反应率

Thirteen benzimidazole derivatives were synthesized by one-step oxidative cyclisation of 1, 2-phenylenediamine or 4-methyl-1, 2-phenylenediamine at room temperature and a series of aromatic aldehydes under imidazolium salt grafted iodobenzene diacetate assisted.

以水为溶剂，在咪唑盐二醋酸碘苯促进下，通过邻苯二胺或4-甲基邻苯二胺与各种芳醛室温氧化环合，一步合成了13种苯并咪唑类衍生物，反应时间25~45 min，反应产率92%~98%。

The effects of catalyst synthesis and esterification reaction conditions on the yield of the isoamyl acetate were investigated.

将该催化剂用于醇酸反应制备乙酸异戊酯，考察了反应条件对酯化率的影响。

This paper studied the synthesis of isoamyl acetate using silver phosphotungstomolybdate heteroployacid as catalyst.

制备了固体磷钼钨杂多酸银盐，并以此为催化剂，对醋酸异戊酯的合成反应进行了研究，探讨了催化剂用量、醇酸摩尔比、反应时间和催化剂重复使用对酯产率的影响。

Synthesis of biodiesel by transesterification of rapeseed oil and methanol catalyzed by KOH/Al2O3 solid base was studied. The catalyst was prepared by isochoric impregnation. Effects of some factors on the transesterification were investigated systematically and reaction conditions were optimized. The optimum reaction conditions on KOH/Al2O3 catalyst were: mass ratio of KOH to Al2O3 20%; calcination temperature 400℃ for 5h; molar ratio of methanol to oil 12:1, the amount of catalyst 5wt%; reaction temperature 60℃ and reaction time 2h.

采用等体积浸渍法制备了KOH/Al2O3负载型固体碱催化剂，并将其用于菜籽油与甲醇酯交换法合成生物柴油的研究；分别考察了催化剂附载量、锻烧温度、醇油摩尔比、反应温度、反应时间等条件对生物柴油产率的影响；结果表明：用等体积浸渍法，在400℃煅烧5h，制得负载量为20%的KOH/Al2O3催化剂。

The results showed that molar ratio of cyclohexanone to ethylene glycol was 1∶1.4, the amount of catalyst was 2% cyclohexanone, amount of cyclohexane was 10 mL, the reaction time 2 h, the yield of cyclohexanone ethylene ketal reached 99.6% under the optimum condition.

通过正交实验得出了最佳反应条件：n∶n=1∶1.4、催化剂用量为环己酮质量的2%、带水剂环己烷用量10.0 mL、反应时间2 h，缩酮产率可达99.6%。

The results indicated the order of factors that influence the oil transesterification ratio within the experimental range was as follows: the rate of rotation r＞catalyst dosage＞mole ratio of methanol to Kosteletzkya virginica oil ＞reaction time＞reaction temperature.

结果表明，在试验范围内各影响因素对酯交换率作用的大小依次为：搅拌强度＞催化剂用量＞醇油摩尔比＞反应时间＞反应温度。

In this paper,with respect to the low reactive activity of ludwigite from Wengquangou for the manufacture of borax by the CO2-soda process,a kind of composite additive was employed for the calcination of ludwigite.

针对碳碱法加工翁泉沟硼铁矿生产硼砂过程中存在的矿石活性低等问题，通过添加复合添加剂对硼铁矿进行活化焙烧，用常压碱解率评价焙烧矿的反应活性，分别考察了复合添加剂用量、焙烧温度以及焙烧时间对翁泉沟硼铁矿反应活性的影响。

The graft polymerization of maleic a...

研究了马来酸酐在PE颗粒中的接枝反应，考察了反应条件对接枝率和酸值的影响。

The free-radical addition reaction of malonic ester with a series of alkenes under the uniform conditions has been studied.

在相同反应条件下，进行一系列烯烃与丙二酸二乙酯的加成反应，求得产率与烯烃结构间的定量关系，即反S型曲线。

The optimum reaction conditions were: at present of acetic anhydride, a stoichiometric quantity of nitric acid, at room temperature for 40 minutes. Nitration of chlorobenzene gave a,50% yield of mononitro compounds, and an ortho-para isomer ratio 0.20 in product distribution of chlorobenzene mononitration.

结果表明：硅钨酸催化性能较好，催化剂载体以纳米二氧化硅最好，反应条件中醋酸酐用量是主要影响因素；SiW_(12)O_(40)~(4-)／纳米SiO_2催化剂具有强对位选择性：在醋酸酐存在下，氯苯与等当量的硝酸室温下反应40分钟，氯苯一硝化产物中邻／对硝基氯苯异构体的质量比达0.2，产率可达50％。

She gently rebuff ed him, but agreed that they could be friends

她婉言拒绝了，但同意作为朋友相处。

If in the penal farm, you were sure to be criticized.

要是在劳改农场，你等着挨绳子吧！