。

This paper reported the synthesis of 2-hydroxyl-1-naphthalene formaldehyde under microwave irradiation with 2-naphthol, hexamethylenamine, solvent of glacial acetic acide, catalysis of sulphuric acid, and discussed the influence of the time and the power of microwave radiation, the proportion and quantity of reagents to the synthetic yield.

利用微波技术,采用2-萘酚与六次甲基四胺为原料,冰乙酸作溶剂,在浓硫酸的催化下合成2-羟基-1-萘甲醛,并考察了微波作用的时间、微波辐射功率、反应试剂的组成与用量等因素对产物产率的影响。

Non-occluding teeth with a hypofunctional periodontium have a lower rate of bone remodeling, and are more susceptible to the injury in periodontal tissues caused by orthodontic force than normally occluding teeth, such as hyalinization or undermining bone resorption, even dentin resorption.

正畸治疗中,无咬合接触的牙周膜废用性萎缩牙较正常咬合接触牙对矫治力反应差,骨改建率低,易发生玻璃样变和潜掘性骨吸收,延缓牙移动,因此对无咬合接触牙的临床治疗中应采用轻力。

Good thermal stability and self-extinguishing behavior was observed with the cured polybenzoxazine resins. Second, furan-containing benzoxazine monomers, P-FBz, BPA-FBz, and 4FP-FBz were prepared using furfurylamine as a raw material. Formation of furfurylamine Mannich bridge networks in the polymerizations of P-FBz and BPA-FBz increased the cross-linking densities and thermal stability of the resulting polybenzoxazines. P-FBz and BPA-FBz- based polymers also exhibited high glass transition temperatures above 300℃, high char yields, and low flammability with a limited oxygen index value of 31. The dielectric (Dk3.21–3.39) and mechanical properties (high storage modulus of 3.0–3.9 GPa and low coefficient of thermal expansion of 37.7– 45.4 ppm) of the P-FBz and BPA-FBz-based polymers were superior or comparable to other polybenzoxazines. 4FP-FBz used for polybenzo- xazine modification by means of formation of benzoxazine hybridation with P-FBz.

第二部份以2-呋喃甲胺为起始物,制备了P-FBz、4FP-FBz与BPA-FBz 三个含呋喃官能基之氧代氮代苯并环己烷的单体;BPA-FBz与P-FBz於开环聚合中形成之Mannich bridge网状结构有效地提升聚氧代氮代苯并环己烷聚合物之交联密度与热安定性;Poly与Poly具有大於300℃之玻璃转移温度、高的焦炭生成率与具有31之极限氧指数(Limited oxygen index, LOI)的难燃性特质,Poly与Poly之介电常数(Dk=3.21~3.39)与机械性质[3.0~3.9 GPa的储存模数与37.7~45.4ppm之低热膨胀系数( Low coefficient of thermal expansion, Low CTE)]均较其他聚氧代氮代苯并环己烷为优;4FP-FBz具有低之介电常数(Dk=2.7),以其作为降低介电常数之反应型改质剂,与P-FBz混成,证实可有效地降低Poly的介电常数。

The lappaconitine hydrobromide was synthesized in a new way,with a yield of 84%.

同时用制备方法操作简便,反应条件温和的新方法合成了强镇痛药物刺乌头碱氢溴酸盐,产率可达84%。

The secondary hydrogenization of tar is the principal procedure to produce HCL. The pyrolysis water produced in H 2 atmosphere is more than that produced in N 2 atomosphere.

轻质烃产率与焦油生成量有关,焦油加氢二次反应是轻质烃生成的主要途径。

However, when indoles were used, the yield can still reach 97% within 40 min..

但当底物为活性较高的吲哚类化合物时,产率最高也可以达到97%,反应时间一般在40分钟以内。

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In the United States, chronic alcoholism and hepatitis C are the most common ones.

在美国,慢性酒精中毒,肝炎是最常见的。

If you have any questions, you can contact me anytime.

如果有任何问题,你可以随时联系我。

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很漂亮,不过停机坪更迷人。那人俏皮地答道。